VERFAHREN ZUM HERSTELLEN EINES HOLZFASERSTOFFS UND HOLZFASERSTOFF-HERSTELLVORRICHTUNG

    公开(公告)号:EP4435175A1

    公开(公告)日:2024-09-25

    申请号:EP23163742.2

    申请日:2023-03-23

    摘要: Die Erfindung betrifft ein Verfahren zum Herstellen eines Holzfaserstoffs, mit den Schritten Erwärmen von Holzhackschnitzeln (18) in einem Vorkocher (16) mittels Wasser oder Dampf (26), danach Kochen der Holzhackschnitzel (18) mittels Dampf (26) in einem Kocher (14), danach Zerfasern der Holzhackschnitzel (18) in einem Refiner (32), sodass Fasermaterial (34) entsteht, wobei ein Teil des Dampfes nach dem Zerfasern abgezweigt und zum Erwärmen der Holzhackschnitzel (18) im Vorkocher (16) verwendet wird, mit dem Schritt Einbringen eines Oxidationsmittels (56) in den abgezweigten Dampf (26), sodass im Dampf (26) enthaltene volatile organische Substanzen oxidiert werden und gereinigter Dampf (68) entsteht, wobei der gereinigte Dampf (68) zumindest teilweise zum Erwärmen der Holzhackschnitzel (18) verwendet wird.

    PROCESS FOR THE PRODUCTION OF A NANOCELLULOSE MATERIAL

    公开(公告)号:EP3409691A1

    公开(公告)日:2018-12-05

    申请号:EP17173805.7

    申请日:2017-05-31

    摘要: A process for the production of a non-derivatized nanocellulose material from a cellulosic fibrous material, comprising the steps of providing a suspension of cellulosic fibrous material in a continuous phase of a non-aqueous process liquid comprising a swelling agent and a processing solvent; allowing the cellulosic fibrous material to swell such as to form a suspension of swollen cellulosic fibrous material in a continuous phase of non-aqueous process liquid; optionally refining said suspension of swollen cellulosic fibrous material in a continuous phase of non-aqueous process liquid to increase the fineness of the swollen cellulosic fibrous material; removing the swelling agent from the rocess liquid such as to form a suspension of cellulosic fibrous material in a continuous phase of processing solvent; subjecting the swollen and optionally refined cellulosic fibrous material to high-shear comminution such as to release of the non-derivatized nanocellulose material from the swollen and optionally refined cellulosic fibrous material and such as to form a dispersion of non-derivatized nanocellulose material in a continuous phase of a processing solvent; contacting the dispersion of non-derivatized nanocellulose material in a continuous phase of a processing solvent with a supercritical fluid such as to remove the processing solvent and isolate the non-derivatized nanocellulose material, wherein the supercritical fluid is preferably supercritical carbon dioxide or ammonia; characterized in that the swelling agent is a low-transition-temperature mixture (LTTM) and in particular a deep eutectic solvent and said low-transition-temperature mixture and in particular said deep eutectic solvent is soluble in the processing solvent and wherein the processing solvent is non-solubilizing for the cellulosic fibrous material and the non-derivatized nanocellulose material.

    HIGH EFFICIENCY PRODUCTION OF NANOFIBRILLATED CELLULOSE

    公开(公告)号:EP3140454A4

    公开(公告)日:2018-03-21

    申请号:EP15789871

    申请日:2015-05-06

    IPC分类号: D21D1/30 D21C9/00 D21H11/18

    摘要: A scalable, energy efficient process for preparing cellulose nanofibers is disclosed. The process employs treating the cellulosic material with a first mechanical refiner with plates having a configuration of blades separated by grooves, and subsequently treating the material with a second mechanical refiner with plates having a configuration of blades separated by grooves different than the first refiner. The plate configurations and treatment operations are selected such that the first refiner produces a first SEL that is greater than the SEL of the second refiner, by as much as 2-50 fold. An exemplary high first SEL may be in the range of 1.5 to 8 J/m. Paper products made with about 2% to about 30% cellulose nanofibers having a length from about 0.2 mm to about 0.5 mm, preferably from 0.2 mm to about 0.4 mm have improved properties.