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    MESOPORÖSES METALLORGANISCHES GERÜSTMATERIAL
    1.
    发明公开
    MESOPORÖSES METALLORGANISCHES GERÜSTMATERIAL 有权
    中孔金属 - 有机骨架

    公开(公告)号：EP1917228A1

    公开(公告)日：2008-05-07

    申请号：EP06792831.7

    申请日：2006-08-16

    Applicant: BASF SE

    Inventor： SCHUBERT, Markus ,  MÜLLER, Ulrich ,  MATTENHEIMER, Hendrick ,  TONIGOLD, Markus

    IPC: C07C51/41 ,  C07F5/06 ,  C01B3/00

    CPC classification number: C07F5/069 ,  C01B3/001 ,  C01B3/0015 ,  C01B3/0026 ,  C07C51/418 ,  Y02E60/327 ,  Y02E60/328 ,  C07C63/307

    Abstract: The invention relates to porous metal-organic framework comprising Al'' and at least one at least bidentate compound. The at least one at least bidentate compound is a six-membered aromatic hydrocarbon ring A, wherein one ore more ring carbon atoms may be replaced by nitrogen and the three substituents X and optionally one or more substituents selected from the group including R, NRR', OR, SR, F, Cl, and Br, wherein R, R' independently represent hydrogen, methyl which is optionally substituted by one or more fluorine atoms or ethyl which is optionally substituted by one or more fluorine atoms and every X independently represents C(=O)O-, C(=S)O-, C(=O)S-, C(=S)S- or the protonized form thereof. The invention also relates to methods for producing said framework and to the use of the novel metal-organic framework.

    VERFAHREN ZUR HERSTELLUNG KUPFERHALTIGER METALLORGANISCHER GERÜSTMATERIALIEN
    5.
    发明公开
    VERFAHREN ZUR HERSTELLUNG KUPFERHALTIGER METALLORGANISCHER GERÜSTMATERIALIEN 有权
    用于生产铜的有机金属骨架材料

    公开(公告)号：EP2049550A1

    公开(公告)日：2009-04-22

    申请号：EP07787520.1

    申请日：2007-07-13

    Applicant: BASF SE

    Inventor： SCHUBERT, Markus ,  ÖZKIRIM, Faruk ,  KIENER, Christoph ,  MÜLLER, Ulrich ,  TONIGOLD, Markus

    IPC: C07F1/00

    CPC classification number: C07F1/005

    Abstract: The present invention relates to methods for producing a porous, organometallic framework material containing a first and at least one second at least bidentate organic compound coordinatively bound to at least one copper ion, including the following steps: (a) Reaction of a reaction mixture in the liquid phase containing at least one copper compound and the first at least bidentate organic compound with formation of a complex intermediate containing at least one copper ion and the first at least bidentate organic compound, wherein the first at least bidentate organic compound derives from a dicarboxylic acid and has a hydrocarbon framework, and (b) Reaction of the complex intermediate with the at least second at least bidentate organic compound, wherein the at least second at least bidentate organic compound is an optionally substituted monocyclic, bicyclic or polycyclic saturated or unsaturated hydrocarbon in which at least two ring carbon atoms are replaced by heteroatoms selected from the group consisting of N, O and S, wherein the reaction mixture in step (a) has less than a threefold excess amount of 25 formic acid based on the copper used in the copper compound.

    MESOPORÖSES METALLORGANISCHES GERÜSTMATERIAL
    6.
    发明授权
    MESOPORÖSES METALLORGANISCHES GERÜSTMATERIAL 有权
    中孔金属 - 有机骨架

    公开(公告)号：EP1917228B1

    公开(公告)日：2010-11-24

    申请号：EP06792831.7

    申请日：2006-08-16

    Applicant: BASF SE

    Inventor： SCHUBERT, Markus ,  MÜLLER, Ulrich ,  MATTENHEIMER, Hendrick ,  TONIGOLD, Markus

    IPC: C07C51/41 ,  C07F5/06 ,  C01B3/00

    CPC classification number: C07F5/069 ,  C01B3/001 ,  C01B3/0015 ,  C01B3/0026 ,  C07C51/418 ,  Y02E60/327 ,  Y02E60/328 ,  C07C63/307

    Abstract: The invention relates to porous metal-organic framework comprising Al'' and at least one at least bidentate compound. The at least one at least bidentate compound is a six-membered aromatic hydrocarbon ring A, wherein one ore more ring carbon atoms may be replaced by nitrogen and the three substituents X and optionally one or more substituents selected from the group including R, NRR', OR, SR, F, Cl, and Br, wherein R, R' independently represent hydrogen, methyl which is optionally substituted by one or more fluorine atoms or ethyl which is optionally substituted by one or more fluorine atoms and every X independently represents C(=O)O-, C(=S)O-, C(=O)S-, C(=S)S- or the protonized form thereof. The invention also relates to methods for producing said framework and to the use of the novel metal-organic framework.

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