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公开(公告)号：JPH1087983A
公开(公告)日：1998-04-07
申请号：JP28282696
申请日：1996-09-18
发明人： MIYAMOTO ATSUSHI , IMAMURA HIDEAKI
IPC分类号： A61K8/49 , A61K8/39 , A61K8/86 , A61Q5/00 , C07C41/46 , C07C43/11 , C08L71/00 , C08L71/02 , A61K7/00
摘要： PROBLEM TO BE SOLVED: To obtain the subject addition product having improved quality, preventing the generation of foul smell with time, and suitable for cosmetics, etc., by adding a compound having antioxidation action to the addition product of a polyhydric alcohol and an alkylene oxide. SOLUTION: The quality of an addition product of a polyhydric alcohol and an alkylene oxide is improved by adding preferably 0.01-0.1wt.% of one or more kinds of compounds having antioxidation action such as dibutylhydroxytoluene to an addition product of a polyhydric alcohol and an alkylene oxide.
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公开(公告)号：JPH07118515A
公开(公告)日：1995-05-09
申请号：JP34224393
申请日：1993-12-15
申请人： BAYER AG
IPC分类号： C07C41/46 , C08G18/08 , C08G18/28 , C08G18/40 , C08G65/32 , C08G65/333 , C08K5/54 , C08K5/5419 , C08L71/02
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公开(公告)号：JPH0253422B2
公开(公告)日：1990-11-16
申请号：JP5820085
申请日：1985-03-25
发明人： OZAKI HITOSHI , HAYASHI JUSON , KAKEHI KOJI , YOKOYAMA HIROMI
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公开(公告)号：JPH0253419B2
公开(公告)日：1990-11-16
申请号：JP3534985
申请日：1985-02-26
发明人： OZAKI HITOSHI , HAYASHI JUSON , KAKEHI KOJI , YOKOYAMA HIROMI
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公开(公告)号：JPH01265049A
公开(公告)日：1989-10-23
申请号：JP9169488
申请日：1988-04-15
发明人： KOKAI HIROYUKI , HONDA YOSHIHIKO , KOBAYASHI KAZUO
IPC分类号： C07C235/16 , C07C41/00 , C07C41/46 , C07C43/12 , C07C67/00 , C07C231/00 , C08K5/52 , C08L71/02 , C10M169/04 , C10N30/08
摘要： PURPOSE:To obtain the title composition useful as lubricant, etc., having excellent heat stability even in the presence of metal, by simultaneously blending a perfluoropolyether and a phosphite compound. CONSTITUTION:A perfluoropolyether shown by formula I (Rf is perfluoromethyl or perfluoroethyl; CF2CF2O and CF2O are randomly bonded; m+n are 3-200; m:n=10:90-90:10) is blended with a perfluoropolyether containing a terminal arylamide group, a reaction product of a diacid fluoride of a perfluoropolyether shown by formula II and an N,N'-diarylphenylenediamine and a compound shown by formula III (R' is alkyl or alkylaryl). The blending ratio is about 2.5-3wt.% of the two components based on the compound shown by formula I and the weight ratio of both components is preferably 1:1.
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公开(公告)号：JPS6413043A
公开(公告)日：1989-01-17
申请号：JP16794087
申请日：1987-07-07
IPC分类号： C07C17/386 , C07B63/00 , C07B63/04 , C07C17/00 , C07C17/38 , C07C17/383 , C07C17/42 , C07C22/04 , C07C22/08 , C07C25/02 , C07C41/00 , C07C41/42 , C07C41/46 , C07C43/225 , C07C67/00
摘要： PURPOSE:To obtain the titled compound in purified state, by using an easily available hexamethylenetetramine as a decomposition suppressing agent, adding a small amount of the amine to neophyl halides prior to distillation and distilling the halides. CONSTITUTION:Neophyl halides of formula I (R1 and R2 are H, halogen, lower alkyl or lower alkoxy; X is halogen) (e.g. 2-methyl-2-(3chloro-4-ethoxyphenyl) propyl chloride) are added with 50-5,000ppm, preferably 100-1,000ppm by weight of hexamethylenetetramine (= urotropin) based on the above compound and distilled by continuous or batch distillation under reduced pressure at 150-230 deg.C to obtain purified neophyl halides of formula I useful as a production raw material for 3phenoxybenzyl 2-phenyl-2-methylpropyl ethers of formula II having high insecticidal and miticidal activities and low toxicity to fishes.
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公开(公告)号：JPS63218633A
公开(公告)日：1988-09-12
申请号：JP5347587
申请日：1987-03-09
发明人： TAKEMOTO KIICHI , MIYATA KANJI , SENDA SHUJI , KOMATA TETSUO
IPC分类号： C07J9/00 , C07B63/02 , C07C17/00 , C07C17/38 , C07C17/395 , C07C19/01 , C07C19/07 , C07C27/00 , C07C29/88 , C07C31/04 , C07C31/08 , C07C31/12 , C07C41/00 , C07C41/46 , C07C43/20 , C07C45/00 , C07C45/78 , C07C45/79 , C07C47/54 , C07C49/78 , C07C51/00 , C07C51/487 , C07C53/02 , C07C53/08 , C07C67/00 , C07C67/48 , C07C201/00 , C07C201/16 , C07C209/00 , C07C209/90 , C07C253/00 , C07C255/03 , C07C255/45 , C07C255/50
摘要： PURPOSE:To enable isolation of an organic compound of high purity in high efficiency, by clathrating the organic compound with a cholic acid or its derivative without complicated and expensive operations, e.g., rectification or column chromatography. CONSTITUTION:An organic compound selected from formulas: R -Y, R -O-R , R -COOH, R -COOR , R -CO-R , R R R N, R -Z or compendious of formulas I and II [R -R are alkyls (R and R -R have 1-5 carbon atoms and R may be substituted with halogens; R and R bear 1 carbon atom or 3 to 8 carbon atoms; R has 2-8 carbon atoms), cycloalkyl, aryl (R and R -R have 6-8 carbon atoms), further R -R , R , R are H; Y is OH, CN, NO2; Z is halogen; R , R are ethylene; X is O, C-C bond; R is 2-8C alkylene] is clathrated with cholic acid or its derivative and made hard soluble in an organic solvent such as acetone. Thus, the organic compound is easily and effectively purified.
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公开(公告)号：JPS61183241A
公开(公告)日：1986-08-15
申请号：JP2191685
申请日：1985-02-08
发明人： OZAKI HITOSHI , HAYASHI YUUSON , KAKEHI KOJI , YOKOYAMA HIROMI
摘要： PURPOSE:To obtain a stabilized odorless aliphatic primary alcohol ethoxylate with very little change in carbonyl value, acid value, pH, hue, etc., with time, by incorporating lactic acid and/or lactate therein. CONSTITUTION:Lactic acid or lactate, e.g. sodium lactate or potassium lactate, or both are incorporated in a 6-30C aliphatic primary alcohol ethoxylate to stabilize the quality thereof. The lactic acid may be prepared by either one of the fermentation and synthetic methods, and the amount to be added is 1-0.05pts. wt. based on 100 pts. wt. aliphatic primary alcohol ethoxylate. Preferably, the pH of the aqueous solution is adjusted to 5-7 range. USE:Surfactants.
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