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公开(公告)号：US08772547B2
公开(公告)日：2014-07-08
申请号：US13255805
申请日：2010-03-11
申请人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
发明人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
IPC分类号： C07C211/00
CPC分类号： C07C211/63 , C07C209/00 , C07C209/26 , C07C2603/74
摘要： The present invention relates to a process for preparing 1-adamantyltrimethylammonium hydroxide, by A) reacting 1-adamantyldimethylamine with dimethyl sulfate to give 1-adamantyltrimethylammonium sulfate; and B) subjecting the 1-adamantyltrimethylammonium sulfate obtained in A) to anion exchange with an ion exchanger loaded with OH ions.
摘要翻译： 本发明涉及一种制备1-金刚烷基三甲基氢氧化铵的方法，通过A）使1-金刚烷基二甲胺与硫酸二甲酯反应得到1-金刚烷基三甲基硫酸铵; 和B）在A）中获得的1-金刚烷基三甲基硫酸铵与负载有OH离子的离子交换剂进行阴离子交换。
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2.发明申请METHOD FOR PRODUCING 1-ADAMANTYL TRIMETHYLAMMONIUM HYDROXIDE 有权1-ADAMANTYL TRIMETHYLAMMONIUM HYDROXIDE的生产方法公开(公告)号：US20120010431A1
公开(公告)日：2012-01-12
申请号：US13255805
申请日：2010-03-11
申请人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
发明人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
IPC分类号： C07C211/33
CPC分类号： C07C211/63 , C07C209/00 , C07C209/26 , C07C2603/74
摘要： The present invention relates to a process for preparing 1-adamantyltrimethyl-ammonium hydroxide.
摘要翻译： 本发明涉及一种制备1-金刚烷基三甲基氢氧化铵的方法。
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公开(公告)号：US20060276649A1
公开(公告)日：2006-12-07
申请号：US10566419
申请日：2004-07-15
申请人： Matthias Frauenkron , Thomas Krug , Holger Evers , Johann-Peter Melder , Roderich Rottger , Markus Siegert , Till Gerlach , Jan Nouwen , Ellen Dahlhoff , Christian Miller
发明人： Matthias Frauenkron , Thomas Krug , Holger Evers , Johann-Peter Melder , Roderich Rottger , Markus Siegert , Till Gerlach , Jan Nouwen , Ellen Dahlhoff , Christian Miller
IPC分类号： C07D241/04 , C07C211/13 , C07C211/09
CPC分类号： C07C209/64 , C07C211/14
摘要： Process for the preparation of ethylenamines, in particular diethylenetriamine (DETA), by continuous reaction of ethylenediamine (EDA) in the presence of a heterogeneous catalyst, where the reaction is carried out in a reaction column.
摘要翻译： 通过乙二胺（EDA）在多相催化剂存在下连续反应制备乙烯胺，特别是二亚乙基三胺（DETA）的方法，其中反应在反应塔中进行。
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公开(公告)号：US07393978B2
公开(公告)日：2008-07-01
申请号：US10566419
申请日：2004-07-15
申请人： Matthias Frauenkron , Thomas Krug , Holger Evers , Johann-Peter Melder , Roderich Röttger , Markus Siegert , Till Gerlach , Jan Nouwen , Ellen Dahlhoff , Christian Miller
发明人： Matthias Frauenkron , Thomas Krug , Holger Evers , Johann-Peter Melder , Roderich Röttger , Markus Siegert , Till Gerlach , Jan Nouwen , Ellen Dahlhoff , Christian Miller
IPC分类号： C07C209/60
CPC分类号： C07C209/64 , C07C211/14
摘要： Process for the preparation of ethylenamines, in particular diethylenetriamine (DETA), by continuous reaction of ethylenediamine (EDA) in the presence of a heterogeneous catalyst, where the reaction is carried out in a reaction column.
摘要翻译： 通过乙二胺（EDA）在多相催化剂存在下连续反应制备乙烯胺，特别是二亚乙基三胺（DETA）的方法，其中反应在反应塔中进行。
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5.发明申请公开(公告)号：US20070135637A1
公开(公告)日：2007-06-14
申请号：US10581311
申请日：2004-12-02
申请人： Marco Bosch , Ulrich Muller , Matthias Frauenkron
发明人： Marco Bosch , Ulrich Muller , Matthias Frauenkron
IPC分类号： C01B39/00 , B01J29/00 , B01J29/06 , C07D487/04
CPC分类号： B01J29/40 , B01J35/023 , B01J37/0009 , B01J37/0018 , B01J2229/42 , C01B39/36 , C01B39/40 , C07D487/08
摘要： Zeolite material of the pentasil type has an alkali metal and alkaline earth metal content of not more than 100 ppm and a molar ratio of Si to Al of from 250 to 1500, at least 90% of the primary particles of the zeolite material being spherical and 95% by weight of the spherical primary particles having a diameter of less than or equal to 1 μm.
摘要翻译： pentasil型沸石材料的碱金属和碱土金属含量不超过100ppm，Si与Al的摩尔比为250至1500，沸石材料的初级颗粒的至少90％为球形， 95重量％的直径小于或等于1μm的球形初级颗粒。
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公开(公告)号：US06365740B1
公开(公告)日：2002-04-02
申请号：US09811433
申请日：2001-03-20
IPC分类号： C07D23942
CPC分类号： C07D239/42
摘要： 2-Methyl-4-amino-5-aminomethylpyrimidine of the formula 1 is prepared by reacting 2-methyl-4-amino-5-alkoxymethylpyrimidine of the formula 2 where R=C1-C6-alkyl, with ammonia in the presence of a catalyst.
