Method for preparation of cross-condensed compound between amino acids and aminoalkylsilane having alkoxy groups using microwave
    1.
    发明授权
    Method for preparation of cross-condensed compound between amino acids and aminoalkylsilane having alkoxy groups using microwave 失效
    使用微波制备具有烷氧基的氨基酸和氨基烷基硅烷之间交联的化合物的方法

    公开(公告)号:US08003815B2

    公开(公告)日:2011-08-23

    申请号:US12739598

    申请日:2008-02-22

    IPC分类号: C07F7/04

    CPC分类号: C07F7/1892

    摘要: The present invention provides a method of preparing a cross-condensed compound of an amino-acid derivative and (aminoalkyl)trialkoxysilane using microwave, including: irradiating and heating an amino-acid derivative and (aminoalkyl)trialkoxysilane in a microwave reactor to obtain a reaction product (step 1); and refining the reaction product obtained in the step 1 by removing an unreacted solid material from the reaction product and then leaving the reaction product at room temperature under vacuum to remove excess (aminoalkyl)trialkoxysilane therefrom (step 2). According to the method, since a cross-condensation reaction is performed using microwave, unlike a conventional condensation reaction, economic efficiency is increased due to no catalyst, short reaction time and no solvent. Further, the yield and selectivity of products is increased, and the condensation reaction can be environment-friendly performed because a solvent which can badly influence the environment may not be used.

    摘要翻译: 本发明提供了使用微波制备氨基酸衍生物和(氨基烷基)三烷氧基硅烷的交联稠合化合物的方法,包括:在微波反应器中照射加热氨基酸衍生物和(氨基烷基)三烷氧基硅烷,得到反应 产品(步骤1); 并通过从反应产物中除去未反应的固体物质,然后在真空下将反应产物在室温下离心以从其中除去过量的(氨基烷基)三烷氧基硅烷,从而精制步骤1中获得的反应产物(步骤2)。 根据该方法,由于使用微波进行交联缩合反应,与常规的缩合反应不同,由于没有催化剂,反应时间短,无溶剂,经济效率提高。 此外,产物的产率和选择性提高,并且缩合反应可以是环境友好的,因为可能不会使用可能严重影响环境的溶剂。

    Method for Preparation of Cross-Condensed Compound Between Amino Acids and Aminoalkylsilane Having Alkoxy Groups Using Microwave
    2.
    发明申请
    Method for Preparation of Cross-Condensed Compound Between Amino Acids and Aminoalkylsilane Having Alkoxy Groups Using Microwave 失效
    使用微波制备具有烷氧基的氨基酸和氨基烷基硅烷之间交联化合物的方法

    公开(公告)号:US20100249444A1

    公开(公告)日:2010-09-30

    申请号:US12739598

    申请日:2008-02-22

    IPC分类号: C07F7/10

    CPC分类号: C07F7/1892

    摘要: The present invention provides a method of preparing a cross-condensed compound of an amino-acid derivative and (aminoalkyl) trialkoxysilane using microwave, including: irradiating and heating an amino-acid derivative and (aminoalkyl) trialkoxysilane in a microwave reactor to obtain a reaction product (step 1); and refining the reaction product obtained in the step 1 by removing an unreacted solid material from the reaction product and then leaving the reaction product at room temperature under vacuum to remove excess (aminoalkyl) trialkoxysilane therefrom (step 2). According to the method, since a cross-condensation reaction is performed using microwave, unlike a conventional condensation reaction, economic efficiency is increased due to no catalyst, short reaction time and no solvent. Further, the yield and selectivity of products is increased, and the condensation reaction can be environment-friendly performed because a solvent which can badly influence the environment may not be used.

    摘要翻译: 本发明提供了使用微波制备氨基酸衍生物和(氨基烷基)三烷氧基硅烷的交联稠合化合物的方法,包括:在微波反应器中照射加热氨基酸衍生物和(氨基烷基)三烷氧基硅烷,得到反应 产品(步骤1); 并通过从反应产物中除去未反应的固体物质,然后在真空下将反应产物在室温下离心以从其中除去过量的(氨基烷基)三烷氧基硅烷,从而精制步骤1中获得的反应产物(步骤2)。 根据该方法,由于使用微波进行交联缩合反应,与常规的缩合反应不同,由于没有催化剂,反应时间短,无溶剂,经济效率提高。 此外,产物的产率和选择性提高,并且缩合反应可以是环境友好的,因为可能不会使用可能严重影响环境的溶剂。

