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    PEROXIDE CURABLE PARTIALLY FLUORINATED POLYMER
    4.
    发明申请
    PEROXIDE CURABLE PARTIALLY FLUORINATED POLYMER 审中-公开

    公开(公告)号：US20200055971A1

    公开(公告)日：2020-02-20

    申请号：US16346145

    申请日：2017-11-03

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Klaus Hintzer ,  Florian D. Jochum ,  Harald Kaspar ,  Kai H. Lochhaas ,  Tilman C. Zipplies

    IPC: C08F214/22 ,  C08F214/26 ,  C08F214/28 ,  C08F214/18

    Abstract: Described herein is a peroxide curable, partially fluorinated polymer derived from: (a) comonomers comprising: (i) 5-28 wt. % of tetrafluoroethylene; (ii) 30-70 wt. % of vinylidene fluoride; and (iii) a monomer selected from 10-45 wt. % of hexafluoropropylene and 10-40 wt, % of a perfluoro ether monomer of the formula Rf-0-(CF2)n—CF═CF2 wherein n is 1 or 0, and Rf represents a perfluoroalkyl residue which may or may not be interrupted by one or more than one oxygen atoms; (b) 0.01-2 wt % of a perfluorinated iodinated vinyl ether based on the total amount of comonomer, wherein the perfluorinated iodinated vinyl ether has the formula: F2C═CF—(CF2)m(0)o—(CF2)n—O—(CF2)p—I where m is 0 or 1; n is an integer of 0-5: o is 0 or 1: and p is an integer of 1-5, wherein when n is 0, o is 0; and (c) 0.01-2 wt % of a chain transfer agent based on the total amount of comonomers wherein the chain transfer agent consists of a diiodo-fluoroalkane and a diiodo-methane. Further described are methods of making the curable partially fluorinated polymers and articles comprising the cured fluoropolymer.

    HIGHLY FLUORINATED ELASTOMERS
    7.
    发明申请
    HIGHLY FLUORINATED ELASTOMERS 有权
    高荧光弹性体

    公开(公告)号：US20170066877A1

    公开(公告)日：2017-03-09

    申请号：US15122538

    申请日：2015-03-03

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Klaus Hintzer ,  Florian D. Jochum ,  Harald Kaspar ,  Kai H. Lochhaas ,  Tilman C. Zipplies ,  Tatsuo Fukushi

    IPC: C08G65/00

    CPC classification number: C08G65/007 ,  C08F214/262 ,  C08K5/06 ,  C08L23/28

    Abstract: Described herein is a peroxide curable, highly fluorinated elastomer derived from (a) a fluorinated di-iodo ether compound of the following formula I: Rf—CF(I)—(CX2)n(CX2CXR)m—O—R″f-Ok—(CXR′CX2)p—(CX2)q—CF(I)—R′f wherein X is independently selected from F, H, and Cl; Rf and R′f are independently selected from F and a monovalent perfluoroalkane having 1-3 carbons; R is F, or a partially fluorinated or perfluorinated alkane comprising 1-3 carbons; R″f is a divalent fluoroalkylene having 1-5 carbons or a divalent fluorinated alkylene ether having 1-8 carbons and at least one ether linkage; k is 0 or 1; and n, m, and p are independently selected from an integer from 0-5, with the proviso that when k is 0, n+m is at least 1 and p+q is at least 1; and (b) a fluorinated monomer.

    Abstract translation: 本文描述的是一种过氧化物可固化的高度氟化的弹性体，其衍生自（a）下式I的氟化二碘醚化合物：Rf-CF（I） - （CX2）n（CX2CXR）m-O-R“f- （CXR'CX2）p-（CX2）q-CF（I）-R'f其中X独立地选自F，H和Cl; Rf和R'f独立地选自F和具有1-3个碳的单价全氟烷烃; R是F，或包含1-3个碳的部分氟化或全氟化烷烃; R“f是具有1-5个碳的二价氟代亚烷基或具有1-8个碳原子和至少一个醚键的二价氟化亚烷基醚; k为0或1; 并且n，m和p独立地选自0-5的整数，条件是当k为0时，n + m为至少1，p + q为至少1; 和（b）氟化单体。

    Composition including amorphous fluoropolymer and fluoroplastic particles and methods of making the same
    9.
    发明授权
    Composition including amorphous fluoropolymer and fluoroplastic particles and methods of making the same 有权

    公开(公告)号：US10557031B2

    公开(公告)日：2020-02-11

    申请号：US15769933

    申请日：2016-10-19

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Tamon Aoki ,  Allen M. Sohlo ,  Yuta Suzuki ,  Kai H. Lochhaas ,  Florian D. Jochum ,  Klaus Hintzer ,  Tilman C. Zipplies

    IPC: C08L15/02 ,  C08L27/18

    Abstract: A composition includes an amorphous fluoropolymer having at least one of: a segment represented by formula I: —CF(Rf)—(CX2)n—(CX2CXR)m—O—R″fOk—(CXR′CX2)p—(CX2)q—CF(R′f)— (I); or a terminal segment represented by formula III: Rf—CF(I)—(CX2)n—(CX2CXR)m—O—R″fOk—(CXR′CX2)p—(CX2)q—CF(R′f)— (III), and fluoroplastic particles having a mean particle size of less than 500 nanometers. Each X is independently F, H, or Cl; Rf and R′f are each independently F or a monovalent perfluoroalkyl having 1 to 3 carbon atoms; R is F or a partially fluorinated or perfluorinated alkyl having 1 to 3 carbon atoms; R″f is a divalent fluoroalkylene having 1 to 8 carbon atoms or a divalent fluorinated alkylene ether having 1 to 20 carbon atoms and at least one ether linkage; k is 0 or 1; and n, m, p, and q are each independently an integer from 0 to 5, with the proviso that when k is 0, n+m is at least 1 and p+q is at least 1. A method of making the composition is also provided.

    Highly fluorinated elastomers
    10.
    发明授权
    Highly fluorinated elastomers 有权

    公开(公告)号：US09982091B2

    公开(公告)日：2018-05-29

    申请号：US15122538

    申请日：2015-03-03

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Klaus Hintzer ,  Florian D. Jochum ,  Harald Kaspar ,  Kai H. Lochhaas ,  Tilman C. Zipplies ,  Tatsuo Fukushi

    IPC: C08G65/00 ,  C08L23/28 ,  C08L15/02

    CPC classification number: C08G65/007 ,  C08F214/262 ,  C08K5/06 ,  C08L23/28

    Abstract: Described herein is a peroxide curable, highly fluorinated elastomer derived from (a) a fluorinated di-iodo ether compound of the following formula I: Rf—CF(I)—(CX2)n—(CX2CXR)m—O—R″f-Ok—(CXR′CX2)p—(CX2)q—CF(I)—R′f wherein X is independently selected from F, H, and Cl; Rf and R′f are independently selected from F and a monovalent perfluoroalkane having 1-3 carbons; R is F, or a partially fluorinated or perfluorinated alkane comprising 1-3 carbons; R″f is a divalent fluoroalkylene having 1-5 carbons or a divalent fluorinated alkylene ether having 1-8 carbons and at least one ether linkage; k is 0 or 1; and n, m, and p are independently selected from an integer from 0-5, with the proviso that when k is 0, n+m is at least 1 and p+q is at least 1; and (b) a fluorinated monomer.

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