摘要翻译： 将式1的2-甲基-4-氨基-5-氨基甲基嘧啶与催化剂存在下的氨反应制得，其中式2的2-甲基-4-氨基-5-烷氧基甲基嘧啶，其中R = C 1 -C 6 - 烷基。
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公开(公告)号：US07872131B2
公开(公告)日：2011-01-18
申请号：US11579923
申请日：2005-05-13
申请人： Ortmund Lang , Matthias Frauenkron
发明人： Ortmund Lang , Matthias Frauenkron
IPC分类号： C07D487/08
CPC分类号： C07D487/08
摘要： Process for preparing a solution of pure triethylenediamine (TEDA), in which TEDA is vaporized, the gaseous TEDA is passed into a liquid solvent 1 (quench) and the TEDA is crystallized from the resulting solution and separated off (solid-liquid separation), wherein the crystalline TEDA obtained is dissolved in a solvent 2 and a stripping gas is passed through the resulting solution (stripping).
摘要翻译： 制备TEDA蒸发的纯三亚乙基二胺（TEDA）溶液的方法，将气态TEDA送入液体溶剂1（骤冷），并将TEDA从所得溶液中结晶并分离（固液分离） 其中将获得的结晶TEDA溶解在溶剂2中，并使汽提气体通过所得溶液（汽提）。
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8.发明授权Shaped body containing a microporous material and at least one silicon-containing binder, method for the production thereof and its use as a catalyst, particularly in a method for producing triethylenediamine (TEDA). 有权包含微孔材料和至少一种含硅粘合剂的成形体，其制备方法及其作为催化剂的用途，特别是在三亚乙基二胺（TEDA）的制造方法中。公开(公告)号：US07582583B2
公开(公告)日：2009-09-01
申请号：US11629889
申请日：2005-06-10
申请人： Marco Bosch , Matthias Frauenkron , Milan Kostur , Otto Hofstadt
发明人： Marco Bosch , Matthias Frauenkron , Milan Kostur , Otto Hofstadt
IPC分类号： B01J29/06 , C07C209/60
CPC分类号： B01J37/086 , B01J29/06 , B01J29/40 , B01J35/002 , B01J35/023 , B01J37/0009 , B01J2229/42 , C07D487/08 , Y10T428/256
摘要： Process for producing a shaped body comprising a microporous material and at least one silicon-containing binder, which comprises the steps (I) preparing a mixture comprising the microporous material, the binder, a make-up aid and a solvent, (II) mixing and densifying the mixture, (III) shaping the densified mixture to give a shaped body, (IV) drying the shaped body and (V) calcining the dried shaped body, wherein the binder used is an organosilicon compound, shaped bodies which can be produced by this process, their use as catalyst, in particular in organic synthesis and very particularly preferably in a process for preparing triethylenediamine (TEDA).
摘要翻译： 包括微孔材料和至少一种含硅粘合剂的成形体的制造方法，其包括步骤（I）制备包含微孔材料，粘合剂，补充助剂和溶剂的混合物，（II）混合 （III）使致密混合物成形，得到成型体，（IV）干燥成形体，（V）煅烧干燥的成形体，其中使用的粘合剂是有机硅化合物，可以生产的成形体 通过该方法，它们用作催化剂，特别是在有机合成中，非常特别优选用于制备三亚乙基二胺（TEDA）的方法。
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公开(公告)号：US20080312439A1
公开(公告)日：2008-12-18
申请号：US12095868
申请日：2006-12-07
申请人： Ortmund Lang , Jurgen Ciprian , Matthias Rauls , Matthias Frauenkron , Gunther van Cauwenberge , Jan Nouwen
发明人： Ortmund Lang , Jurgen Ciprian , Matthias Rauls , Matthias Frauenkron , Gunther van Cauwenberge , Jan Nouwen
IPC分类号： C07D487/02
CPC分类号： C07D487/08
摘要： The present invention relates to a process for working up triethylenediamine (TEDA) in which TEDA is vaporized and the gaseous TEDA is introduced into a solvent, subsequently crystallized and separated off from this and the mother liquor formed is extracted with an extractant, wherein the raffinate phase obtained after the extraction stage is worked up further by adsorption in which extractant and/or by-products and intermediates present in the raffinate phase are removed therefrom.
摘要翻译： 本发明涉及一种处理其中TEDA蒸发并将气态TEDA引入溶剂中的三亚乙基二胺（TEDA）的方法，随后结晶并与其分离，形成的母液用萃取剂萃取，其中萃余剂 通过吸附进一步处理提取阶段之后获得的相，其中从其中除去萃余剂和/或副产物和存在于萃余相中的中间体。
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公开(公告)号：US20080021218A1
公开(公告)日：2008-01-24
申请号：US11579923
申请日：2005-05-13
申请人： Ortmund Lang , Matthias Frauenkron
发明人： Ortmund Lang , Matthias Frauenkron
IPC分类号： C07D487/08
CPC分类号： C07D487/08
摘要： Process for preparing a solution of pure triethylenediamine (TEDA), in which TEDA is vaporized, the gaseous TEDA is passed into a liquid solvent 1 (quench) and the TEDA is crystallized from the resulting solution and separated off (solid-liquid separation), wherein the crystalline TEDA obtained is dissolved in a solvent 2 and a stripping gas is passed through the resulting solution (stripping).
摘要翻译： 制备TEDA蒸发的纯三亚乙基二胺（TEDA）溶液的方法，将气态TEDA送入液体溶剂1（骤冷），并将TEDA从所得溶液中结晶并分离（固液分离） 其中将获得的结晶TEDA溶解在溶剂2中，并使汽提气体通过所得溶液（汽提）。
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