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    PROCESS FOR PRODUCING AMIDE COMPOUND
    3.
    发明公开
    PROCESS FOR PRODUCING AMIDE COMPOUND 审中-公开
    VERFAHREN ZUR HERSTELLUNG EINER AMIDVERBINDUNG

    公开(公告)号：EP3135767A1

    公开(公告)日：2017-03-01

    申请号：EP16187709.7

    申请日：2006-10-06

    申请人： Mitsui Chemicals, Inc.

    发明人： SHIBAMOTO, Hiroko ,  AIKAWA, Toshikazu ,  ARII, Teruo ,  MURAMOTO, Masanori ,  FUKUDA, Takeshi ,  ITO, Kiyoshi ,  ABE, Takeya ,  HAZAMA, Souichi

    IPC分类号： C12P13/02 ,  C07C233/09 ,  C08F20/56 ,  C07C231/06 ,  C08F220/56 ,  C07C253/32

    CPC分类号： C12P13/00 ,  C07C231/06 ,  C08F220/56 ,  C12P13/02 ,  C07C233/09

    摘要： [PROBLEMS]
    The present invention provides a method for efficiently producing a corresponding amide compound from a nitrile compound by a reaction using a nitrile hydratase and a method for producing an amide-based polymer excellent in quality from the amide compound. In addition, the present invention provides a method for more efficiently producing an acrylamide with higher quality by a microbial catalyst containing a nitrile hydratase and the like and a method for producing an acrylamide-based polymer, which is excellent in hue, has a good balance between the water solubility and the high molecular weight and is also excellent in quality, by using the acrylamide.

    摘要翻译： 本发明提供一种通过使用腈水解酶的反应从腈化合物有效地制备相应的酰胺化合物的方法和由酰胺化合物制备质量优异的酰胺类聚合物的方法。 此外，本发明提供了通过含有腈水合酶等的微生物催化剂更高效地制备丙烯酰胺的方法和色调优异的丙烯酰胺系聚合物的制造方法，具有良好的平衡性 在水溶性和高分子量之间，并且通过使用丙烯酰胺也具有优异的质量。

    PROCESS FOR PRODUCING (METH)ACRYLAMIDE
    5.
    发明公开
    PROCESS FOR PRODUCING (METH)ACRYLAMIDE 审中-公开
    HERSTELLUNGSVERFAHRENFÜR（METH）ACRYLAMID

    公开(公告)号：EP1988172A1

    公开(公告)日：2008-11-05

    申请号：EP07714532.4

    申请日：2007-02-20

    申请人： Mitsui Chemicals, Inc.

    发明人： ABE, Takeya ,  FUKUDA, Takeshi

    IPC分类号： C12P13/02

    CPC分类号： C12P13/02

    摘要： A process for producing high-quality (meth)acrylonitrile efficiently by an action of a microbial catalyst or the like that contains nitrile hydratase is provided.
    The present invention is directed to a process for producing (meth) acrylamide from (meth) acrylonitrile in an aqueous solution that is put in a reactor and relates to one process for producing (meth) acrylamide that includes the steps of (A) to (C) : (A) adding to the reactor a microorganism or a processed product of the microorganism that contains nitrile hydratase; (B) adding to the reactor an alkali; and (C) adding to the reactor (meth) acrylonitrile, in which an addition line used in the step (A), an addition line used in the step (B), and an addition line used in the step (C) are different from one another, and to another process for producing (meth)acrylamide from (meth)acrylonitrile by an action of the microorganism or processed product of the microorganism that produces nitrile hydratase, in which a mixture of (meth)acrylonitrile and water is added to an aqueous solution that is put in a reactor and contains an alkali and a microorganism or a processed product of the microorganism that produces nitrile hydratase through an addition line of the reactor.