    Method of manufacturing single crystal wire and other single crystal metallic articles
    3.
    发明授权
    Method of manufacturing single crystal wire and other single crystal metallic articles 有权
    单晶线及其他单晶金属制品的制造方法

    公开(公告)号:US08663388B2

    公开(公告)日:2014-03-04

    申请号:US12436754

    申请日:2009-05-06

    IPC分类号: C30B11/00

    摘要: Disclosed are a single crystal wire and other single crystal articles, and a manufacturing method thereof. The method comprises the steps of: placing into a growth crucible at least one metal selected from the group consisting of gold, copper, silver, aluminum and nickel; heating and melting the metal placed in the growth crucible; growing a single crystal using metal crystal as a seed by Czochralski or Bridgman method; cutting the grown single crystal by electric discharge machining; and machining the cut single crystal and producing a wire or other articles such as a ring. In the method, the grown metal single crystal is cut into a disc-shaped piece by electric discharge machining. The piece is transformed into a single crystal wire or other articles by wire-cut electric discharge machining, and the single crystal wire can be used as a ring, a pendant, or a wire for high-quality cables for audio and video systems. Also, the single crystal formed into the disc-shaped piece by electric discharge machining can be used as a substrate and a target for deposition.

    摘要翻译: 公开了单晶线及其它单晶制品及其制造方法。 该方法包括以下步骤:将生长坩埚放入至少一种选自金,铜,银,铝和镍的金属; 加热和熔化置于生长坩埚中的金属; 使用Czochralski或Bridgman方法生长使用金属晶体作为种子的单晶; 通过放电加工切割生长的单晶; 并加工切割的单晶并生产线或其它物品如环。 在该方法中,通过放电加工将成长的金属单晶切割成圆盘状的片。 该片通过线切割放电加工转换为单晶线或其他物品,单晶线可用作音频和视频系统的高品质电缆的环形,吊坠或线材。 此外,通过放电加工形成为盘状片的单晶可以用作基板和沉积靶。

    Frequency synthesizer and frequency synthesizing method using optical injection locking
    4.
    发明授权
    Frequency synthesizer and frequency synthesizing method using optical injection locking 有权
    频率合成器和频率合成方法采用光学注入锁定

    公开(公告)号:US07953131B2

    公开(公告)日:2011-05-31

    申请号:US12421444

    申请日:2009-04-09

    IPC分类号: H01S3/10

    摘要: The present invention relates to an optical frequency synthesizer and an optical frequency synthesizing method using femtosecond laser optical injection locking, which inject a femtosecond laser optical frequency comb into a diode laser, thus obtaining single-mode laser light, phase-locked to only a single mode in the optical frequency comb, and which change the optical frequency and interval, that is, the repetition rate, of a femtosecond laser, together with the frequency of a semiconductor laser, thus scanning optical frequencies while realizing a single desired optical frequency. The optical frequency synthesizer using femtosecond laser optical injection locking, includes a mode-locked femtosecond laser (110), which is a master laser, and a diode laser (120), which is a slave laser and into which laser light emitted from the femtosecond laser is injected.

    摘要翻译: 本发明涉及一种使用飞秒激光光注入锁定的光频合成器和光频合成方法,其中将飞秒激光光频梳针注入二极管激光器,从而获得单模激光,仅锁定一个单模激光 模式,并且将飞秒激光的光频率和间隔,即重复频率与半导体激光器的频率一起改变,从而在实现单个期望的光频率的同时扫描光频率。 使用飞秒激光光注入锁定的光频合成器包括作为主激光器的锁模飞秒激光器(110)和作为从属激光器的二极管激光器(120),其中从飞秒发射的激光 激光被注射。

    BUMPER BEAM ASSEMBLY FOR VEHICLE
    5.
    发明申请
    BUMPER BEAM ASSEMBLY FOR VEHICLE 有权
    用于车辆的BUMPER BEAM ASSEMBLY FOR VEHICLE

    公开(公告)号:US20110285152A1

    公开(公告)日:2011-11-24

    申请号:US13114818

    申请日:2011-05-24

    IPC分类号: B60R19/02

    摘要: A bumper beam assembly for a vehicle may include a bumper beam having a horizontal support plate, front and rear vertical support plates attached to the horizontal support plate, wherein the rear vertical support plate includes an insertion hole, a partition formed along the horizontal support plate between the front and rear vertical support plates, and a stay, an end portion of which may be inserted into the insertion hole.

