摘要:
A method of producing methyl methacrylate comprising the following steps: Thermal decomposition step: a hydrocarbon having 3 or more carbon atoms is thermally decomposed to obtain a decomposed gas having a total content of propyne and propadiene of 2 wt% or more, Separation step: mixed liquid rich in propyne and propadiene is separated from the decomposed gas obtained in the thermal decomposition step, Propyne purification step: the mixed liquid rich in propyne and propadiene obtained in the separation step is subjected to extractive distillation, for separation into purified propyne, and crude propadiene containing propadiene as the main component, Isomerization step: the crude propadiene obtained in the propyne purification step is isomerized in the presence of an isomerization catalyst, to obtain crude propyne containing propyne as the main component, and Carbonylation step: the purified propyne obtained in the propyne purification step is reacted with carbon monoxide and methanol in the presence of a group VIII metal catalyst system, to produce methyl methacrylate.
摘要:
In a method for producing chlorine comprising oxidizing hydrogen chloride present in a gas containing the hydrogen chloride using a gas containing oxygen in the presence of a catalyst, an improvement which comprises conducting the oxidation of the hydrogen chloride in a reaction region comprising at least two catalyst-packed layers connected in series and carrying out the temperature control of at least one reaction region using a heat exchange system is disclosed. This method enables the inhibition of formation of excess hot spots and effective utilization of the catalyst-packed layers, which results in maintaining stable activity of the catalyst and in the production of chlorine in high yield with good stability.
摘要:
In a chemical reaction device (100) that improves an yield of a product and that causes a reaction, progress of which in a gaseous phase is restricted by a chemical equilibrium between a source material and the product, a cumulative value is not less than 500 mm 2 , the cumulative value being obtained by cumulatively adding, from one end to the other end of a cooling surface (53) in a height direction, products of (i) a distance L between (a) a surface of a catalyst layer (3) which surface is in contact with a transmission wall (40) and (b) an outer surface of the cooling surface (53) and (ii) a height H of the catalyst layer (3) corresponding to the outer surface having the distance L.
摘要:
A dehydration method for removing water from a hydrolysis reaction mixture containing unreacted water generated when monochlorobenzene is hydrolyzed to produce phenol, the method for dehydrating the hydrolysis reaction mixture comprising the steps of supplying a hydrolysis reaction mixture to a distillation tower, supplying a liquid containing monochlorobenzene to the tower top portion of the distillation tower, and removing the substantially whole amount of the water in the hydrolysis reaction mixture together with monochlorobenzene from the tower top portion by distillation.
摘要:
A process for producing chlorine comprising the step of oxidizing hydrogen chloride in a gas containing hydrogen chloride with a gas containing oxygen in the presence of a catalyst, wherein the oxidation of hydrogen chloride is carried out in at least two reaction zones each comprising a catalyst-packed layer, which are arranged in series, and a temperature in at least one of said reaction zones is controlled with a heat exchange system. According to this process, the stable activity of the catalyst is maintained and chlorine can be stably obtained at a high yield since the excessive hot spot in the catalyst-packed layer is suppressed and the catalyst-packed layer can be effectively used.
摘要:
In a chemical reaction device (100) that improves an yield of a product and that causes a reaction, progress of which in a gaseous phase is restricted by a chemical equilibrium between a source material and the product, a cumulative value is not less than 500 mm 2 , the cumulative value being obtained by cumulatively adding, from one end to the other end of a cooling surface (53) in a height direction, products of (i) a distance L between (a) a surface of a catalyst layer (3) which surface is in contact with a transmission wall (40) and (b) an outer surface of the cooling surface (53) and (ii) a height H of the catalyst layer (3) corresponding to the outer surface having the distance L.
摘要:
In a chemical reaction device (100) that improves an yield of a product and that causes a reaction, progress of which in a gaseous phase is restricted by a chemical equilibrium between a source material and the product, a cumulative value is not less than 500 mm 2 , the cumulative value being obtained by cumulatively adding, from one end to the other end of a cooling surface (53) in a height direction, products of (i) a distance L between (a) a surface of a catalyst layer (3) which surface is in contact with a transmission wall (40) and (b) an outer surface of the cooling surface (53) and (ii) a height H of the catalyst layer (3) corresponding to the outer surface having the distance L.
摘要:
The present specification discloses a method of producing a concentrated carbonate aqueous solution. The present invention relates to a method for producing a concentrated carbonate aqueous solution, comprising a step of dewatering a hydrogen carbonate aqueous solution by means of a salt blocking membrane to prepare a concentrated hydrogen carbonate aqueous solution, wherein the concentrated hydrogen carbonate aqueous solution obtained in the above step is heated to thermally decompose the hydrogen carbonate into carbonate, carbon dioxide and water, and to evaporate water to obtain a concentrate of the carbonate aqueous solution.