VERFAHREN ZUR HERSTELLUNG VON HALOGENE ENTHALTENDEN ORGANISCHEN PHOSPHORVERBINDUNGEN
    3.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON HALOGENE ENTHALTENDEN ORGANISCHEN PHOSPHORVERBINDUNGEN 有权
    用于生产含HALOGENE有机磷剂

    公开(公告)号:EP2044092A1

    公开(公告)日:2009-04-08

    申请号:EP07787009.5

    申请日:2007-07-03

    申请人: BASF SE

    IPC分类号: C07F9/48

    CPC分类号: C07F9/4891 C07F9/4875

    摘要: The invention relates to a method for producing compounds of general formula XPR2(OR1) (Ia), wherein X represents chlorine, bromine or iodine and R1 represents an organic radical, by reacting compounds of general formula X2PR2 (II), wherein X has the above-mentioned meaning and R2 represents an organic radical, with compounds of general formula R1OH (III), wherein R1 has the above-mentioned meaning, to form a mixture IV, wherein a) the secondary reaction is carried out at a temperature of between 50 to 240°C and at a pressure of 0,001 to 0,9 bar, b) from the mixture IV, the compounds (Ia) are separated from the compounds PR2(OR1)2 (Ib) and optionally from the compounds II and c) compounds (Ib) and optionally non-reacted compounds II are guided back to the synthesis step.