    摘要翻译: 用于车辆的保险杠梁组件可以包括具有水平支撑板的缓冲梁,附接到水平支撑板的前后垂直支撑板,其中后垂直支撑板包括插入孔,沿着水平支撑板形成的隔板 在前后垂直支撑板之间,并且其端部可以插入到插入孔中的撑杆。

    OPTICAL FREQUENCY SYNTHESIZER AND OPTICAL FREQUENCY SYNTHESIZING METHOD USING FEMTOSECOND LASER OPTICAL INJECTION LOCKING
    6.
    发明申请
    OPTICAL FREQUENCY SYNTHESIZER AND OPTICAL FREQUENCY SYNTHESIZING METHOD USING FEMTOSECOND LASER OPTICAL INJECTION LOCKING 有权
    光学合成器和光学频率合成方法使用FEMTOSECOND激光光学注入锁定

    公开(公告)号:US20090225795A1

    公开(公告)日:2009-09-10

    申请号:US12421444

    申请日:2009-04-09

    IPC分类号: H01S3/098 H01S3/10

    摘要: The present invention relates to an optical frequency synthesizer and an optical frequency synthesizing method using femtosecond laser optical injection locking, which inject a femtosecond laser optical frequency comb into a diode laser, thus obtaining single-mode laser light, phase-locked to only a single mode in the optical frequency comb, and which change the optical frequency and interval, that is, the repetition rate, of a femtosecond laser, together with the frequency of a semiconductor laser, thus scanning optical frequencies while realizing a single desired optical frequency. The optical frequency synthesizer using femtosecond laser optical injection locking, includes a mode-locked femtosecond laser (110), which is a master laser, and a diode laser (120), which is a slave laser and into which laser light emitted from the femtosecond laser is injected.

    摘要翻译: 本发明涉及一种使用飞秒激光光注入锁定的光频合成器和光频合成方法,其中将飞秒激光光频梳针注入二极管激光器,从而获得单模激光,仅锁定一个单模激光 模式,并且将飞秒激光的光频率和间隔,即重复频率与半导体激光器的频率一起改变,从而在实现单个期望的光频率的同时扫描光频率。 使用飞秒激光光注入锁定的光频合成器包括作为主激光器的锁模飞秒激光器(110)和作为从属激光器的二极管激光器(120),其中从飞秒发射的激光 激光被注射。

    METHOD OF MANUFACTURING SINGLE CRYSTAL WIRE
    7.
    发明申请
    METHOD OF MANUFACTURING SINGLE CRYSTAL WIRE 有权
    制造单晶线的方法

    公开(公告)号:US20090211516A1

    公开(公告)日:2009-08-27

    申请号:US12436754

    申请日:2009-05-06

    IPC分类号: C30B15/14

    摘要: Disclosed are a single crystal wire and a manufacturing method thereof. The method comprises the steps of: placing into a growth crucible at least one metal selected from the group consisting of gold, copper, silver, aluminum and nickel; heating and melting the metal placed in the growth crucible; growing a single crystal using the metal crystal as a seed by the Czochralski or Bridgman method; cutting the grown single crystal by electric discharge machining; and forming the cut single crystal into a wire. In the method, the grown metal single crystal is formed into a disc-shaped piece by electric discharge machining. The piece is formed into a single crystal wire by wire-cut electric discharge machining, and the single crystal wire can be used as a ring, a pendant or a wire within a high-quality cable making a connection in audio and video systems. Also, the single crystal formed into the disc-shaped piece by electric discharge machining can be used as a substrate and a target for deposition.

