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公开(公告)号：US5741850A
公开(公告)日：1998-04-21
申请号：US704478
申请日：1996-08-27
CPC分类号： C08J3/03 , B01F3/0807 , B01F3/0853 , B01F7/00 , C08J2383/04
摘要： A method capable of the continuous mass-production without pressurization and using a low drive force of highly uniform and very storage-stable organopolysiloxane emulsions. The method for the continuous preparation of organopolysiloxane emulsions includes processes (I) and (II). Process (I) is the continuous supply of (a) organopolysiloxane fluid or gum, (b) emulsifying agent, and (c) water to a mixer having a first-stage shearing and stirring mechanism with a stator and a turbine-type rotor having blades that are slanted obliquely from the radial direction when viewed from the axial direction, and a second-stage shearing and stirring mechanism with a stator and a turbine-type rotor having blades that describe spiral curves with respect to the axial direction, and the discharge of an organopolysiloxane-in-water emulsion with an organopolysiloxane content of 10 to 99 weight %. Process (II) is the introduction of dilution water and the emulsion of process (I) into a mixer as described for process (I). A gas can also be injected in process (I).
摘要翻译： 能够连续大量生产而不加压并且使用高度均匀且非常储存稳定的有机基聚硅氧烷乳液的低驱动力的方法。 连续制备有机聚硅氧烷乳液的方法包括方法（I）和（II）。 方法（I）是连续供应（a）有机聚硅氧烷流体或胶，（b）乳化剂，和（c）水到具有第一级剪切和搅拌机构的混合器中，定子和涡轮型转子具有 从轴向观察时沿径向倾斜倾斜的叶片，具有定子的涡轮式转子的第二级剪切搅拌机构，具有描述相对于轴向的螺旋曲线的叶片的涡轮型转子， 的有机聚硅氧烷含量为10至99重量％的有机聚硅氧烷水包油乳液。 方法（II）是按照方法（I）所述将稀释水和方法（I）的乳液引入混合器中。 在工艺（I）中也可以注入气体。
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公开(公告)号：US5806975A
公开(公告)日：1998-09-15
申请号：US736634
申请日：1996-10-24
CPC分类号： C08J3/03 , B01F3/10 , B01F7/042 , B29B7/46 , B29B7/482 , B29C47/6087 , B29C47/662 , B01F3/0807 , C08J2383/04
摘要： A method of continuous emulsification that can emulsify high-viscosity organopolysiloxane gums and is capable of continuous mass production. A compounding extruder is used whose barrel 1 contains at least 2 mixing element-equipped shafts 3 installed in parallel. On each shaft elevations and depressions are formed along the axial direction and the elevations and depressions on respective shafts intermesh. Organopolysiloxane gum, emulsifying agent, and water are continuously supplied as starting materials to this compounding extruder, and an organopolysiloxane-in-water emulsion is produced by mixing and homogenizing the starting materials by subjecting them through rotation of the mixing element-equipped shafts to a shearing action at a shear rate of at least 10/second (i.e. 10 reciprocal seconds).
摘要翻译： 连续乳化的方法，其可以乳化高粘度有机聚硅氧烷胶，并能够连续批量生产。 使用复合挤出机，其机筒1包含至少两个并联安装的混合元件的轴3。 在每个轴上，沿着轴向形成高度和凹陷，并且各轴的高度和凹陷互相啮合。 将有机聚硅氧烷胶，乳化剂和水作为起始原料连续地供给到该配混挤出机中，通过使原料混合并使其混合均匀化的轴旋转至 剪切速率至少为10 /秒（即10倒数秒）。
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公开(公告)号：US06448360B2
公开(公告)日：2002-09-10
申请号：US09765047
申请日：2001-01-19
IPC分类号： C08G7708
CPC分类号： C08G77/20 , C07F7/0874 , C08G77/045
摘要： A process for the production of a cyclic siloxane described by formula (R1(CH3)SiO)d comprising reacting in the presence of an alkali catalyst a siloxane mixture comprising a silane or a linear siloxane described by general formula HO(R1(CH3)SiO)bH and a cyclic siloxane described by general formula (R1(CH3)SiO)c, where R1 is an alkenyl group having 6 to 14 carbon atoms, b is an integer of one or greater, c is an integer of 3 or greater, and d is an integer of 3 or greater.
