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    Elastomeric compounds incorporating metal-treated carbon blacks
    1.
    发明授权
    Elastomeric compounds incorporating metal-treated carbon blacks 失效
    掺入金属处理炭黑的弹性体化合物

    公开(公告)号：US06150453A

    公开(公告)日：2000-11-21

    申请号：US49568

    申请日：1998-03-27

    申请人： Khaled Mahmud ,  Meng-Jiao Wang ,  Yakov Evgenjevich Kutsovsky

    发明人： Khaled Mahmud ,  Meng-Jiao Wang ,  Yakov Evgenjevich Kutsovsky

    IPC分类号： C08L21/00 ,  C08K3/00 ,  C08K3/04 ,  C08K3/22 ,  C08K9/02 ,  C08K9/06 ,  C08L101/00 ,  C09C1/56 ,  C09C1/58

    CPC分类号： C09C1/58 ,  C08K9/02 ,  C01P2006/12 ,  C01P2006/19

    摘要： Disclosed are elastomeric compounds including an elastomer and an aggregate comprising a carbon phase and a metal-containing species phase, optionally including a coupling agent. Also disclosed is an aggregate comprising a carbon phase and a metal-containing species phase. A variety of elastomers and formulations employing such elastomers are contemplated and disclosed. Elastomeric compounds incorporating an elastomer and the aggregate are also disclosed. Also disclosed are methods for preparing elastomers compounded with the aggregate, and methods of improving various properties of elastomeric compounds, such as abrasion resistance, hysteresis, wet skid resistance, and/or wet traction.

    摘要翻译： 公开了包括弹性体和包含碳相和含金属物质相的骨料的弹性体化合物，任选地包括偶联剂。 还公开了包含碳相和含金属物质相的骨料。 考虑和公开了使用这种弹性体的各种弹性体和制剂。 还公开了包含弹性体和聚集体的弹性体化合物。 还公开了用于制备与骨料混合的弹性体的方法，以及改善弹性体化合物的各种性能的方法，例如耐磨性，滞后性，抗湿滑性和/或湿牵引力。

    Elastomeric compounds incorporating silicon-treated carbon blacks
    2.
    发明授权
    Elastomeric compounds incorporating silicon-treated carbon blacks 有权
    掺入硅处理炭黑的弹性体化合物

    公开(公告)号：US06448309B2

    公开(公告)日：2002-09-10

    申请号：US09813439

    申请日：2001-03-21

    申请人： Khaled Mahmud ,  Meng-Jiao Wang ,  Robert A. Francis ,  James A. Belmont

    发明人： Khaled Mahmud ,  Meng-Jiao Wang ,  Robert A. Francis ,  James A. Belmont

    IPC分类号： C08K324

    CPC分类号： C08K5/5406 ,  C01P2002/88 ,  C01P2004/04 ,  C01P2006/12 ,  C01P2006/19 ,  C08K9/06 ,  C09C1/50 ,  C09C1/56 ,  C09C1/565 ,  C08L21/00

    摘要： Disclosed are elastomeric compounds including an elastomer and a silicon-treated carbon black, and optionally including a coupling agent. The elastomeric compound exhibits poorer abrasion resistance in the absence of a coupling agent, lower hysteresis at high temperature and comparable or increased hysteresis at low temperature compared to an elastomer containing an untreated carbon black. A variety of elastomers and formulations employing such elastomers are contemplated and disclosed. Elastomeric compounds incorporating an elastomer and an oxidized, silicon-treated carbon black are also disclosed. Also disclosed are methods for preparing elastomers compounded with the treated carbon black.

    摘要翻译： 公开了包括弹性体和经硅处理的炭黑的弹性体化合物，并且任选地包括偶联剂。 弹性体组合物在不含偶联剂的情况下表现出较差的耐磨性，与含有未处理的炭黑的弹性体相比，在高温下具有较低的滞后和在低温下可比或增加的滞后。 考虑并公开了使用这种弹性体的各种弹性体和制剂。 还公开了掺入弹性体和氧化的，硅处理的炭黑的弹性体化合物。 还公开了制备与处理过的炭黑混合的弹性体的方法。

    Method of making a multi-phase aggregate using a multi-stage process
    3.
    发明授权
    Method of making a multi-phase aggregate using a multi-stage process 失效
    使用多级方法制造多相聚集体的方法

