Method of manufacturing bottomed cylindrical sintered body
    14.
    发明专利
    Method of manufacturing bottomed cylindrical sintered body 有权
    制造底部圆柱形烧结体的方法

    公开(公告)号:JP2011003548A

    公开(公告)日:2011-01-06

    申请号:JP2010182007

    申请日:2010-08-17

    Abstract: PROBLEM TO BE SOLVED: To provide a method capable of manufacturing a bottomed cylindrical sintered body having high formability, an outer circumference of about 3.0 mm or smaller, that is, a small diameter, and a thickness of about 0.1 to 0.3 mm at low cost.SOLUTION: The method sequentially includes: a raw material-preparing step of preparing a raw material by adding 40 to 60 vol.% of binder including thermoplastic resin and wax to metal powder and then heating and kneading it; a filling step of filling a die hole of a press-molding die with a predetermined amount of the raw material; a pressurizing/molding step of molding the raw material in the press-molding die into a shape of a cup by pressurizing the raw material in a vertical direction using a punch; an extracting step of extracting a cup-shaped compact obtained after the pressurizing/molding step; a de-binder step of removing the binder by heating the extracted cup-shaped compact; and a sintering step of diffusing and bonding the powder by heating the cup-shaped compact from which the binder is removed.

    Abstract translation: 要解决的问题:为了提供一种能够制造成型性高的有底圆柱形烧结体的方法,外径为约3.0mm或更小,即小直径,厚度为约0.1至0.3mm,低成本 该方法依次包括:原料准备步骤,通过向金属粉末中加入40〜60体积%的包含热塑性树脂和蜡的粘合剂,然后加热和捏合来制备原料; 填充步骤,用预定量的原料填充压模模具的模孔; 加压/成型步骤,通过使用冲头将原料在垂直方向上加压成型,将加压成型模具中的原料成型为杯状; 提取步骤,提取在加压/成型步骤后获得的杯状压块; 脱粘合剂步骤,通过加热提取的杯形压块来去除粘合剂; 以及烧结步骤,通过加热去除粘合剂的杯形压块来扩散和粘合粉末。

    Method for manufacturing noble metal fine particle
    18.
    发明专利
    Method for manufacturing noble metal fine particle 有权
    制造金属微粒的方法

    公开(公告)号:JP2009249722A

    公开(公告)日:2009-10-29

    申请号:JP2008102372

    申请日:2008-04-10

    Abstract: PROBLEM TO BE SOLVED: To provide a method for manufacturing noble metal fine particles, by which noble metal fine particles are obtained whose particle diameter and alloy composition are easy to control and whose crystallinity and purity are high.
    SOLUTION: The method for manufacturing noble metal fine particles includes the steps of: (1) obtaining a molten mixture containing a noble metal chloride, by insufflating chlorine gas into a mixture of a molten salt of an alkali metal chloride and a noble metal; (2) obtaining a noble metal oxide as a precipitate by adding an alkali metal carbonate to the molten mixture under an inert gas atmosphere; (3) obtaining a mixture containing noble metal oxide fine particles, by pulverizing the noble metal oxide with at least one of an alkali metal carbonate and an alkali earth metal carbonate; and (4) obtaining noble metal fine particles by heating the mixture obtained in the step (3), in an atmosphere of gas containing hydrogen, and then treating the heat-treated mixture with acid.
    COPYRIGHT: (C)2010,JPO&INPIT

    Abstract translation: 要解决的问题:提供一种贵金属微粒的制造方法,通过该方法可以获得其粒径和合金组成容易控制且结晶度和纯度高的贵金属微粒。 解决方案:贵金属微粒的制造方法包括以下步骤:(1)通过将氯气吹入碱金属氯化物的熔融盐和贵金属的混合物中,得到含有贵金属氯化物的熔融混合物 金属; (2)在惰性气体气氛下,向熔融混合物中加入碱金属碳酸盐,得到贵金属氧化物作为沉淀物; (3)通过用碱金属碳酸盐和碱土金属碳酸盐中的至少一种粉碎所述贵金属氧化物,得到含有贵金属氧化物微粒的混合物; 和(4)通过在含氢气体的气氛中加热步骤(3)中获得的混合物,然后用酸处理热处理的混合物来获得贵金属微粒。 版权所有(C)2010,JPO&INPIT

    Superhard material and tool
    19.
    发明专利
    Superhard material and tool 审中-公开
    超级材料和工具

    公开(公告)号:JP2009052071A

    公开(公告)日:2009-03-12

    申请号:JP2007218470

    申请日:2007-08-24

    Abstract: PROBLEM TO BE SOLVED: To solve such a conventional problem that, although cemented carbide is a high hardness and high toughness material and various trace elements including vanadium carbide (VC) are added to bring out its performances, the grain size of a raw material prepared by pulverizing a carbide become large when the vanadium carbide (VC) is used and, as a result, uniform improvement of properties in a product cannot be done.
    SOLUTION: One of component materials of a stock for a tool, such as a hob, is replaced from a carbide to vanadium trioxide (V
    2 O
    3 ) as an oxide. Since vanadium oxide is softer than vanadium carbide, vanadium oxide can be easily reduced in particle size in a mixing step using a ball mill in the course of raw material blending. The hardness of cemented carbide after sintering can hereby be increased by the effect of the vanadium trioxide uniformly dispersed in the raw material.
    COPYRIGHT: (C)2009,JPO&INPIT

    Abstract translation: 要解决的问题为了解决这样一个常规问题,尽管硬质合金是高硬度和高韧性的材料,并且添加了包括碳化钒(VC)在内的各种微量元素以提高其性能,但是其粒径 当使用碳化钒(VC)时,通过粉碎碳化物制备的原料变大,结果不能使产品的性能得到均匀的提高。

    解决方案:用于工具的坯料(例如炉刀)的组分材料之一被碳化物替换为三氧化二钒(V 2 SB 3 O 3 / SB 3),作为 氧化物。 由于氧化钒比碳化钒软,所以在原料混合的过程中,使用球磨机的混合工序中的氧化钒粒径容易降低。 因此,通过均匀分散在原料中的三氧化二钒的效果,可以提高烧结后的硬质合金的硬度。 版权所有(C)2009,JPO&INPIT

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