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    PROCESS FOR MAKING LITHIATED TRANSITION METAL OXIDES
    1.
    发明公开
    PROCESS FOR MAKING LITHIATED TRANSITION METAL OXIDES 有权
    制备锂过渡金属氧化物的方法

    公开(公告)号：EP3224882A2

    公开(公告)日：2017-10-04

    申请号：EP15795202.9

    申请日：2015-11-18

    Applicant: BASF SE

    Inventor： VOLKOV, Aleksei ,  SCHULZ-DOBRICK, Martin ,  SCHRÖDLE, Simon ,  LAMPERT, Jordan

    IPC: H01M4/36 ,  H01M4/505 ,  H01M4/525 ,  H01M4/58 ,  C01G53/00

    CPC classification number: H01M4/364 ,  C01G53/50 ,  C01P2004/50 ,  C01P2004/51 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/11 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/40 ,  H01M4/505 ,  H01M4/525 ,  H01M4/5825 ,  H01M4/623 ,  H01M4/625 ,  H01M10/0525 ,  H01M2004/028

    Abstract: The present invention is directed towards a process for making a lithiated transition metal oxide, said process comprising the following steps: (a) providing a precursor selected from mixed oxides, hydroxides, oxyhydroxides, and carbonates of nickel and at least one transition metal selected from manganese and cobalt, wherein at least 45 mole-% of the cations of the precursor are Ni cations, (b) mixing said precursor with at least one lithium salt selected from LiOH, Li2O, Li2CO3, and LiNO3, thereby obtaining a mixture, (c) adding at least one phosphorus compound of general formula (I) XyH3−yPO4 (I) wherein X is selected from NH4 and Li, y is 1 or 2, to the mixture obtained in step (b), wherein steps (b) and (c) may be performed consecutively or simultaneously, treating the mixture so obtained at a temperature in the range of from 650 to 950° C.

    Abstract translation: 本发明涉及一种制备锂化过渡金属氧化物的方法，所述方法包括以下步骤：（a）提供选自镍的混合氧化物，氢氧化物，羟基氧化物和碳酸盐以及至少一种选自 锰和钴，其中前体的阳离子的至少45摩尔％为Ni阳离子，（b）将所述前体与选自LiOH，Li 2 O，Li 2 CO 3和LiNO 3中的至少一种锂盐混合，由此获得混合物，（ c）向步骤（b）中获得的混合物中加入至少一种通式（I）X y H 3-y PO 4（I）的磷化合物，其中X选自NH 4和Li，y为1或2，其中步骤（b） 和（c）可以连续或同时进行，在650-950℃的温度下处理如此得到的混合物。

    VERFAHREN ZUR HERSTELLUNG VON WÄSSRIGEN LÖSUNGEN VON KOBALTSULFAT
    5.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON WÄSSRIGEN LÖSUNGEN VON KOBALTSULFAT 有权
    VERFAHREN ZUR HERSTELLUNG VONWÄSSRIGENLÖSUNGENVON KOBALTSULFAT

    公开(公告)号：EP2872447A1

    公开(公告)日：2015-05-20

    申请号：EP13732498.4

    申请日：2013-06-28

    Applicant: BASF SE

    Inventor： SCHRÖDLE, Simon ,  WAGNER, Oliver

    IPC: C01G51/10

    CPC classification number: C01G51/10 ,  C01P2006/80

    Abstract: The invention relates to a method for producing an aqueous cobalt sulphate solution having a pH value of at least 4, characterised in that (a) metallic cobalt dissolves in aqueous sulfuric acid in an atmosphere which is low in oxygen, hydrogen or inert gas, and (b) the thus produced acidic cobalt sulphate solution is treated with oxygen, oxygen-containing gas or a substance which can eliminate the oxygen in an aqueous medium.

    Abstract translation: 本发明涉及一种生产pH值至少为4的硫酸钴水溶液的方法，其特征在于（a）金属钴溶解在氧气，氢气或惰性气体含量低的气氛中的硫酸水溶液中，和 （b）用氧气，含氧气体或能消除含水介质中的氧的物质处理这样产生的酸性硫酸钴溶液。

    VERFAHREN ZUR HERSTELLUNG VON ÜBERGANGSMETALLCARBONATEN
    6.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON ÜBERGANGSMETALLCARBONATEN 有权
    VERFAHREN ZUR HERSTELLUNG VONÜBERGANGSMETALLCARBONATEN

    公开(公告)号：EP2663528A2

    公开(公告)日：2013-11-20

    申请号：EP12700046.1

    申请日：2012-01-09

    Applicant: BASF SE

    Inventor： SCHULZ-DOBRICK, Martin ,  SCHRÖDLE, Simon

    IPC: C01G53/00 ,  C01B31/24

    CPC classification number: C01G53/006 ,  C01B32/60 ,  C01P2004/32 ,  C01P2004/61 ,  C01P2006/11 ,  C01P2006/16 ,  H01M4/505 ,  H01M4/525 ,  H01M4/5825

    Abstract: The invention relates to a method for producing transition metal carbonates having an average particle diameter in the range from 6 to 19 µm (D50), characterized in that at least one solution of at least one transition metal salt is combined with at least one solution of at least one alkali metal carbonate or alkali metal hydrogen carbonate in a stirring vessel, whereby an aqueous suspension of transition metal carbonate is produced. The invention is also characterized in that, in at least one further compartment, a mechanical power in the range from 50 to 10000 W/I is continuously applied to a fraction of the suspension, with respect to the fraction of the suspension, and that the fraction is subsequently fed back into the stirring vessel.

    Abstract translation: 本发明涉及制备平均粒径为6-19μm（D50）的过渡金属碳酸盐的方法，其特征在于将至少一种过渡金属盐的至少一种溶液与至少一种 至少一种碱金属碳酸盐或碱金属碳酸氢盐在搅拌容器中，由此生成过渡金属碳酸盐的含水悬浮液。 本发明的特征还在于，在至少一个另外的隔室中，相对于悬浮液的部分，将50至10000W / l范围内的机械功率连续地施加至一部分悬浮液，并且 随后将馏分返回到搅拌容器中。

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