    公开(公告)号：US5904762A

    公开(公告)日：1999-05-18

    申请号：US837493

    申请日：1997-04-18

    申请人： Khaled Mahmud ,  Meng-Jiao Wang

    发明人： Khaled Mahmud ,  Meng-Jiao Wang

    IPC分类号： C08K3/34 ,  C08K3/00 ,  C08K3/04 ,  C08K9/06 ,  C08L21/00 ,  C09C1/50 ,  C09C1/56 ,  C09C3/12 ,  C09C1/44

    CPC分类号： C09C1/56 ,  C08K3/04 ,  C08K9/06 ,  C09C1/50 ,  C01P2004/50 ,  C01P2006/12

    摘要： A method of making an aggregate comprising at least a carbon phase and a silicon-containing species phase is disclosed. The method involves introducing a first feedstock into a first stage of a multi-stage reactor, and introducing a second feedstock into the reactor at a location downstream of the first stage. The first and second feedstock comprise a carbon black-yielding feedstock, and at least one feedstock also comprises a silicon-containing compound. The reactor is operated at a sufficient temperature to decompose the silicon-containing compound and to pyrolize the carbon black-yielding feedstock. An additional method is disclosed which involves making an aggregate comprising a carbon phase and a silicon-containing species phase using multi-stage reactor having at least three stages for introducing a feedstock, wherein at least one of the feedstocks comprises a carbon black-yielding feedstock and wherein at least one of the feedstock comprises a silicon-containing compound. Besides producing the aggregate comprising a carbon phase and a silicon-containing species phase, silica and/or carbon black may also result from the processes of the present invention. A further method is disclosed which involves making an aggregate comprising a carbon phase and a metal-containing species phase using a multi-stage reactor having at least two stages for introducing feedstocks, wherein at least one of the feedstocks comprises a carbon black-yielding feedstock and where at least one of the feedstocks comprises a metal-containing compound. The aggregates of the present invention when incorporated into elastomeric compositions preferably lead to improved wet skid resistance properties.

    摘要翻译： 公开了一种制备包含至少一个碳相和含硅物质相的聚集体的方法。 该方法包括将第一原料引入多级反应器的第一级，并且在第一级下游的位置将第二原料引入反应器。 第一和第二原料包括产生炭黑的原料，并且至少一种原料还包含含硅化合物。 反应器在足够的温度下运行以分解含硅化合物并且对产生炭黑的原料进行热解。 公开了一种额外的方法，其涉及使用具有至少三个阶段的多级反应器制备包含碳相和含硅物质相的聚集体，用于引入原料，其中至少一种原料包含产生炭黑的原料 并且其中所述原料中的至少一种包含含硅化合物。 除了生产包含碳相和含硅物质相的骨料外，二氧化硅和/或炭黑也可以由本发明的方法产生。 公开了一种另外的方法，其涉及使用具有至少两个阶段的多级反应器来制备包含碳相和含金属物质相的聚集体以引入原料，其中至少一种原料包含产生炭黑的原料 并且其中至少一种原料包含含金属的化合物。 当结合到弹性体组合物中时，本发明的聚集体优选地导致改进的抗湿滑性能。

    Method of making a multi-phase aggregate using a multi-stage process
    5.
    发明授权
    Method of making a multi-phase aggregate using a multi-stage process 失效
    使用多级方法制造多相聚集体的方法

    公开(公告)号：US06709506B2

    公开(公告)日：2004-03-23

    申请号：US09975699

    申请日：2001-10-11

    申请人： Khaled Mahmud ,  Meng-Jiao Wang ,  Yakov Kutsovsky

    发明人： Khaled Mahmud ,  Meng-Jiao Wang ,  Yakov Kutsovsky

    IPC分类号： C08K902

    CPC分类号： C09C1/56 ,  C01P2004/50 ,  C01P2006/12 ,  C08K3/04 ,  C08K9/06 ,  C09C1/50 ,  Y02T10/862 ,  C08L21/00

    摘要： An aggregate including a carbon phase and a silicon-containing species phase is described, wherein a difference between BET (N2) surface area and t-area of the aggregate is from about 2 to 10 m2/g; a difference between BET (N2) surface area and t-area of from about 1 to 50 m2/after HF treatment; a ratio of from about 0.1 to 10; a weight average aggregate size measured by DCP after HF treatment that is reduced by about 5% to 40%; a silica ash content in the aggregate of from about 0.05% to 1% based on the weight of the aggregate after HF treatment and based on ash resulting from silicon-containing compound; and a BET surface area of silica ash in the aggregate of from about 200 m2/g to 700 m2/g, wherein the silicon-containing species phase is present primarily at the surface of the aggregate.

