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1.发明授权VERFAHREN DER WIEDERBESCHICKUNG DER REAKTIONSROHRE EINES ROHRBÜNDELREAKTORS MIT EINEM NEUEN KATALYSATORFESTBETT 无效方法RE馈送管式反应器的反应管中新的催化剂固定床
公开(公告)号：EP2155376B1
公开(公告)日：2012-07-11
申请号：EP08760298.3
申请日：2008-05-30
申请人： BASF SE
发明人： SCHLIEPHAKE, Volker , BOTT, Klaus , BECHER, Rolf-Dieter , MÜLLER-ENGEL, Klaus Joachim , PETZOLDT, Jochen , CREMER, Ulrich , RAICHLE, Andreas
IPC分类号： B01J8/06
CPC分类号： C07C51/252 , B01J8/0045 , B01J8/06 , B01J2208/00761 , B08B9/0436 , C07C45/35
摘要： A method of recharging the reaction tubes of a tube-bundle reactor with a new catalyst fixed bed in which a heterogeneously catalysed partial gas phase oxidation of an organic compound has been carried out in advance in a precursor catalyst fixed bed having Mo-containing multielement oxidative compositions and with formation of a steam-containing product gas mixture, in which, before the recharging, molybdenum oxide and/or molybdenum oxide hydrate-containing solid coating deposited on the tube interior walls is brushed off using a brush.
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2.发明授权VERFAHREN ZUR RÜCKSPALTUNG VON IN EINER FLÜSSIGKEIT F ENTHALTENEN MICHAEL-ADDUKTEN, DIE BEI DER HERSTELLUNG VON ACRYLSÄURE ODER DEREN ESTER GEBILDET WURDEN 有权用于备份斯普利特所载˚F迈克尔液态法，加合物涉及丙烯酸的生产，取得了酯类化合物
公开(公告)号：EP2376417B1
公开(公告)日：2016-10-19
申请号：EP09768013.6
申请日：2009-11-30
申请人： BASF SE
发明人： SCHLIEPHAKE, Volker , FRIESE, Thorsten , BOTT, Klaus , BLECHSCHMITT, Michael , BLUM, Till , MÜLLER-ENGEL, Klaus, Joachim
IPC分类号： C07C51/42
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3.发明公开VERFAHREN ZUR RÜCKSPALTUNG VON IN EINER FLÜSSIGKEIT F ENTHALTENEN MICHAEL-ADDUKTEN, DIE BEI DER HERSTELLUNG VON ACRYLSÄURE ODER DEREN ESTER GEBILDET WURDEN 有权用于备份斯普利特所载˚F迈克尔液态法，加合物涉及丙烯酸的生产，取得了酯类化合物
公开(公告)号：EP2376417A2
公开(公告)日：2011-10-19
申请号：EP09768013.6
申请日：2009-11-30
申请人： BASF SE
发明人： SCHLIEPHAKE, Volker , FRIESE, Thorsten , BOTT, Klaus , BLECHSCHMITT, Michael , BLUM, Till , MÜLLER-ENGEL, Klaus, Joachim
IPC分类号： C07C51/42
摘要： The invention relates to a method for cleaving Michael adducts that are contained in a fluid F at a weight proportion of ≥ 10 wt % and that were formed in the production of acrylic acid or esters thereof, in a cleaving device, which comprises a pump P and a separation column K having installations that effect separation and a recirculation heat exchanger UW, wherein for the purpose of feeding the cleaving energy, the pump P draws sump fluid from the sump chamber of the separation column K and continuously feeds said sump fluid back into the sump chamber above the level of the sump fluid through the recirculation heat exchanger UW, and wherein the pump P is a radial centrifugal pump having an open impeller.
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4.发明公开VERFAHREN DER WIEDERBESCHICKUNG DER REAKTIONSROHRE EINES ROHRBÜNDELREAKTORS MIT EINEM NEUEN KATALYSATORFESTBETT 无效方法RE馈送管式反应器的反应管中新的催化剂固定床
公开(公告)号：EP2155376A1
公开(公告)日：2010-02-24
申请号：EP08760298.3
申请日：2008-05-30
申请人： BASF SE
发明人： SCHLIEPHAKE, Volker , BOTT, Klaus , BECHER, Rolf-Dieter , MÜLLER-ENGEL, Klaus Joachim , PETZOLDT, Jochen , CREMER, Ulrich , RAICHLE, Andreas
IPC分类号： B01J8/06
CPC分类号： C07C51/252 , B01J8/0045 , B01J8/06 , B01J2208/00761 , B08B9/0436 , C07C45/35
摘要： A method of recharging the reaction tubes of a tube-bundle reactor with a new catalyst fixed bed in which a heterogeneously catalysed partial gas phase oxidation of an organic compound has been carried out in advance in a precursor catalyst fixed bed having Mo-containing multielement oxidative compositions and with formation of a steam-containing product gas mixture, in which, before the recharging, molybdenum oxide and/or molybdenum oxide hydrate-containing solid coating deposited on the tube interior walls is brushed off using a brush.
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