Method for preparation of an alane-etherate complex and alane
    12.
    发明授权
    Method for preparation of an alane-etherate complex and alane 有权
    丙烷 - 乙醚络合物和丙烷的制备方法

    公开(公告)号:US09550672B2

    公开(公告)日:2017-01-24

    申请号:US14558240

    申请日:2014-12-02

    CPC classification number: C01B6/06

    Abstract: The invention relates to methods of forming an alane-etherate complex and α-alane from the alane-etherate complex. The methods include reacting an alkyl halide with a metal alanate in a solvent including an ether. A tertiary amine may also be added to the reaction. The alane is collected after removal of the solvent and/or the tertiary amine. An electrospraying process can be used to remove the solvent.

    Abstract translation: 本发明涉及从丙烷 - 乙醚合物络合物形成丙烷 - 乙醚合物络合物和α-甲烷的方法。 所述方法包括使烷基卤与金属铝酸盐在包括醚的溶剂中反应。 也可以向反应中加入叔胺。 在除去溶剂和/或叔胺之后收集丙烷。 可以使用电喷雾方法除去溶剂。

    Hydrogen generator
    13.
    发明授权
    Hydrogen generator 有权
    氢发生器

    公开(公告)号:US09231264B2

    公开(公告)日:2016-01-05

    申请号:US14506260

    申请日:2014-10-03

    Abstract: A hydrogen generator and a fuel cell system including a fuel cell battery and the hydrogen generator. The hydrogen generator includes a cartridge, a housing with a cavity to removably contain the cartridge, and an initiation system. The cartridge includes a casing; a plurality of pellets including a hydrogen containing material; a plurality of solid heat transfer members in contact with but not penetrating the casing; a hydrogen outlet in the casing; and a hydrogen flow path from each pellet to the hydrogen outlet. A plurality of heating elements is disposed inside the housing. When the cartridge is in the cavity, each heating element is disposed so heat can be conducted from the heating element and through the casing and corresponding heat transfer member to initiate the release of hydrogen gas. The initiation system can selectively heat one or more pellets to release hydrogen gas as needed.

    Abstract translation: 一种氢发生器和包括燃料电池和氢发生器的燃料电池系统。 氢气发生器包括筒,具有可移除地容纳盒的空腔的壳体和起始系统。 盒包括壳体; 包含含氢材料的多个粒料; 多个固体传热构件,其与壳体接触但不穿透壳体; 壳体中的氢出口; 以及从每个颗粒到氢气出口的氢气流动路径。 多个加热元件设置在壳体内。 当盒位于空腔中时,每个加热元件被设置成使得热量可以从加热元件通过壳体和相应的传热构件传导以开始释放氢气。 起始系统可以根据需要选择性地加热一个或多个粒料以释放氢气。

    MIXED METAL BOROHYDRIDES
    14.
    发明申请
    MIXED METAL BOROHYDRIDES 审中-公开
    混合金属硼氢化物

    公开(公告)号:US20150166336A1

    公开(公告)日:2015-06-18

    申请号:US14629317

    申请日:2015-02-23

    CPC classification number: H01M8/04216 C01B6/23 C01B35/00

    Abstract: The invention relates to mixed metal borohydrides used for solid hydrogen storage. The mixed metal borohydrides are synthesized through solution synthesis using multiple metal borohydrides. First and second precursor solutions are prepared and combined to create a mixture in which the mixed metal borohydride is formed. The solvent is removed, leaving the mixed metal borohydride. The first precursor solution consisting essentially of lithium borohydride, and the second precursor solution consisting essentially of a borohydride compound containing one or more metal cations selected from the group of metals consisting of sodium, magnesium, calcium and titanium.

    Abstract translation: 本发明涉及用于固体储氢的混合金属硼氢化物。 通过使用多种金属硼氢化物的溶液合成来合成混合金属硼氢化物。 制备和组合第一和第二前体溶液以产生其中形成混合金属硼氢化物的混合物。 除去溶剂,留下混合金属硼氢化物。 基本上由硼氢化锂组成的第一前体溶液和基本上由含有一种或多种选自钠,镁,钙和钛的金属组成的金属阳离子的硼氢化合物组成的第二前体溶液。

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