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1.发明公开METHOD FOR PREPARING CATALYST USED FOR PREPARING CHLORINE, CATALYST AND METHOD FOR PREPARING CHLORINE 审中-公开制造用于氯，催化剂及加工生产用催化剂的生产氯
公开(公告)号：EP3097976A1
公开(公告)日：2016-11-30
申请号：EP14879293.0
申请日：2014-01-27
发明人： LOU, Yinchuan , LV, Yang , YI, Guangquan , SHAO, Liangfeng , ZHANG, Hongke , HUA, Weiqi , DING, Jiansheng
CPC分类号： B01J23/8993 , B01J21/02 , B01J21/12 , B01J23/002 , B01J23/868 , B01J23/8892 , B01J35/002 , B01J35/023 , B01J37/0009 , B01J37/0045 , B01J37/0072 , B01J37/0236 , B01J37/04 , B01J37/08 , B01J37/088 , B01J2523/00 , C01B7/04 , B01J2523/13 , B01J2523/17 , B01J2523/305 , B01J2523/31 , B01J2523/3706 , B01J2523/3712 , B01J2523/41 , B01J2523/67 , B01J2523/72 , B01J2523/821 , B01J2523/23
摘要： The present invention relates to a method for preparing catalyst used for preparing chlorine by oxidizing hydrogen chloride. The method is mixing a slurry mainly containing boron and chromium with a slurry mainly containing copper, boron, alkali-metal elements, rare-earth elements, aluminum sol, silica sol, carrier and optionally other metal elements, the mixing temperature being not more than 100°C, and the residence time being not more than 120 minutes, the mixed slurry is successively treated with spray drying, high temperature calcination, so that the catalyst is obtained. The present invention also relates to the catalyst prepared through the method, use of the catalyst used in the process of preparing chlorine by oxidizing hydrogen chloride and a method for preparing chlorine by using the catalyst. The catalyst is used for preparing chlorine by oxidizing hydrogen chloride with oxygen or air in fluidized bed reactor, and has an excellent activity and anti-caking property, a relatively good mechanical strength and a relatively long service life.
摘要翻译： 本发明涉及用于制备用于通过氧化氯化氢制备氯气的催化剂的方法。 该方法是混合主要含有硼和铬与主要含有铜，硼，碱金属元素，稀土类元素，铝溶胶，二氧化硅溶胶，载体和任选的其它金属元素，混合温度为不超过浆料的浆料 100℃，并且停留时间不大于120分钟的混合浆料依次用喷雾干燥，高温煅烧处理，所以没有催化剂被得到。 因此，本发明涉及通过所述方法制备的催化剂，使用在通过氧化氯化氢以及用于通过使用该催化剂制备氯的方法制备氯的方法中使用的催化剂。 所述催化剂是用于通过在流化床反应器中的氧气或空气氧化氯化氢制备氯气的，并且具有优异的活性和抗结块性，相对良好的机械强度和相对长的使用寿命。
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2.发明公开
公开(公告)号：EP3040359A1
公开(公告)日：2016-07-06
申请号：EP13892354.5
申请日：2013-09-09
发明人： ZHANG, Lei , GAO, Zhikun , XIONG, Zhansen , ZHANG, Hongke , TIAN, Qin , HUA, Weiqi
IPC分类号： C08G64/14
摘要： The present invention relates to a method for preparing branched polycarbonate with a continuous two-phase interface phosgene method. Firstly, an aqueous solution of alkali metal hydroxide with triphenol and polyphenol dissolved therein reacts with a certain amount of phosgene in the present of inert organic solvent to prepare a prepolymer, and then a coupling reaction is performed among the prepolymer, an aqueous solution of alkali metal hydroxide with bisphenol and phosgene dissolved therein to finally obtain a polycarbonate resin. The method can avoid a cross-linking reaction, reduce the cost and improve the quality of the product, while improving the conversion ratio of the branching agent and the branching degree of the product.
