VERFAHREN ZUR HERSTELLUNG VON CAPROLACTAM AUS 6-AMINOCAPRONITRIL
    5.
    发明授权
    VERFAHREN ZUR HERSTELLUNG VON CAPROLACTAM AUS 6-AMINOCAPRONITRIL 有权
    用于生产己内酰胺OFF 6-氨基己腈

    公开(公告)号:EP1280768B1

    公开(公告)日:2009-12-09

    申请号:EP01951465.2

    申请日:2001-04-30

    Applicant: BASF SE

    CPC classification number: C07D201/08 C07D201/16

    Abstract: The invention relates to a method for producing caprolactam, characterized in that a) a mixture (I) containing 6-aminocapronitrile and water in the liquid phase is converted into a mixture (II) containing caprolactam, ammonia, water, high boilers and low boilers in the presence of a catalyst; b) ammonia is then removed from mixture (II), leaving a mixture (III) containing caprolactam, water, high boilers and low boilers; c) water is then removed from mixture (III) leaving a mixture (IV) containing caprolactam, high boilers and low boilers, and d) a solid (V) containing caprolactam is obtained from mixture (IV) by crystallization, the proportion by weight of caprolactam in the solid (V) being greater than that in the mixture (IV).

    VERFAHREN ZUR REINIGUNG VON N2O
    10.
    发明公开
    VERFAHREN ZUR REINIGUNG VON N2O 有权
    清理方法氧化亚氮

    公开(公告)号:EP2271584A1

    公开(公告)日:2011-01-12

    申请号:EP09727777.6

    申请日:2009-03-13

    Applicant: BASF SE

    CPC classification number: C01B21/22 C07C45/28 C07C49/607

    Abstract: The present invention relates to a process for purifying a gas mixture containing dinitrogen monoxide at least comprising treatment of a gas mixture G-O containing dinitrogen monoxide with a gas mixture G-A being obtained, at least comprising the absorption of the gas mixture G-O in a solvent mixture LM-I with an off-gas stream and a composition Z-A being obtained, and desorption of a gas mixture G-1 from the composition Z-A with a solvent mixture LM-I' being obtained, subsequent condensation of the gas mixture G-A with a liquid composition Z-1 containing dinitrogen monoxide and a gaseous mixture G-K being obtained, wherein the gaseous mixture G-K is recirculated to the process.

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