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    METHOD FOR PRODUCING α-AMINOKETONE COMPOUND
    1.
    发明专利
    METHOD FOR PRODUCING α-AMINOKETONE COMPOUND 有权
    生产α-氨基酮类化合物的方法

    公开(公告)号：JP2010120886A

    公开(公告)日：2010-06-03

    申请号：JP2008296815

    申请日：2008-11-20

    申请人： Kao Corp ,  花王株式会社

    发明人： WATANABE MASAHIKO ,  TATENO GOSUKE ,  MIMURA YASUYUKI

    IPC分类号： C07C221/00 ,  C07B61/00 ,  C07C225/06

    摘要： PROBLEM TO BE SOLVED: To provide a method for producing an α-aminoketone compound highly selectively and efficiently in a high yield. SOLUTION: The method for producing an α-aminoketone compound comprises causing a trihydric or higher-hydric alcohol (B) to react with a secondary amine compound (C) in the presence of a catalyst (A) comprising at least one metal component selected from the group consisting of copper, nickel, ruthenium, aluminum and iron. COPYRIGHT: (C)2010,JPO&INPIT

    摘要翻译： 待解决的问题：提供高选择性和有效地以高产率生产α-氨基酮化合物的方法。 解决方案：α-氨基酮化合物的制备方法包括在含有至少一种金属（A）的催化剂（A）的存在下，使三羟基或更高级的醇（B）与仲胺化合物（C）反应， 选自铜，镍，钌，铝和铁的组分。 版权所有（C）2010，JPO＆INPIT

    Softening agent composition
    2.
    发明专利
    Softening agent composition 审中-公开
    软化剂组合物

    公开(公告)号：JP2006070408A

    公开(公告)日：2006-03-16

    申请号：JP2004257983

    申请日：2004-09-06

    申请人： Kao Corp ,  花王株式会社

    发明人： MIMURA YASUYUKI ,  TAMURA HIROYUKI

    IPC分类号： D06M13/402 ,  D06M13/188 ,  D06M13/463

    摘要： PROBLEM TO BE SOLVED: To provide a softening agent composition excellent in a softening effect and a deodorizing effect.
    SOLUTION: This softening agent composition contains (a) an amine compound expressed by formula (1) (R
    1 is a 1-4C alkyl group or the like; R
    2 and R
    3 are each a 11-22C hydrocarbon group; and m and n are each 1 to 6) or its inorganic acid salt in an amount of 3-50 mass%, (b) a quaternary ammonium salt expressed by formula (2) (two or three members of R
    4 , R
    5 , R
    6 and R
    7 are each an 8-12C alkyl group and the other members are each a 1-3C alkyl or the like; and Z
    - is an anionic group) in an amount of 0.1-15 mass%, and (c) an 8-22C fatty acid or its salt in an amount of 0.1-5 mass%, wherein a mass ratio of the component (a) to the component (b) is 50/1 to 15/1.
    COPYRIGHT: (C)2006,JPO&NCIPI

    摘要翻译： 待解决的问题：提供软化效果和除臭效果优异的软化剂组合物。 该软化剂组合物含有（a）由式（1）表示的胺化合物（R 1 SP 1是1-4C烷基等; R 2， SP＆gt;和R＆lt; SP＆gt; 3＆lt; SP＆gt;各自为11-22C烃基，m和n各自为1〜6）或其无机酸盐为3-50质量％，（b） 由式（2）表示的季铵盐（R 4 ，R 5 ，R SP 6和/或SP 7的两个或三个成员 各自为8-12C烷基，其它成员各自为1-3C烷基等; Z - 为阴离子基团），其量为0.1-15质量％ ，（c）成分（a）与成分（b）的质量比为50/1〜15/1的碳原子数为8〜22的脂肪酸或其盐，为0.1〜5质量％。 版权所有（C）2006，JPO＆NCIPI

    METHOD FOR PRODUCING α-AMINOKETONE COMPOUND
    3.
    发明专利
    METHOD FOR PRODUCING α-AMINOKETONE COMPOUND 有权
    生产α-氨基酮类化合物的方法

    公开(公告)号：JP2010173970A

    公开(公告)日：2010-08-12

    申请号：JP2009018559

    申请日：2009-01-29

    申请人： Kao Corp ,  花王株式会社

    发明人： WATANABE MASAHIKO ,  TATENO GOSUKE ,  MIMURA YASUYUKI

    IPC分类号： C07C221/00 ,  C07C225/20

    摘要： PROBLEM TO BE SOLVED: To provide a method for producing an α-aminoketone compound in one step by using a tri- or more hydric alcohol. SOLUTION: The method for producing the α-aminoketone compound comprises reaction of the tri- or more hydric alcohol (B) with a secondary amine compound (C) in the presence of a catalyst (A) containing one or more metal components selected from cobalt, yttrium and palladium. COPYRIGHT: (C)2010,JPO&INPIT

    摘要翻译： 待解决的问题：提供一种通过使用三价或更多种醇制成α-氨基酮化合物的方法。 解决方案：α-氨基酮化合物的制备方法包括在含有一种或多种金属组分的催化剂（A）的存在下，三元醇或更多的乙醇（B）与仲胺化合物（C）的反应 选自钴，钇和钯。 版权所有（C）2010，JPO＆INPIT