    摘要翻译: 公开了一种单晶线及其制造方法。 该方法包括以下步骤:将生长坩埚放入至少一种选自金,铜,银,铝和镍的金属; 加热和熔化置于生长坩埚中的金属; 使用Czochralski或Bridgman方法生长使用金属晶体作为种子的单晶; 通过放电加工切割生长的单晶; 并将切割的单晶形成线。 在该方法中,通过放电加工将生长的金属单晶形成为盘状片。 该片通过线切割放电加工形成单晶线,并且单晶线可以用作在音频和视频系统中连接的高质量电缆中的环,吊线或线。 此外,通过放电加工形成为盘状片的单晶可以用作基板和沉积靶。

    Para-chlorination of aromatic compound
    8.
    发明授权
    Para-chlorination of aromatic compound 失效
    芳香化合物的对氯

    公开(公告)号:US6028232A

    公开(公告)日:2000-02-22

    申请号:US860711

    申请日:1997-09-23

    CPC分类号: B01J29/60 C07B39/00 C07C17/12

    摘要: The present invention relates to a catalyst for preparing para-chloro aromatic compounds by the liquid-phase chlorination method. The catalyst is prepared by loading transition metal salts, rare earth metal salts or a mixture thereof, and alkali metal or alkaline earth metal chlorides having a melting point of 300.degree. C. or more, by solid-state method or impregnation method, into zeolite L being ion-exchanged by alkali metal. The present invention also relates to a process for preparing para-isomers of the chlorinated compounds by using the catalyst.

    摘要翻译: PCT No.PCT / KR96 / 00213 Sec。 371日期1997年9月23日 102(e)1997年9月23日PCT PCT 1996年11月23日PCT公布。 第WO97 / 18893号公报 日期:1997年5月29日本发明涉及通过液相氯化法制备对氯芳族化合物的催化剂。 通过将过渡金属盐,稀土金属盐或其混合物和熔点为300℃以上的碱金属或碱土金属氯化物通过固相法或浸渍法加入到沸石中制备催化剂 L被碱金属离子交换。 本发明还涉及通过使用催化剂制备氯代化合物的对位异构体的方法。

    Bumper beam assembly for vehicle
    9.
    发明授权
    Bumper beam assembly for vehicle 有权
    用于车辆的保险杠梁总成

    公开(公告)号:US08336934B2

    公开(公告)日:2012-12-25

    申请号:US13114818

    申请日:2011-05-24

    IPC分类号: B60R19/24

    摘要: A bumper beam assembly for a vehicle may include a bumper beam having a horizontal support plate, front and rear vertical support plates attached to the horizontal support plate, wherein the rear vertical support plate includes an insertion hole, a partition formed along the horizontal support plate between the front and rear vertical support plates, and a stay, an end portion of which may be inserted into the insertion hole.

    摘要翻译: 用于车辆的保险杠梁组件可以包括具有水平支撑板的缓冲梁,附接到水平支撑板的前后垂直支撑板,其中后垂直支撑板包括插入孔,沿着水平支撑板形成的隔板 在前后垂直支撑板之间,并且其端部可以插入到插入孔中的撑杆。

    Single crystal wire and manufacturing method of the same
    10.
    发明申请
    Single crystal wire and manufacturing method of the same 审中-公开
    单晶线及其制造方法相同

    公开(公告)号:US20070169857A1

    公开(公告)日:2007-07-26

    申请号:US11726272

    申请日:2007-03-21

    IPC分类号: C22F1/00

    摘要: Disclosed are a single crystal wire and a manufacturing method thereof. The method comprises the steps of: placing into a growth crucible at least one metal selected from the group consisting of gold, copper, silver, aluminum and nickel; heating and melting the metal placed in the growth crucible; growing a single crystal using the metal crystal as a seed by the Czochralski or Bridgmari method; cutting the grown single crystal by electric discharge machining; and forming the cut single crystal into a wire. In the method, the grown metal single crystal is formed into a disc-shaped piece by electric discharge machining. The piece is formed into a single crystal wire by wire-cut electric discharge machining, and the single crystal wire can be used as a ring, a pendant or a wire within a high-quality cable making a connection in audio and video systems. Also, the single crystal formed into the disc-shaped piece by electric discharge machining can be used as a substrate and a target for deposition.

    摘要翻译: 公开了一种单晶线及其制造方法。 该方法包括以下步骤:将生长坩埚放入至少一种选自金,铜,银,铝和镍的金属; 加热和熔化置于生长坩埚中的金属; 使用Czochralski或Bridgmari方法生长使用金属晶体作为种子的单晶; 通过放电加工切割生长的单晶; 并将切割的单晶形成线。 在该方法中,通过放电加工将生长的金属单晶形成为盘状片。 该片通过线切割放电加工形成单晶线,并且单晶线可以用作在音频和视频系统中连接的高质量电缆中的环,吊线或线。 此外,通过放电加工形成为盘状片的单晶可以用作基板和沉积靶。