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公开(公告)号：US5525323A
公开(公告)日：1996-06-11
申请号：US266353
申请日：1994-06-30
申请人： Ulrich Mueller , Axel Reich , Klaus Unger
发明人： Ulrich Mueller , Axel Reich , Klaus Unger
IPC分类号： B01J20/18 , B01J29/04 , B01J29/40 , B01J35/08 , C01B39/36 , C07C45/46 , C07C45/73 , C07C45/74
CPC分类号： C07C45/73 , B01J20/183 , B01J29/04 , B01J29/40 , B01J35/08 , C01B39/36 , C07C45/46 , C07C45/74 , B01J2229/26 , B01J2229/36 , B01J2229/42 , Y02P20/582 , Y10S423/22 , Y10S423/29 , Y10S423/34
摘要： Abstract of the Disclosure: Pentasil zeolites agglomerated in the form of hollow spheres and having a particle size of from 5 to 200 micron are prepared by treating a mixture of an aqueous alkylenediamine, alkylenetriamine and/or alkylenetetramine, silica and an aluminum, boron and/or titanium salt at from 20.degree. to 100.degree. C., then crystallizing the product at from 110.degree. to 200.degree. C. and from 0.01 to 50 bar and calcining it at from 400.degree. to 650.degree. C., and said zeolites are used as catalysts and/or adsorbents.
摘要翻译： 公开摘要：通过处理亚烷基二胺，亚烷基三胺和/或亚烷基四胺，二氧化硅和铝，硼和/或其混合物的混合物来制备中空球形式并且具有5至200微米粒度的pentasil沸石， 或钛盐，然后在110℃至200℃和0.01至50巴下使产物结晶，并在400至650℃下煅烧，并使用所述沸石 作为催化剂和/或吸附剂。
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公开(公告)号：US5368836A
公开(公告)日：1994-11-29
申请号：US024967
申请日：1993-03-02
申请人： Michael Grebner , Axel Reich , Horst Reichert , Ferdi Schuth , Klaus Unger
发明人： Michael Grebner , Axel Reich , Horst Reichert , Ferdi Schuth , Klaus Unger
IPC分类号： B01D53/02 , B01J20/10 , B01J20/30 , C01B3/00 , C01B23/00 , C01B33/20 , C01B37/02 , C01B39/04 , C01C1/12 , C01B33/26
摘要： The invention relates to a process for the preparation of low-template clathrasil, comprising heat-treating an alkaline aqueous silicate-containing medium containing crystallization seeds and an amount of a template such that the template content of the clathrasil, relative to the number of moles of the SiO.sub.2 of the medium, is less than 2 mol %.
摘要翻译： 本发明涉及一种制备低模板层状蓝宝石的方法，包括热处理含有结晶晶种的碱性含水硅酸盐介质和一定量的模板，使得相对于摩尔数的摩尔数的模板含量 的介质的SiO 2小于2摩尔％。
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公开(公告)号：US06656522B2
公开(公告)日：2003-12-02
申请号：US10139477
申请日：2002-05-06
IPC分类号： B05D302
CPC分类号： C23C18/1225 , C03C17/3417 , C23C18/1216 , C23C18/1254 , G02B1/115 , Y10T428/24942 , Y10T428/24975 , Y10T428/265
摘要： The invention includes a bilayer antireflection coating, multilayer antireflection coatings, and a method for making a multilayer antireflective coated substrate. The bilayer and multilayer coatings include layers having metallic oxides, at least one layer in each of such coatings having as a material with an index of refraction at least about 1.90, a layer comprising oxides of zirconium such that when subjected to heat treatments, such as tempering, the coatings substantially retain their optical properties. The coatings further include layers having materials of low index of refraction which include oxides of aluminum which provide coating stability and increased precursor storage life. In the method, the layers are applied by successive dip coating techniques using solvent-based solutions and the resulting coatings can be used to coat large sized substrates which can be later cut, trimmed and/or otherwise shaped and later heat treated with substantial retention of optical properties.
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4.发明授权Antireflection coatings and other multilayer optical coatings for heat-treatable inorganic substrates and methods for making same 失效用于可热处理的无机基材的抗反射涂层和其它多层光学涂层及其制造方法公开(公告)号：US06410173B1
公开(公告)日：2002-06-25
申请号：US09201599
申请日：1998-11-30
IPC分类号： B32B900
CPC分类号： C23C18/1225 , C03C17/3417 , C23C18/1216 , C23C18/1254 , G02B1/115 , Y10T428/24942 , Y10T428/24975 , Y10T428/265
摘要： The invention includes a bilayer antireflection coating, multilayer antireflection coatings, and a method for making a multilayer antireflective coated substrate. The bilayer and multilayer coatings include layers having metallic oxides, at least one layer in each of such coatings having as a material with an index of refraction at least about 1.90, a layer comprising oxides of zirconium such that when subjected to heat treatments, such as tempering, the coatings substantially retain their optical properties. The coatings further include layers having materials of low index of refraction which include oxides of aluminum which provide coating stability and increased coating solution storage life. In the method, the layers are applied by successive dip coating techniques using solvent-based solutions and the resulting coatings can be used to coat large sized substrates which can be later cut, trimmed and/or otherwise shaped and later heat treated with substantial retention of optical properties.
摘要翻译： 本发明包括双层抗反射涂层，多层抗反射涂层以及制备多层抗反射涂层基材的方法。 双层和多层涂层包括具有金属氧化物的层，每个这样的涂层中的至少一个层具有折射率至少约1.90的材料，包含锆的氧化物的层，使得当经受热处理时，例如 回火，涂层基本保持其光学性能。 涂层还包括具有低折射率的材料的层，其包括提供涂层稳定性和增加的涂层溶液储存寿命的铝的氧化物。 在该方法中，通过使用基于溶剂的溶液的连续浸涂技术来施加层，并且所得到的涂层可用于涂覆大尺寸的基底，其可以稍后切割，修剪和/或以其它方式成形，然后以大量保留 光学性能。
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5.发明授权Clathrasil of the dodecasil 1 H structural type having a small average crystal size 失效十二面体1 H结构型的斜纹石具有小的平均晶体尺寸
公开(公告)号：US5435988A
公开(公告)日：1995-07-25
申请号：US24962
申请日：1993-03-02
申请人： Michael Grebner , Axel Reich , Ferdi Schuth , Klaus Unger
发明人： Michael Grebner , Axel Reich , Ferdi Schuth , Klaus Unger
IPC分类号： A61K8/18 , A61K8/25 , A61K8/41 , A61K8/46 , A61K8/49 , A61Q1/02 , B01J13/06 , C01B33/20 , C01B37/02 , C01B39/00 , C01B39/04 , C08K3/34 , C08K9/04 , C09B67/02 , C09C1/28 , C09C3/06 , C09C3/08 , C09D7/12 , C09D17/00 , C01B33/26 , B01J29/06
CPC分类号： C01B37/02 , C09C1/28 , C09C3/08 , C01P2002/30
摘要： The invention relates to a process for the preparation of crystalline clathrasil of the dodecasil 1 H structural type having an average crystal size of not more than 20 .mu.m, characterised in that an alkaline aqueous silicate-containing medium comprising templates and crystallisation seeds is heat-treated, the crystallisation seeds content, relative to the SiO.sub.2 content of the medium, being not less than 1% by weight.
摘要翻译： 本发明涉及一种制备平均晶体尺寸不超过20μm的十二硅胶结构型结晶型螯合物的方法，其特征在于含有模板和结晶种子的碱性含水硅酸盐介质是热 - 相对于介质的SiO 2含量的结晶种子含量不小于1重量％。
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