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3.发明公开METHOD FOR PREPARING DIAMINO-DICYCLOHEXYL METHANE 有权VERFAHREN ZUR HERSTELLUNG VON DIAMINO-DICYCLOHEXYL-METHAN
公开(公告)号：EP3000803A1
公开(公告)日：2016-03-30
申请号：EP13885426.0
申请日：2013-11-22
发明人： LI, Xin , CHEN, Hao , ZHANG, Congying , GAO, Shan , LIU, Zhenguo , WANG, Weijia , TANG, Lei , LIU, Zhipeng , LI, Yuan , JIANG, Qingmei , SONG, Jinhong , HUA, Weiqi , DING, Hao
IPC分类号： C07C211/36 , C07C209/72
摘要： Disclosed is a method for preparing diamino-dicyclohexyl methane (H 12 MDA) by hydrogenation of diamino-diphenyl methane (MDA). In the process, 4,4'-MDA used as the starting material is firstly hydrogenated to prepare 4,4'-H 12 MDA. When the activity of the catalyst is reduced, the feed is switched from 4,4'-MDA to the mixture of 2,4'-MDA and 4,4'-MDA, and then when the conversion is stabilized, the feed is switched to 4,4'-MDA again. The deactivated catalyst is activated on line by switching the feed to the mixture of 2,4'-MDA and 4,4'-MDA. 4,4'-H 12 MDA having the trans-trans isomer content of 16~24wt% is produced, and the mixture of 2,4'-H 12 MDA and 4,4'-H 12 MDA is also produced, wherein the content of 2,4'-H 12 MDA in the mixture is 4~15 wt%.
摘要翻译： 公开了通过二氨基二苯基甲烷（MDA）的氢化制备二氨基二环己基甲烷（H 12 MDA）的方法。 在此过程中，首先氢化作为原料的4,4'-MDA，制备4,4'-H 12 MDA。 当催化剂的活性降低时，将进料从4,4'-MDA转化为2,4'-MDA和4,4'-MDA的混合物，然后当转化稳定时，进料被切换 至4,4'-MDA。 通过将进料转化为2,4'-MDA和4,4'-MDA的混合物，使活化的催化剂在线活化。 产生具有16〜24重量％的反式异构体含量的4,4'-H 12 MDA，并且还生产2,4'-H 12 MDA和4,4'-H 12 MDA的混合物，其中 混合物中2,4'-H 12 MDA的含量为4〜15重量％。
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公开(公告)号：EP4006076A1
公开(公告)日：2022-06-01
申请号：EP20847915.4
申请日：2020-07-20
发明人： LI, Jianfeng , SHANG, Yonghua , WU, Qian , ZHU, Fulin , WANG, Peng , CHEN, Hao , SHI, Peimeng , HUA, Weiqi , LI, Yuan
摘要： Provided are a preparation method for a polyurethane optical resin and applications thereof. The preparation method for the polyurethane optical resin comprises: a raw material composition comprising isocyanate and a polythiol compound undergoes a polymerization to produce the polyurethane optical resin. The turbidity value of the isocyanate used in the raw material composition is controlled at ≤ 2 NTU. The polyurethane optical resin produced is applicable in manufacturing optical products.
