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    PREPARATION OF PHOSPHONITRILIC ESTER
    81.
    发明专利
    PREPARATION OF PHOSPHONITRILIC ESTER 失效

    公开(公告)号：JPS5843985A

    公开(公告)日：1983-03-14

    申请号：JP14216081

    申请日：1981-09-08

    申请人： OTSUKA KAGAKU YAKUHIN

    发明人： SUZUE MASAYOSHI ,  TADA YUUJI

    IPC分类号： C07F9/02 ,  C07F9/24

    摘要： PURPOSE:To obtain the tilted compound useful as a compound for providing a high polymer compound with flame retardancy, heat resistance, etc., by reacting a phosphonitrilic halide with an alcohol in the absence of a dehydrohalogenating agent, eliminating an evolved hydrogen halide. CONSTITUTION:A phosphonitrilic halide is reacted with a bifunctional or more functional alcohol (e.g., 2,2-dimethyl-1,3-propanediol, dipropylene glycol, etc.) at 70-180 deg.C, preferably at 85-135 deg.C for 5-30hr without using a dehydrohalogenating agent. In the operation, an evolved hydrogen halide is removed by bubbling an inert gas in the reaction solution or passing it on the reaction solution. The reaction product is then reacted with a metal alcoholate, ammonia, a primary amine or secondary amine, to give the desired substance with a low content of unsubstituted halogen atom.

    COMPOSITION OF STABILIZED HIGH POLYMER
    88.
    发明专利
    COMPOSITION OF STABILIZED HIGH POLYMER 失效

    公开(公告)号：JPS56115333A

    公开(公告)日：1981-09-10

    申请号：JP1880180

    申请日：1980-02-18

    申请人： KATSUTA KAKO KK

    发明人： NOGUCHI KATSUTOSHI

    IPC分类号： C08K5/00 ,  C07F9/02 ,  C07F9/09 ,  C07F9/6574 ,  C08K5/51 ,  C08K5/52 ,  C08L1/00 ,  C08L7/00 ,  C08L21/00 ,  C08L23/00 ,  C08L27/00 ,  C08L51/00 ,  C08L51/02 ,  C08L101/00

    摘要： PURPOSE:A composition, having improved resistance to weather and discoloration and reduced plateout phenomenon, and obtained by incorporating a metallic salt of a phosphorus compound, of specific structure with a high polymer. CONSTITUTION:(A) A high polymer, e.g. polyvinyl chloride, is incorporated with (B) preferably 0.001-5wt%, based on the component (A), phosphorus compound expressed by formula I [X1 is formula I or II; R1, R2, R3 and R4 are H, aryl alkylaryl, polyhydric phenol or alcohol residue or group containing epoxy or formulas III-VIII, etc., and at least one is H; Y1 is polyhydric alcohol or phenol residue; M1, M2, M3 and M4 are alkaline earth or zinc family metal; R5 is alkylene or arylene; R6 is H, (cyclo)alkyl, (alkyl)aryl, etc.; R7 and R8 are (cyclo)alkyl, (alkyl)aryl, alkenyl, etc.; R9, R10 and R12 are H, (aryl)alkyl, (alkyl)aryl, etc.; R11 is (alkyl) aryl, etc.; a is 1-10] to give the aimed composition.

    ETOPHYLLINEEMODIFIED PHOSPHAZENE POLYMER AND PREPARATION OF THE SAME
    90.
    发明专利
    ETOPHYLLINEEMODIFIED PHOSPHAZENE POLYMER AND PREPARATION OF THE SAME 失效

    公开(公告)号：JPS5630432A

    公开(公告)日：1981-03-27

    申请号：JP10540679

    申请日：1979-08-18

    申请人： OTSUKA KAGAKU YAKUHIN

    发明人： YOKOYAMA MASAAKI ,  OGATA YUZURU ,  NAKANAGA TAKEFUMI ,  SUZUE MASAYOSHI

    IPC分类号： C08G79/00 ,  C07F9/02 ,  C07F9/22 ,  C07F9/6561 ,  C08G79/02 ,  C08G79/04

    摘要： PURPOSE:To efficiently obtain titled polymer, useful as a medicine such as a diuretic etc., by the reaction of a specified phosphazene polymer, etophylline and a reactant of formula R-H (wherein R is 1-3C alkoxy etc.). CONSTITUTION:An etophylline-modified phosphazene polymer of formula III (wherein X is 0.1-1) is obtained by the reaction of a phosphazene polymer of formula I (wherein n is 3-10,000), etophylline of formula II and a reactant of formula R-H (wherein R is 1-3C alkoxy, propylamino or phenoxy) at once or in an arbitrary order. The reaction is carried out in an organic solvent such as benzene, xylene or ethylene glycol. Caustic soda, triethylamine, etc. is preferably used as a scavenger of hydrogen chloride. USE:A medicine such as a diuretic, cardiac or muscular relaxants.