公开(公告)号：US11661478B2

公开(公告)日：2023-05-30

申请号：US16489931

申请日：2018-02-06

Applicant: SHOWA DENKO K.K.

Inventor： Takuya Minami ,  Yoshishige Okuno ,  Yuta Yamaguchi ,  Ryuuta Miyasaka ,  Naoya Fukumoto ,  Hiroko Hattori ,  Hiroyuki Tomita ,  Michio Seri ,  Naoko Ito ,  Ichiro Ota ,  Katsumi Murofushi

IPC: C08G65/331 ,  C08G65/333 ,  C10M107/38 ,  G11B5/725 ,  C10N40/18

CPC classification number: C08G65/331 ,  C08G65/333 ,  C10M107/38 ,  G11B5/7257 ,  C10N2040/18

Abstract: A fluorine-containing ether compound of the present invention is represented by the following General Formula (1). (In the General Formula (1), X is a trivalent atom or a trivalent atom group, A is a linking group including at least one polar group, B is a linking group having a perfluoropolyether chain, and D is a polar group or a substituent having a polar group at the end.)

[Chem. 1]

XA-B-D)3  (1)

公开(公告)号：US11279664B2

公开(公告)日：2022-03-22

申请号：US16082349

申请日：2017-01-30

Applicant: SHOWA DENKO K.K.

Inventor： Daisuke Yagyu ,  Yuta Yamaguchi ,  Naoya Fukumoto ,  Tsuyoshi Kato ,  Shoko Uetake ,  Hiroyuki Tomita ,  Ryuuta Miyasaka ,  Naoko Ito ,  Ichiro Ota ,  Katsumi Murofushi

IPC: C07C43/23 ,  C10M105/54 ,  G11B5/725 ,  C10M107/38 ,  C07C43/178 ,  C07D277/24 ,  C07D303/26 ,  C07D333/16 ,  C07D409/12 ,  G11B5/733 ,  C10N30/06 ,  C10N40/18 ,  C10N50/00

Abstract: The present invention relates to a fluorine-containing ether compound represented by Formula (1), R1—R2—CH2—R3—CH2—R4  (1). (In Formula (1), R1 is an end group including an organic group having at least one double bond or triple bond, R2 is a divalent linking group bonded to R1 by etheric oxygen, R3 is a perfluoropolyether chain, R4 is an end group having two or three polar groups with each polar group being bonded to different carbon atoms, and the carbon atoms, to which the polar groups are bonded, being bonded to each other via a linking group including carbon atoms to which the polar groups are not bonded.)

公开(公告)号：US09646643B2

公开(公告)日：2017-05-09

申请号：US14171937

申请日：2014-02-04

Applicant: SHOWA DENKO K.K.

Inventor： Ichiro Ota

IPC: G11B5/84 ,  H01F41/30

CPC classification number: G11B5/8408 ,  H01F41/308

Abstract: A method of fabricating a magnetic recording medium sequentially forms a magnetic recording layer, a protection layer, and a lubricant layer on a stacked body. The lubricant layer is formed on a surface of the protection layer by vapor-phase lubrication without exposing the stacked body to atmosphere after forming the protection layer on the stacked body. Nitrogen atoms or oxygen atoms are injected onto the surface of the protection layer after forming the protection layer and before forming the lubricant layer.

公开(公告)号：US11292979B2

公开(公告)日：2022-04-05

申请号：US15999837

申请日：2017-02-20

Applicant: SHOWA DENKO K.K.

Inventor： Yuta Yamaguchi ,  Naoya Fukumoto ,  Naoko Ito ,  Hiroyuki Tomita ,  Ichiro Ota ,  Katsumi Murofushi

IPC: C10M105/54 ,  C07C43/13 ,  G11B5/725 ,  C10N40/18

Abstract: A fluorine-containing ether compound represented by a formula (1) shown below. R4—CH2—R3—CH2—R2—CH2—R1—CH2—R2—CH2—R3—CH2—R5  (1) In formula (1), R1 and R3 represent the same or different perfluoropolyether chains, R2 represents a linking group containing at least one polar group, one or both of R4 and R5 represent a terminal group containing two or more polar groups, and R4 and R5 are different.

