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11.发明申请Silicon composite, making method, and non-aqueous electrolyte secondary cell negative electrode material 审中-公开硅复合材料，制造方法和非水电解质二次电池负极材料公开(公告)号：US20060003227A1
公开(公告)日：2006-01-05
申请号：US11166173
申请日：2005-06-27
CPC分类号： H01M4/366 , H01M4/0421 , H01M4/13 , H01M4/134 , H01M4/139 , H01M4/38 , H01M4/386 , H01M4/58 , H01M10/052 , H01M10/44 , H01M2004/027 , Y02E60/122 , Y02P70/54 , Y10T428/2993
摘要： A silicon composite comprises silicon particles whose surface is at least partially coated with a silicon carbide layer. It is prepared by subjecting a silicon powder to thermal CVD with an organic hydrocarbon gas and/or vapor at 900-1,400° C., and heating the powder for removing an excess free carbon layer from the surface through oxidative decomposition.
摘要翻译： 硅复合物包括其表面至少部分地涂覆有碳化硅层的硅颗粒。 通过在900-1,400℃下用有机烃气体和/或蒸气对硅粉进行热CVD，并通过氧化分解从表面加热除去过量游离碳层的粉末。
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公开(公告)号：US20070254102A1
公开(公告)日：2007-11-01
申请号：US11790234
申请日：2007-04-24
申请人： Hirofumi Fukuoka , Mikio Aramata , Satoru Miyawaki
发明人： Hirofumi Fukuoka , Mikio Aramata , Satoru Miyawaki
IPC分类号： C23C14/10
CPC分类号： C23C14/10 , C01B33/113 , H01M4/131 , H01M4/485 , H01M10/052
摘要： A method for producing a SiOx (x
摘要翻译： 提供了一种制备SiO x（x <1）的方法。 所生产的SiO x x适于用作生产具有大容量的锂离子二次电池的负极材料，该锂离子二次电池在重复使用的循环中不会经历劣化，并且在初始时具有低的不可逆容量 充放电。 制备SiO x（x <1）的方法包括以下步骤：在产生氧化硅气体的原料中加热至1,100至1,600℃范围内的温度， 惰性气体或减压下产生氧化硅气体，同时在惰性气体存在或减压下将金属硅加热至1800至2400℃的温度，以产生硅气体， 并且在衬底的表面上沉淀氧化硅气体和金属硅气体的气体混合物。
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13.发明申请SiCO-Li COMPOSITE, MAKING METHOD, AND NON-AQUEOUS ELECTROLYTE SECONDARY CELL NEGATIVE ELECTRODE MATERIAL 审中-公开SiCO-Li复合材料，制备方法和非水电解质二次电池负极电极材料公开(公告)号：US20070224509A1
公开(公告)日：2007-09-27
申请号：US11689671
申请日：2007-03-22
CPC分类号： H01M4/1391 , H01M4/0471 , H01M4/131 , H01M4/136 , H01M4/485 , H01M2004/027
摘要： A SiCO—Li composite is prepared by causing a reactive silane and/or siloxane having crosslinkable groups to crosslink, sintering the crosslinked product into an inorganic Si—C—O composite, and doping the Si—C—O composite with lithium. When the SiCO—Li composite is used as a negative electrode, a lithium ion secondary cell exhibits good cycle performance, unique discharge characteristics and improved initial efficiency.
摘要翻译： 通过使具有可交联基团的反应性硅烷和/或硅氧烷交联，将交联产物烧结成无机Si-C-O复合物，并用锂掺杂Si-C-O复合物来制备SiCO-Li复合材料。 当使用SiCO-Li复合物作为负极时，锂离子二次电池表现出良好的循环性能，独特的放电特性和初始效率的提高。
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14.发明申请Non-aqueous electrolyte secondary cell negative electrode material and metallic silicon power therefor 审中-公开非水电解质二次电池负极材料和金属硅电力公开(公告)号：US20060051670A1
公开(公告)日：2006-03-09
申请号：US11213744
申请日：2005-08-30
申请人： Mikio Aramata , Satoru Miyawaki , Hirofumi Fukuoka
发明人： Mikio Aramata , Satoru Miyawaki , Hirofumi Fukuoka
CPC分类号： H01M4/38 , C01B33/023 , H01M4/625 , H01M2004/021 , Y10T428/2993
摘要： A metallic silicon powder is prepared by effecting chemical reduction on silica stone, metallurgical refinement, and metallurgical and/or chemical purification to reduce the content of impurities. The powder is best suited as a negative electrode material for non-aqueous electrolyte secondary cells, affording better cycle performance.