    摘要翻译： 提供了通过含有腈水合酶的微生物催化剂等的作用有效地生产高质量（甲基）丙烯腈的方法。 本发明涉及一种在（甲基）丙烯酰胺中由放置在反应器中的水溶液中制备（甲基）丙烯酰胺的方法，涉及一种制备（甲基）丙烯酰胺的方法，该方法包括步骤（A）至（ C）：（A）向反应器中加入微生物或含有腈水合酶的微生物的加工产物; （B）向反应器中加入碱; 和（C）在步骤（A）中使用的添加线，步骤（B）中使用的加成线和步骤（C）中使用的加成线的反应器（甲基）丙烯腈中加入 和（甲基）丙烯腈通过微生物或产生腈水合酶的微生物的加工产物（其中加入（甲基）丙烯腈和水的混合物）的加工产物的作用制备（甲基）丙烯酰胺的另一种方法， 放入反应器中并含有通过反应器的加料管产生腈水合酶的微生物或微生物的微生物或加工产物的水溶液。

    PROCESS FOR PRODUCING AMIDE COMPOUND
    8.
    发明公开
    PROCESS FOR PRODUCING AMIDE COMPOUND 有权
    VERFAHREN ZUR HERSTELLUNG EINER AMIDVERBINDUNG

    公开(公告)号：EP1944376A1

    公开(公告)日：2008-07-16

    申请号：EP06811414.9

    申请日：2006-10-06

    申请人： Mitsui Chemicals, Inc.

    发明人： SHIBAMOTO, Hiroko ,  AIKAWA, Toshikazu ,  ARII, Teruo ,  MURAMOTO, Masanori ,  FUKUDA, Takeshi ,  ITO, Kiyoshi ,  ABE, Takeya ,  HAZAMA, Souichi

    IPC分类号： C12P13/02 ,  C07C233/09 ,  C08F20/56

    CPC分类号： C12P13/00 ,  C07C231/06 ,  C08F220/56 ,  C12P13/02 ,  C07C233/09

    摘要： [PROBLEMS]
    The present invention provides a method for efficiently producing a corresponding amide compound from a nitrile compound by a reaction using a nitrile hydratase and a method for producing an amide-based polymer excellent in quality from the amide compound. In addition, the present invention provides a method for more efficiently producing an acrylamide with higher quality by a microbial catalyst containing a nitrile hydratase and the like and a method for producing an acrylamide-based polymer, which is excellent in hue, has a good balance between the water solubility and the high molecular weight and is also excellent in quality, by using the acrylamide.
    [MEANS FOR SOLVING THE PROBLEMS]
    The method for producing an amide compound of the present invention is characterized in that in a method for producing an amide compound from a nitrile compound in an aqueous medium in the presence of a catalyst having a nitrile hydratase activity, the concentration of benzene in the aqueous medium is 4.0 ppm or less. In addition, the method for producing an amide-based polymer of the present invention is characterized by homopolymerizing the amide compound or by copolymerizing the amide compound and at least unsaturated monomer copolymerizable with the amide compound. Further, the method for producing acrylamide of the present invention is characterized by hydrating acrylonitrile having a concentration of acrolein of 1 ppm or less by a microbial cell containing a nitrile hydratase or a processed product of the microbial cell in an aqueous medium. Furthermore, the method for producing an acrylamide-based polymer of the present invention is characterized by homopolymerizing the acrylamide or by copolymerizing the acrylamide and at least one unsaturated monomer copolymerizable with the acrylamide.

    摘要翻译： 本发明提供一种通过使用腈水解酶的反应从腈化合物有效地制备相应的酰胺化合物的方法和由酰胺化合物制备质量优异的酰胺类聚合物的方法。 此外，本发明提供了通过含有腈水合酶等的微生物催化剂更高效地制备丙烯酰胺的方法和色调优异的丙烯酰胺系聚合物的制造方法，具有良好的平衡性 在水溶性和高分子量之间，并且通过使用丙烯酰胺也具有优异的质量。 解决问题的手段本发明的酰胺化合物的制造方法的特征在于，在具有腈水合酶活性的催化剂存在下，在水性介质中由腈化合物制备酰胺化合物的方法， 水介质中苯的浓度为4.0ppm以下。 此外，本发明的酰胺系聚合物的制造方法的特征在于，使酰胺化合物均聚，或者使酰胺化合物与能与酰胺化合物共聚的至少不饱和单体共聚。 此外，本发明的丙烯酰胺的制造方法的特征在于，通过含有腈水合酶的微生物细胞或微生物细胞的加工产物在水性介质中将丙烯醛浓度为1ppm以下的丙烯腈水合。 此外，本发明的丙烯酰胺系聚合物的制造方法的特征在于，使丙烯酰胺均聚，或者使丙烯酰胺与可与丙烯酰胺共聚的至少一种不饱和单体共聚。