公开(公告)号：US10134435B2

公开(公告)日：2018-11-20

申请号：US14575385

申请日：2014-12-18

Applicant: SHOWA DENKO K.K.

Inventor： Ichiro Ota

IPC: C23C16/26 ,  G11B5/84 ,  C23C14/06 ,  C23C14/22 ,  C23C16/27 ,  H01J37/32

Abstract: A carbon film forming method, that introduces a raw material gas including carbon into a film forming chamber, ionizes the gas by using an ion source, accelerates the ionized gas, and radiates the ionized gas to a surface of a substrate to form a carbon film on the surface of the substrate, includes forming the carbon film while rotating a first magnet, which is provided on the opposite side of the substrate across a region in which the raw material gas is ionized so as to be eccentric and/or inclined with respect to a central axis connecting the center of the ion source and a position corresponding to the center of the substrate held by the holder, in a circumferential direction.

公开(公告)号：US11514945B2

公开(公告)日：2022-11-29

申请号：US16489919

申请日：2018-02-20

Applicant: SHOWA DENKO K.K.

Inventor： Hiroyuki Tomita ,  Hiroko Hattori ,  Naoya Fukumoto ,  Ryuuta Miyasaka ,  Naoko Ito ,  Ichiro Ota ,  Katsumi Murofushi

IPC: G11B5/84 ,  G11B5/72 ,  C08G65/332 ,  C08G65/333 ,  C10M107/38 ,  G11B5/725

Abstract: A lubricant for a magnetic recording medium capable of forming a lubricant layer having excellent adhesion to a protective layer is provided. A lubricant for a magnetic recording medium contains a fluorine-containing ether compound in which a group having an ethylenic carbon-carbon double bond is disposed at one or both terminals of a perfluoroalkyl polyether chain. It is preferable that the group having the ethylenic carbon-carbon double bond is disposed at one terminal of the perfluoroalkyl polyether chain, and a hydroxyl group is disposed at other terminal. It is preferable that the lubricant for a magnetic recording medium contains a compound in which one or more functional groups selected from a hydroxyl group, an amino group, an amido group and a carboxyl group is disposed at one or both terminals of a perfluoroalkyl polyether chain.

公开(公告)号：US20140079877A1

公开(公告)日：2014-03-20

申请号：US14017387

申请日：2013-09-04

Applicant: SHOWA DENKO K.K.

Inventor： Yasuyuki Tsutatani ,  Daisuke Shiomi ,  Satoru Ueno ,  Ichiro Ota ,  Takehiko Okabe

IPC: G11B5/85

CPC classification number: G11B5/85 ,  C23C14/564 ,  G11B5/8408

Abstract: A method of fabricating a magnetic recording medium sequentially forms a magnetic recording layer, a protection layer, and a lubricant layer on a stacked body. The lubricant layer is formed by vapor-phase lubrication without exposing the stacked body to atmosphere after forming the protection layer on the stacked body. A region having a gas pressure P3 is provided in a transport path of the stacked body after the formation of the protection layer and before the formation of the lubricant layer, satisfying relationships P3>P1 and P3>P2, where P1 denotes a process gas pressure at a time of forming the protection layer, and P2 denotes a process gas pressure at a time of forming the lubricant layer.

Abstract translation: 制造磁记录介质的方法在层叠体上依次形成磁记录层，保护层和润滑层。 通过气相润滑形成润滑剂层，而不在层叠体上形成保护层后将层叠体暴露在大气中。 具有气体压力P3的区域在形成保护层之后并在形成润滑剂层之前设置在堆叠体的输送路径中，满足关系P3> P1和P3> P2，其中P1表示处理气体压力 在形成保护层时，P2表示形成润滑剂层时的工艺气体压力。