摘要翻译： 通过在石英石上进行化学还原，冶金精炼和冶金和/或化学纯化来制备金属硅粉，以减少杂质含量。 该粉末最适合作为非水电解质二次电池的负极材料，提供更好的循环性能。
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15.发明申请公开(公告)号：US20050031958A1
公开(公告)日：2005-02-10
申请号：US10910317
申请日：2004-08-04
申请人： Hirofumi Fukuoka , Mikio Aramata , Kazuma Momii , Satoru Miyawaki
发明人： Hirofumi Fukuoka , Mikio Aramata , Kazuma Momii , Satoru Miyawaki
IPC分类号： C01B33/02 , B05D5/12 , H01M4/00 , H01M4/02 , H01M4/04 , H01M4/36 , H01M4/38 , H01M4/587 , H01M4/62 , H01M4/58
CPC分类号： H01M10/0525 , H01M4/0471 , H01M4/366 , H01M4/386 , H01M4/625
摘要： A metallic silicon-containing composite in which metallic silicon nuclei are coated with an inert material which does not contribute to adsorption and desorption of lithium ions is a useful negative electrode material for lithium ion secondary batteries. Using the composite as a negative electrode active material, a lithium ion secondary battery having a high capacity and excellent cycle performance can be fabricated.
摘要翻译： 一种金属硅复合物，其中金属硅核被不利于锂离子的吸附和解吸的惰性材料涂覆，是用于锂离子二次电池的有用的负极材料。 使用复合物作为负极活性物质，可以制造具有高容量和优异的循环性能的锂离子二次电池。
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16.发明申请SILICON COMPOSITE, MAKING METHOD, AND NON-AQUEOUS ELECTROLYTE SECONDARY CELL NEGATIVE ELECTRODE MATERIAL 审中-公开硅复合材料，制造方法和非水电解质二次电池负极电极材料公开(公告)号：US20110001097A1
公开(公告)日：2011-01-06
申请号：US12883558
申请日：2010-09-16
CPC分类号： H01M4/366 , H01M4/0421 , H01M4/13 , H01M4/134 , H01M4/139 , H01M4/38 , H01M4/386 , H01M4/58 , H01M10/052 , H01M10/44 , H01M2004/027 , Y02E60/122 , Y02P70/54 , Y10T428/2993
摘要： A silicon composite comprises silicon particles whose surface is at least partially coated with a silicon carbide layer. It is prepared by subjecting a silicon powder to thermal CVD with an organic hydrocarbon gas and/or vapor at 900-1,400° C., and heating the powder for removing an excess free carbon layer from the surface through oxidative decomposition.
摘要翻译： 硅复合物包括其表面至少部分地涂覆有碳化硅层的硅颗粒。 通过在900-1,400℃下用有机烃气体和/或蒸气对硅粉进行热CVD，并通过氧化分解从表面加热除去过量游离碳层的粉末。
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17.发明申请公开(公告)号：US20050214644A1
公开(公告)日：2005-09-29
申请号：US11085518
申请日：2005-03-22
IPC分类号： C01B21/068 , C01B31/36 , C01B33/00 , C01B33/12 , H01B1/04 , H01B1/12 , H01M4/02 , H01M4/13 , H01M4/131 , H01M4/133 , H01M4/136 , H01M4/139 , H01M4/36 , H01M4/38 , H01M4/48 , H01M4/485 , H01M4/58 , H01M4/587 , H01M4/60 , H01M4/62 , H01M10/0525 , H01M10/36
CPC分类号： H01B1/122 , H01M4/0471 , H01M4/13 , H01M4/131 , H01M4/133 , H01M4/136 , H01M4/139 , H01M4/364 , H01M4/386 , H01M4/485 , H01M4/58 , H01M4/587 , H01M4/60 , H01M10/0525 , H01M2004/021 , H01M2004/027
摘要： Silicon composite particles are prepared by sintering primary fine particles of silicon, silicon alloy or silicon oxide together with an organosilicon compound. Sintering of the organosilicon compound results in a silicon-base inorganic compound which serves as a binder. Each particle has the structure that silicon or silicon alloy fine particles are dispersed in the silicon-base inorganic compound binder, and voids are present within the particle.