摘要翻译： 通过在碱催化剂存在下反应制备环状硅氧烷的方法，所述硅氧烷混合物包含由通式表示的硅烷或线性硅氧烷和由通式R 1表示的环状硅氧烷，所述硅氧烷混合物是具有6至14个 碳原子，b为1以上的整数，c为3以上的整数，d为3以上的整数。
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公开(公告)号：US5942574A
公开(公告)日：1999-08-24
申请号：US5677
申请日：1998-01-12
CPC分类号： C08J3/03 , B01F3/10 , B01F7/042 , B29B7/46 , B29B7/482 , B29C47/6087 , B29C47/662 , B01F3/0807 , C08J2383/04
摘要： A method of continuous emulsification that can emulsify high-viscosity organopolysiloxane gums and is capable of continuous mass production. A compounding extruder is used whose barrel 1 contains at least 2 mixing element-equipped shafts 3 installed in parallel. On each shaft elevations and depressions are formed along the axial direction and the elevations and depressions on respective shafts intermesh. Organopolysiloxane gum, emulsifying agent, and water are continuously supplied as starting materials to this compounding extruder, and an organopolysiloxane-in-water emulsion is produced by mixing and homogenizing the starting materials by subjecting them through rotation of the mixing element-equipped shafts to a shearing action at a shear rate of at least 10/second (i.e. 10 reciprocal seconds).
摘要翻译： 连续乳化的方法，其可以乳化高粘度有机聚硅氧烷胶，并能够连续批量生产。 使用复合挤出机，其机筒1包含至少两个并联安装的混合元件的轴3。 在每个轴上，沿着轴向形成高度和凹陷，并且各轴的高度和凹陷互相啮合。 将有机聚硅氧烷胶，乳化剂和水作为起始原料连续地供给到该配混挤出机中，通过使原料混合并使其混合均匀化的轴旋转至 剪切速率至少为10 /秒（即10倒数秒）。
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公开(公告)号：US5665796A
公开(公告)日：1997-09-09
申请号：US596971
申请日：1996-02-05
CPC分类号： B01F3/0853 , B01F3/0807 , B01F5/162 , B01F5/165 , B01F7/00816 , B01F7/00825 , C08J3/03 , C08J2383/04 , Y10S516/929
摘要： Method and apparatus for preparing uniform highly dispersed emulsions by using a low drive power and without pressurization, making possible continuous mass production of uniform organopolysiloxane emulsions. An organopolysiloxane, water and a emulsifying agent, are continuously fed across a first-stage shearing and stirring mechanism and a second-stage shearing and stirring mechanism. The first-stage mechanism is a stator and turbine-type rotor whose blades are slanted obliquely from the radial direction when viewed from the axial direction. The second-stage mechanism is a stator and turbine-type rotor whose blades describe spiral curves with respect to the axial direction. The two mechanisms are arranged serially and separated from one another by a relaxation zone. Emulsification is carried out in the first-stage mechanism by an intake and shearing action at a shear rate of at least 100/second, and in the second-stage mechanism by a phase reversal rotating effect and shearing action at a shear rate of at least 100/second.
摘要翻译： 通过使用低驱动力并且不加压来制备均匀的高度分散乳液的方法和装置，使连续大量生产均匀的有机聚硅氧烷乳液。 有机聚硅氧烷，水和乳化剂，连续地通过第一阶段剪切和搅拌机构和第二阶段剪切和搅拌机构。 第一级机构是从轴向观察时叶片从径向倾斜倾斜的定子和涡轮式转子。 第二级机构是定子和涡轮式转子，其叶片描述相对于轴向的螺旋曲线。 这两个机构串联布置，并通过松弛区彼此分离。 在第一阶段机理中，通过在至少100 /秒的剪切速率下的进入和剪切作用进行乳化，并且在第二阶段机理中通过相位旋转效应和至少剪切速率下的剪切作用 100 /秒。
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公开(公告)号：US5633303A
公开(公告)日：1997-05-27
申请号：US586507
申请日：1996-01-11
IPC分类号： B01J13/00 , A61K8/06 , A61K8/891 , A61Q5/02 , A61Q5/12 , A61Q19/00 , C08J3/03 , C08L83/02 , C08L83/04 , C09G1/12 , C08K3/20
摘要： An organopolysiloxane gum emulsion is afforded by the emulsification of an organopolysiloxane gum in water. The organopolysiloxane gum emulsion is useful as a cosmetic base, lustrant, lubricant, antifoam, fiber-treatment agent, and paint additive. The organopolysiloxane gum emulsion includes(A) 100 weight parts organopolysiloxane gum whose plasticity at 25.degree. C. is at least 0.75 mm,(B) 1 to 100 weight parts emulsifying agent, and(C) 3 to 800 weight parts water.
摘要翻译： 通过在水中乳化有机聚硅氧烷胶来提供有机聚硅氧烷胶乳。 有机聚硅氧烷胶乳可用作化妆品基质，发光剂，润滑剂，消泡剂，纤维处理剂和涂料添加剂。 有机聚硅氧烷胶乳含有（A）100重量份在25℃下的塑性为至少0.75mm的有机聚硅氧烷胶，（B）1至100重量份的乳化剂和（C）3至800重量份的水。
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