摘要:
The invention relates to a method for purifying unsaturated compounds, wherein the purification is carried out in a plant with at least two evaporators and the evaporators are connected such that a part of the unsaturated compound runs in a circuit wherein the vapour condensed in the first evaporator is isolated and the vapour condensed in the second evaporator is introduced into the first evaporator, characterised in that the mass flow with which the condensed vapours in the first evaporator are isolated from the mixture for purifying is less than the mass flow with which the condensed vapours from the second evaporator are introduced into the first evaporator. The invention further relates to a plant for carrying out said method, comprising at least three evaporators connected to each other such that the residue in the liquid state from the first evaporator can be introduced into the second condenser, the condensed vapours from the second evaporator can be introduced into the first evaporator and the liquid phase residue in the second evaporator can be introduced into the third evaporator and the condensed vapours from the third evaporator cab introduced into second evaporator.
摘要:
The invention relates to a method for continuously producing alkylamino(meth)acrylamides by reacting alkyl(meth)acrylates with high-boiling amines. A catalyst activation and special regeneration technique allow for product qualities that have not yet been achieved. Furthermore, very high space-time and total yields can be achieved.
摘要:
The present invention relates to a method for purifying monomers, wherein at least part of the monomers present in a starting composition is evaporated and is subsequently condensed, characterized in that at least part of the starting composition is evaporated in a short path evaporator, wherein the mass flow density of the vapors m is selected according to the relation (I), where M is the average molecular mass of the vapors in the short path evaporator in kg/kmol, T is the temperature of the vapors in K, p i is the pressure in the short path evaporator in mbar, and m is the mass flow density of the vapors in kg/(m 2. h). The present invention further relates to a system for carrying out the method.
摘要:
The invention relates to a composition comprising at least one hydroxyalkyl(meth)acrylate which composition is stabilized for purification and contains at least one hydroquinone monomethyl ether and 4-hydroxy-2,2,6,6-tetramethylpiperidino-N-oxyl. The invention further relates to methods for purifying and for producing hydroxyalkyl(meth)acrylates. The invention also relates to a composition which can be obtained by said methods.