摘要翻译： 通过将硅，硅合金或氧化硅的一次微粒与有机硅化合物一起烧结来制备硅复合颗粒。 有机硅化合物的烧结产生作为粘合剂的硅基无机化合物。 每个颗粒具有将硅或硅合金细颗粒分散在硅基无机化合物粘合剂中的结构，并且在颗粒内存在空隙。
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公开(公告)号：US06787189B2
公开(公告)日：2004-09-07
申请号：US10307924
申请日：2002-12-03
申请人： Hidetaka Konno , Mikio Aramata , Hirofumi Fukuoka
发明人： Hidetaka Konno , Mikio Aramata , Hirofumi Fukuoka
IPC分类号： B05D302
CPC分类号： H01M4/583 , C01B32/20 , C04B35/5603 , C04B35/565 , C04B35/6264 , C04B2235/3826 , C04B2235/3895 , C04B2235/425 , C04B2235/483 , C04B2235/5427 , C04B2235/5436 , C04B2235/96 , C04B2235/9684 , H01M10/0525
摘要： A C/Si/O composite material having improved oxidation resistance is prepared by impregnating graphite with a crosslinkable silane or siloxane, causing the silane or siloxane to crosslink within the graphite, and heating at 300-1,200° C. in a non-oxidizing gas. The C/Si/O composite material can be efficiently prepared through simple steps, on an industrial scale and at a low cost and will find use as a high-temperature structural material by virtue of oxidation resistance.
摘要翻译： 通过用可交联的硅烷或硅氧烷浸渍石墨制备具有改善的抗氧化性的C / Si / O复合材料，使硅烷或硅氧烷在石墨内交联，并在非氧化气体中在300-1200℃下加热。 C / Si / O复合材料可以通过简单的步骤以工业规模和低成本有效地制备，并且由于抗氧化性而被用作高温结构材料。
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公开(公告)号：US07794681B2
公开(公告)日：2010-09-14
申请号：US11790031
申请日：2007-04-23
申请人： Hirofumi Fukuoka , Mikio Aramata , Satoru Miyawaki
发明人： Hirofumi Fukuoka , Mikio Aramata , Satoru Miyawaki
IPC分类号： C01B33/12 , C01B15/14 , C01B21/068 , B01D5/00 , B01D7/00
CPC分类号： C01B33/113 , C01B33/182
摘要： An efficient method for producing a silicon oxide powder at a low cost is provided. This method comprises the steps of heating a powder mixture of a silicon dioxide powder and a metal silicon powder to a temperature of 1,100 to 1,450° C. in an inert gas or under reduced pressure to generate silicon monoxide gas, and precipitating the silicon monoxide gas on a surface of a substrate to produce the silicon oxide powder, and in this method, the silicon dioxide powder has an average particle diameter of up to 1 μm, and the metal silicon powder has an average particle diameter of 30 μm.
摘要翻译： 提供了一种以低成本生产氧化硅粉末的有效方法。 该方法包括以惰性气体或减压的方式将二氧化硅粉末和金属硅粉末的粉末混合物加热至1100〜1450℃的温度，生成一氧化硅气体，使一氧化硅气体 在基板的表面上形成氧化硅粉末，在该方法中，二氧化硅粉末的平均粒径为1μm以下，金属硅粉的平均粒径为30μm。
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20.发明授权公开(公告)号：US07790316B2
公开(公告)日：2010-09-07
申请号：US11085518
申请日：2005-03-22
CPC分类号： H01B1/122 , H01M4/0471 , H01M4/13 , H01M4/131 , H01M4/133 , H01M4/136 , H01M4/139 , H01M4/364 , H01M4/386 , H01M4/485 , H01M4/58 , H01M4/587 , H01M4/60 , H01M10/0525 , H01M2004/021 , H01M2004/027
摘要： Silicon composite particles are prepared by sintering primary fine particles of silicon, silicon alloy or silicon oxide together with an organosilicon compound. Sintering of the organosilicon compound results in a silicon-base inorganic compound which serves as a binder. Each particle has the structure that silicon or silicon alloy fine particles are dispersed in the silicon-base inorganic compound binder, and voids are present within the particle.
摘要翻译： 通过将硅，硅合金或氧化硅的一次微粒与有机硅化合物一起烧结来制备硅复合颗粒。 有机硅化合物的烧结产生作为粘合剂的硅基无机化合物。 每个颗粒具有将硅或硅合金细颗粒分散在硅基无机化合物粘合剂中的结构，并且在颗粒内存在空隙。
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