LAYERED PLATINATE, LAYERED PLATINIC ACID, PLATINIC ACID NANOSHEET, PLATINUM NANOSHEET AND PRODUCTION METHOD THEREOF

    公开(公告)号:EP4455095A1

    公开(公告)日:2024-10-30

    申请号:EP22910512.7

    申请日:2022-10-03

    IPC分类号: C01G55/00 B82Y30/00 B82Y40/00

    摘要: To provide a layered platinate, a layered platinic acid, a platinic acid nanosheet, a platinum nanosheet, and a manufacturing method of the platinum nanosheet that are used for fabricating a platinum nanosheet usable as an electrocatalyst for fuel cells, a catalyst for purifying exhaust gas, a catalyst for synthesizing chemical products, and the like.
    The above-described problem is solved by a layered platinate comprising M x Pt y O z ·nH 2 O (where M is a monovalent metal), the M x Pt y O z ·nH 2 O being layered (the M being potassium and diffraction peaks are at 2Θ diffraction angles of 13° and 26°); a layered platinic acid comprising H x Pt y O z ·nH 2 O, the H x Pt y O z ·nH 2 O being layered; a platinic acid nanosheet having a thickness of 1 nm or less; and a platinum nanosheet having a thickness of 0.6 nm or less.

    HYDROTHERMAL SYNTHESIS METHOD FOR NANO LITHIUM MANGANESE IRON PHOSPHATE

    公开(公告)号:EP4393875A1

    公开(公告)日:2024-07-03

    申请号:EP22937121.6

    申请日:2022-08-05

    发明人: TIAN, Yihong

    CPC分类号: Y02E60/10

    摘要: The present invention relates to the technical field of preparation of lithium battery raw materials, especially to a hydrothermal synthesis method for nano lithium iron manganese phosphate, including the following steps: mixing lithium phosphate with water, adding them to autoclave 1, heating from room temperature to 140-150°C while stirring to obtain slurry A; dissolving ferrous sulfate and manganese sulfate in water, adding them to autoclave 2, and heating to 140-150°C to obtain slurry B; heating autoclave 3 to 140-150°C, adding slurry A and slurry B in concurrent flow to autoclave 3, stirring, maintaining reaction at 140-150°C for 2-4 hours; stopping heating, cooling, opening a discharge valve, filtering product, washing filter cake, drying in vacuum to obtain lithium iron manganese phosphate powder, and coating with carbon. High-temperature mixing of reaction raw materials creates a true molecular mixing reaction starting condition. Prepared material particles are uniform with a three-dimensional scale reaching a nano scale, which is conducive to shortening lithium ion diffusion paths, fundamentally improving electrochemical performance of the material and prolonging its cycle life.