    PRODUCTION OF ALIPHATIC NITRILE
    5.
    发明专利
    PRODUCTION OF ALIPHATIC NITRILE 失效

    公开(公告)号：JP2000080069A

    公开(公告)日：2000-03-21

    申请号：JP14041499

    申请日：1999-05-20

    申请人： KAO CORP

    发明人： TERASAKA MICHIO ,  MIMURA YASUYUKI ,  ABE YUTAKA

    IPC分类号： B01J21/06 ,  B01J23/08 ,  B01J23/20 ,  C07B61/00 ,  C07C253/22 ,  C07C255/03

    摘要： PROBLEM TO BE SOLVED: To obtain an aliphatic nitrile having a high quality in a high yield by reacting an aliphatic carboxylic acid with ammonia in the presence of a highly active compound oxide catalyst slightly soluble in the reaction solution. SOLUTION: This method for producing (D) an aliphatic nitrile comprises reacting (A) an aliphatic carboxylic acid with (B) ammonia in the presence of (C) a compound oxide catalyst containing titanium oxide as a main component. The component A is preferably a 6-22C carboxylic acid, preferably caproic acid, caprylic acid, capric acid, lauric acid, etc. The component C is preferably a compound oxide catalyst comprising titanium dioxide and the oxides of one or more elements selected from the group consisting of niobium, zirconium, tantalum, gallium, and germanium. The oxides except the titanium dioxide in the component C are preferably contained in an amount of 1-25 wt.%. Thereby, the catalyst is not dissolved in the product, and the product having a high quality can be provided.

    PRODUCTION OF ALIPHATIC NITRILE
    6.
    发明专利
    PRODUCTION OF ALIPHATIC NITRILE 失效

    公开(公告)号：JP2000016977A

    公开(公告)日：2000-01-18

    申请号：JP11799099

    申请日：1999-04-26

    申请人： KAO CORP

    发明人： TERASAKA MICHIO ,  MIMURA YASUYUKI ,  ABE YUTAKA

    IPC分类号： B01J23/20 ,  C07B61/00 ,  C07C253/22 ,  C07C255/03

    摘要： PROBLEM TO BE SOLVED: To produce an aliphatic nitrile having high quality in high yield at a low cost without causing the dissolution of catalyst into the product by reacting an aliphatic carboxylic acid with ammonia in the presence of niobium oxide. SOLUTION: The objective compound is produced by reacting preferably 6-22C aliphatic carboxlylic acid (e.g. caproic acid or caprylic acid) with ammonia in the presence of preferably 0.3-3 wt.% (based on the carboxylic acid) of niobium oxide (e.g. niobium pentaoxide or niobium tetraoxide) treated with an aqueous solution of an acid (preferably hydrochloric acid or boric acid) having a concentration of preferably 0.1-5 mol/L preferably at 250-300 deg.C. In the case of performing the reaction by a fixed bed flow process, the average retention time of the reaction mixture in the catalyst layer is preferably 1 sec to 10 min. The niobium oxide can be produced by suspending niobium oxide in an aqueous solution of an acid for >=24 hr and evaporating the mixture to dryness and baking preferably at

    PRODUCTION OF HIGH-QUALITY TERTIARY AMINE
    7.
    发明专利
    PRODUCTION OF HIGH-QUALITY TERTIARY AMINE 失效

    公开(公告)号：JPH11116539A

    公开(公告)日：1999-04-27

    申请号：JP27432097

    申请日：1997-10-07

    申请人： KAO CORP

    发明人： TANIGUCHI HIDEKI ,  MIMURA YASUYUKI ,  ABE YUTAKA

    IPC分类号： B01J23/755 ,  C07B61/00 ,  C07C209/16 ,  C07C209/60 ,  C07C209/84 ,  C07C211/08

    摘要： PROBLEM TO BE SOLVED: To obtain a high-quality aliphatic tertiary amine which contains little non-amine components such as esters and alcohols, and has good hue, and a derivative from which gives no turbidity even after long term storage. SOLUTION: The amine is obtained by (i) reacting a molecule of an aliphatic primary alcohol with a molecule of dimethylamine, (ii) reacting two molecules of an aliphatic primary alcohol with a molecule of methylamine, or (iii) reacting three molecules of an aliphatic primary alcohol with a molecule of ammonia, to give a crude aliphatic tertiary amine, and adding an alkali to the obtained product, followed by distillation.

    PRODUCTION OF ALIPHATIC NITRILE
    8.
    发明专利
    PRODUCTION OF ALIPHATIC NITRILE 失效

    公开(公告)号：JP2000080070A

    公开(公告)日：2000-03-21

    申请号：JP14041599

    申请日：1999-05-20

    申请人： KAO CORP

    发明人： MIMURA YASUYUKI ,  TERASAKA MICHIO ,  ABE YUTAKA

    IPC分类号： B01J21/06 ,  B01J23/08 ,  B01J23/20 ,  C07B61/00 ,  C07C253/22 ,  C07C255/03

    摘要： PROBLEM TO BE SOLVED: To obtain an aliphatic nitrile having a high quality in a high yield at a low cost by reacting an aliphatic carboxylic acid lower alkyl ester with ammonia in the presence of a highly active compound oxide catalyst slightly soluble in the reaction solution. SOLUTION: This method for producing (D) an aliphatic nitrile comprises reacting (A) an aliphatic carboxylic acid lower alkyl ester with (B) ammonia in the presence of (C) a compound oxide catalyst containing titanium oxide as a main component. The component A is preferably a 6-22C carboxylic acid methyl ester, preferably caproic acid methyl ester, caprylic acid methyl ester, etc. The component C is preferably a compound oxide catalyst comprising titanium dioxide and the oxides of one or more elements selected from the group consisting of niobium, zirconium, tantalum, gallium, and germanium. The oxides except the titanium dioxide in the component C are preferably contained in an amount of 1-25 wt.%. The component has high activity at a temperature of