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5.发明授权
公开(公告)号：EP2736842B1
公开(公告)日：2017-11-29
申请号：EP12750308.4
申请日：2012-05-26
发明人： DING, Jiansheng , LUO, Wuxi , CHEN, Bin , ZHANG, Kunpeng , HUA, Weiqi
CPC分类号： C01B7/04 , C01B7/0706 , C01B7/0737 , Y02P20/228
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6.发明公开CATALYST FOR PREPARING PHOSGENE AND METHOD FOR PREPARING PHOSGENE USING THE SAME 有权制造用催化剂光气和工艺是这样就产生光气
公开(公告)号：EP3038745A1
公开(公告)日：2016-07-06
申请号：EP14841157.2
申请日：2014-02-11
发明人： CHEN, Bin , LUO, Wuxi , YAO, Yu , SHAO, Liangfeng , WANG, Lei , ZHANG, Hongke , HUA, Weiqi
IPC分类号： B01J23/04 , B01J21/18 , B01J27/224 , B01J35/00
CPC分类号： C01B31/28 , B01J21/18 , B01J23/04 , B01J27/10 , B01J27/224 , B01J31/06 , B01J35/0006 , B01J35/023 , B01J35/04 , B01J37/0219 , B01J37/0236 , B01J37/08 , B01J37/084 , B01J37/24 , C01B32/80
摘要： The present invention relates to a catalyst for preparing phosgene and a method for preparing phosgene using the catalyst. Said method comprises: modifying the surface of an activated carbon coating/foamed silicon carbide structural catalyst using an alkali metal salt; filling the catalysts having different thickness of the activated carbon coating and different amount of the alkali metal salt in different sections in the axial direction of the multi-tubular reactor of the fixed bed, and preparing phosgene using Cl2 and CO. The radial and axial temperature difference of the catalyst bed is lowered by using the alkali metal salt-modified activated carbon coating/foamed silicon carbide structural catalyst and by segmental filling, so that high temperature of tube wall is obtained in the case of a larger tube diameter, and high quality of steam is obtained stably.
摘要翻译： 本发明涉及一种用于制备光气和使用该催化剂制备光气的方法的催化剂。 所述方法包括：使用修改的碱金属盐的活性炭涂层/泡沫碳化硅结构催化剂的表面上; 填充具有使用Cl 2和CO的活性碳涂层的不同厚度和不同量在固定床多管式反应器的轴线方向不同的部分的碱金属盐，和光气制备的催化剂。 催化剂床的径向和轴向温差是通过使用碱金属盐改性的活性炭涂层/泡沫碳化硅结构催化剂和节段性填充降低，所以没有管壁的高温在一个较大的管的情况下，获得 直径，和水蒸汽的高品质被稳定地获得。
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公开(公告)号：EP3904336A1
公开(公告)日：2021-11-03
申请号：EP18944569.5
申请日：2018-12-26
发明人： HUA, Weiqi , LI, Tonghe , SHANG, Yonghua , SUN, Shuchang , WANG, Jingxu , HAN, Jinping , LI, Qiang , LI, Wenbin , LI, Jing , WANG, Pengfei , LI, Yuan
IPC分类号： C07C263/10 , C07C265/00
摘要： Disclosed is a method for preparing an isocyanate in a gaseous phase, comprising feeding, in the presence or absence of an inert gas, an amine-containing gas stream and a phosgene-containing gas stream into a reaction region, allowing the amine and the phosgene to contact in gaseous forms and undergo a phosgenation reaction in the reaction region, thus preparing the target isocyanate in a gaseous form in the reaction region. The phosgene-containing stream is subjected to preheating and warming before being fed into the reaction region, and the phosgene-containing stream comprises a substance A at a mass fraction of
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公开(公告)号：EP3904482A1
公开(公告)日：2021-11-03
申请号：EP18945060.4
申请日：2018-12-27
发明人： JU, Changxun , LIU, Bin , WANG, Mingyong , YE, Tian , SHI, Zhengyang , LI, Yuan , HUA, Weiqi
IPC分类号： C09J171/02 , C08G65/336 , C08G65/28
摘要： Disclosed by the present invention is a method for preparing a reactive sealant resin, the method comprising: (1) under the action of an alkali catalyst, polymerizing a hydroxyl-containing initiator with an epoxy compound to obtain a polyether polyol; (2) adding an alkoxide reagent and a halogenated end-capping agent containing a double bond to the polyether polyol obtained in step (1) for reaction, so as to obtain a crude double-bonded polyether product, and refining the crude product to obtain a modified polyether product; and (3) subjecting the modified polyether and hydrogen-containing silane to silane end-capping reaction under the action of a hydrosilylation catalyst, so as to obtain the target product, i.e., a reactive sealant resin. The resin has excellent properties as well as good adhesion and paintability.