    摘要翻译： 描述了包含碳相和含硅物质相的聚集体，其中BET（N2）表面积和聚集体的t面积之间的差为约2至10m 2 / g; HF处理后的BET（N2）表面积和t-面积之间的差异为约1〜50m 2 / 约0.1至10的比率; 通过HF处理后的DCP测量的重量平均聚集体尺寸减少约5％至40％; 基于HF处理后的骨料的重量和基于由含硅化合物产生的灰分，总灰分中的二氧化硅灰分含量为约0.05％至1％ 和聚集体中二氧化硅灰分的BET表面积为约200m 2 / g至700m 2 / g，其中含硅物质相主要存在于聚集体的表面。

    Method of making a multi-phase aggregate using a multi-stage process
    6.
    发明授权
    Method of making a multi-phase aggregate using a multi-stage process 有权
    使用多级方法制造多相聚集体的方法

    公开(公告)号：US06686409B2

    公开(公告)日：2004-02-03

    申请号：US09927222

    申请日：2001-08-10

    申请人： Khaled Mahmud ,  Meng-Jiao Wang ,  Yakov Kutsovsky

    发明人： Khaled Mahmud ,  Meng-Jiao Wang ,  Yakov Kutsovsky

    IPC分类号： C08U900

    CPC分类号： C09C1/56 ,  C01P2004/50 ,  C01P2006/12 ,  C08K3/04 ,  C08K9/06 ,  C09C1/50 ,  Y02T10/862 ,  C08L21/00

    摘要： A method of making an aggregate having a carbon phase and a silicon-containing species phase is described and includes introducing a carbon black-yielding feedstock and a silicon-containing compound feedstock into different stages of a multi-stage reactor. The reactor operates at a sufficient temperature to decompose the silicon-containing compound and to form a carbon black phase from the carbon black-yielding feedstock. At least one of the feedstocks may include a diluent, such as an alcohol, water, and aqueous based solution, and mixtures thereof.

    摘要翻译： 描述了制备具有碳相和含硅物质相的骨料的方法，并且包括将产生炭黑的原料和含硅化合物原料引入多级反应器的不同阶段。 反应器在足够的温度下操作以分解含硅化合物并从产生炭黑的原料形成炭黑相。 至少一种原料可以包括稀释剂，例如醇，水和基于水的溶液，以及它们的混合物。

    Method of making a multi-phase aggregate using a multi-stage process
    7.
    发明授权
    Method of making a multi-phase aggregate using a multi-stage process 有权
    使用多级方法制造多相聚集体的方法

    公开(公告)号：US06211279B1

    公开(公告)日：2001-04-03

    申请号：US09375044

    申请日：1999-08-16

    申请人： Khaled Mahmud ,  Meng-Jiao Wang

    发明人： Khaled Mahmud ,  Meng-Jiao Wang

    IPC分类号： C08K300

    CPC分类号： C09C1/56 ,  C01P2004/50 ,  C01P2006/12 ,  C08K3/04 ,  C08K9/06 ,  C09C1/50 ,  Y02T10/862 ,  C08L21/00

    摘要： Elastomeric compositions are described and include at least one elastomer and an aggregate having a carbon phase and a silicon-containing species phase. The aggregate exhibits one or more specific characteristics. Methods of improving the rolling resistance of an elastomeric composition are also described and include introducing the aggregate into an elastomeric composition.

    摘要翻译： 描述弹性组合物，并且包括至少一种弹性体和具有碳相和含硅物质相的骨料。 聚集体具有一个或多个特定特征。 还描述了改善弹性体组合物的滚动阻力的方法，并且包括将聚集体引入弹性体组合物中。

    Method of making a multi-phase aggregate using a multi-stage process
    8.
    发明授权
    Method of making a multi-phase aggregate using a multi-stage process 失效
    使用多级方法制造多相聚集体的方法

    公开(公告)号：US6057387A

    公开(公告)日：2000-05-02

    申请号：US61871

    申请日：1998-04-17

    申请人： Khaled Mahmud ,  Meng-Jiao Wang

    发明人： Khaled Mahmud ,  Meng-Jiao Wang

    IPC分类号： C08K3/34 ,  C08K3/00 ,  C08K3/04 ,  C08K9/06 ,  C08L21/00 ,  C09C1/50 ,  C09C1/56 ,  C09C3/12 ,  C08K9/02 ,  C08K3/18

    CPC分类号： C09C1/56 ,  C08K3/04 ,  C08K9/06 ,  C09C1/50 ,  C01P2004/50 ,  C01P2006/12

    摘要： A method of making an aggregate comprising at least a carbon phase and a silicon-containing species phase is disclosed. The method involves introducing a first feedstock into a first stage of a multi-stage reactor, and introducing a second feedstock into the reactor at a location downstream of the first stage. The first and second feedstock comprise a carbon black-yielding feedstock, and at least one feedstock also comprises a silicon-containing compound. The reactor is operated at a sufficient temperature to decompose the silicon-containing compound and to pyrolize the carbon black-yielding feedstock. An additional method is disclosed which involves making an aggregate comprising a carbon phase and a silicon-containing species phase using multi-stage reactor having at least the stages for introducing a feedstock, wherein at least one of the feedstocks comprises a carbon black-yielding feedstock and wherein at least one of the feedstock comprises a silicon-containing compound. Besides producing the aggregate comprising a carbon phase and a silicon-containing species phase, silica and/or carbon black may also result from the processes of the present invention. A further method is disclosed which involves making an aggregate comprising a carbon phase and a metal-containing species phase using a multi-stage reactor having at least two stages for introducing feedstocks, wherein at least one of the feedstocks comprises a carbon black-yielding feedstock and where at least one of the feedstocks comprises a metal-containing compound. The aggregates of the present invention when incorporated into elastomeric compositions preferably lead to improved wet skid resistance properties.

    摘要翻译： 公开了一种制备包含至少一个碳相和含硅物质相的聚集体的方法。 该方法包括将第一原料引入多级反应器的第一级，并且在第一级下游的位置将第二原料引入反应器。 第一和第二原料包括产生炭黑的原料，并且至少一种原料还包含含硅化合物。 反应器在足够的温度下运行以分解含硅化合物并且对产生炭黑的原料进行热解。 公开了一种额外的方法，其涉及使用至少具有用于引入原料的阶段的多级反应器制备包含碳相和含硅物质相的骨料，其中至少一种原料包含产生炭黑的原料 并且其中所述原料中的至少一种包含含硅化合物。 除了生产包含碳相和含硅物质相的骨料外，二氧化硅和/或炭黑也可以由本发明的方法产生。 公开了一种另外的方法，其涉及使用具有至少两个阶段的多级反应器来制备包含碳相和含金属物质相的聚集体以引入原料，其中至少一种原料包含产生炭黑的原料 并且其中至少一种原料包含含金属的化合物。 当结合到弹性体组合物中时，本发明的聚集体优选地导致改进的抗湿滑性能。

    Elastomeric compounds incorporating silicon-treated carbon blacks
    9.
    发明授权
    Elastomeric compounds incorporating silicon-treated carbon blacks 有权
    掺入硅处理炭黑的弹性体化合物

    公开(公告)号：US07199176B2

    公开(公告)日：2007-04-03

    申请号：US10192403

    申请日：2002-07-10

    申请人： Khaled Mahmud ,  Meng-Jiao Wang ,  Robert A. Francis ,  James A. Belmont

    发明人： Khaled Mahmud ,  Meng-Jiao Wang ,  Robert A. Francis ,  James A. Belmont

    IPC分类号： C08K3/04

    CPC分类号： C08K5/5406 ,  C01P2002/88 ,  C01P2004/04 ,  C01P2006/12 ,  C01P2006/19 ,  C08K9/06 ,  C09C1/50 ,  C09C1/56 ,  C09C1/565 ,  C08L21/00

    摘要： Disclosed are elastomeric compounds including an elastomer and a silicon-treated carbon black, and optionally including a coupling agent. The elastomeric compound exhibits poorer abrasion resistance in the absence of a coupling agent, lower hysteresis at high temperature and comparable or increased hysteresis at low temperature compared to an elastomer containing an untreated carbon black. A variety of elastomers and formulations employing such elastomers are contemplated and disclosed. Elastomeric compounds incorporating an elastomer and an oxidized, silicon-treated carbon black are also disclosed. Also disclosed are methods for preparing elastomers compounded with the treated carbon black.

    摘要翻译： 公开了包括弹性体和经硅处理的炭黑的弹性体化合物，并且任选地包括偶联剂。 弹性体组合物在不含偶联剂的情况下表现出较差的耐磨性，与含有未处理的炭黑的弹性体相比，在高温下具有较低的滞后和在低温下可比或增加的滞后。 考虑并公开了使用这种弹性体的各种弹性体和制剂。 还公开了掺入弹性体和氧化的，硅处理的炭黑的弹性体化合物。 还公开了制备与处理过的炭黑混合的弹性体的方法。