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9.发明公开COMPOSITE CATALYST, PREPARATION PROCESS THEREOF, AND PROCESS FOR CATALYZING THE TRIMERIZATION OF BUTADIENE USING THE COMPOSITE CATALYST 审中-公开复合催化剂，用于生产IT，AND METHOD FOR催化丁二烯三聚与复合催化剂
公开(公告)号：EP2890494A1
公开(公告)日：2015-07-08
申请号：EP13832707.7
申请日：2013-05-09
发明人： QIN, Lei , HUA, Weiqi , CHENG, Ruihua , LI, Yuan , LIU, Baiping , HU, Bingbo
IPC分类号： B01J31/38 , C07C13/277 , C07C2/46
CPC分类号： B01J31/0215 , B01J31/0209 , B01J31/0212 , B01J31/0232 , B01J31/122 , B01J31/128 , B01J31/143 , B01J31/146 , B01J31/2226 , B01J31/38 , B01J2231/20 , C07C2/465 , C07C2531/02 , C07C2531/14 , C07C2531/38 , C07C13/277
摘要： The present invention relates to a composite catalyst, preparation process thereof, and process for catalyzing the trimerization of butadiene using the composite catalyst. The composite catalyst comprises: (A) a titanium compound catalyst active component, (B) an organometallic compound co-catalyst component, (C) a sulfoxide compound catalyst-modifying component, (D) a monoester compound catalyst-modifying component, and (E) a solvent component. The composite catalyst has advantages of excellent selectivity, high catalytic activity, easy preparation and so on.
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10.发明公开3-AMINOMETHYL-3, 5, 5-TRIMETHYL CYCLOHEXYLAMINE PREPARATION METHOD 有权HERSTELLUNGSVERFAHRENFÜR3-氨基乙基-3,5,5-三甲基环己基胺
公开(公告)号：EP2743251A1
公开(公告)日：2014-06-18
申请号：EP11870592.0
申请日：2011-09-06
发明人： CHEN, Changsheng , LI, Yuan , ZHAO, Wenjuan , CUI, Hongyin , HUA, Weiqi
IPC分类号： C07C211/36 , C07C209/48
CPC分类号： C07C209/62 , C07C209/48 , C07C209/52 , C07C211/36 , C07C253/30 , C07C2601/14 , C07C255/61 , C07C255/46
摘要： Provided is a 3-aminomethyl-3,5,5-trimethylcyclohexylamine preparation method. A feeding flow of 3-cyano-3,5,5-trimethylcyclohexylimine is reacted with NH 3 and hydrogen in the presence of a hydrogenation catalyst; the method is characterized by: firstly adding a basic compound to the feeding flow of 3-cyano-3,5,5-trimethylcyclohexylimine, and then after a portion of 3-cyano-3,5,5-trimethylcyclohexylimine has reacted, adding an acidic compound to reaction materials for further hydrogenation reaction to prepare the product. The method ensures that the aminonitrile content in the product is low, thus effectively reducing the duration of the reaction and greatly reducing the consumption of the catalyst during the hydrogenation reaction process.
摘要翻译： 提供3-氨基甲基-3,5,5-三甲基环己胺制备方法。 在氢化催化剂存在下，将3-氰基-3,5,5-三甲基环己基亚胺的进料流与NH 3和氢气反应; 该方法的特征在于：首先向3-氰基-3,5,5-三甲基环己基亚胺的进料流中加入碱性化合物，然后在一部分3-氰基-3,5,5-三甲基环己基亚胺反应后，加入 酸性化合物与反应物进行进一步氢化反应制备产物。 该方法确保了产物中氨腈含量低，有效地降低了反应持续时间，大大降低了氢化反应过程中催化剂的消耗。
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