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74 条记录 (耗时 0.039 秒)

    Phase change inks and process for the preparation thereof
    12.
    发明授权
    Phase change inks and process for the preparation thereof 有权
    相变油墨及其制备方法

    公开(公告)号：US06878198B1

    公开(公告)日：2005-04-12

    申请号：US10722164

    申请日：2003-11-25

    申请人： Stephan V. Drappel ,  Marcel P. Breton ,  James D. Mayo ,  Raymond W. Wong ,  Christine E. Bedford ,  Danielle C. Boils-Boissier ,  Sandra J. Gardner ,  Paul F. Smith

    发明人： Stephan V. Drappel ,  Marcel P. Breton ,  James D. Mayo ,  Raymond W. Wong ,  Christine E. Bedford ,  Danielle C. Boils-Boissier ,  Sandra J. Gardner ,  Paul F. Smith

    IPC分类号： C09D11/00

    CPC分类号： C09D11/34

    摘要： Phase change ink compositions comprising (a) an ink carrier comprising a monoamide and a tetra-amide, and (b) pigment particles having oxygen-containing functional groups on the surfaces thereof. Also, processes for preparing a phase change ink which comprise (a) melting a tetra-amide which is solid at about 25° C.; (b) admixing with the molten tetra-amide pigment particles having oxygen-containing functional groups on the surfaces thereof; (c) maintaining the mixture of pigment and tetra-amide at a temperature of at least about 100° C. and at a temperature of no more than about 200° C. for a period sufficient to enable the molten tetra-amide to wet the pigment particle surfaces; (d) subsequent to wetting of the pigment particle surfaces with the molten tetra-amide, adding to the mixture a monoamide; (e) subsequent to addition of the monoamide, subjecting the resulting mixture to high shear mixing; and (f) subsequent to subjecting the mixture to high shear mixing, optionally adding to the mixture additional ink ingredients.

    摘要翻译： 相变油墨组合物，其包含（a）包含单酰胺和四酰胺的油墨载体，和（b）在其表面上具有含氧官能团的颜料颗粒。 另外，制备相变油墨的方法包括（a）在约25℃熔化固体的四酰胺; （b）与表面具有含氧官能团的熔融四酰胺颜料颗粒混合; （c）将颜料和四酰胺的混合物在至少约100℃的温度和不超过约200℃的温度下保持足以使熔融的四酰胺湿润的时间 颜料颗粒表面; （d）在用四酰胺熔融物润湿颜料颗粒表面之后，向混合物中加入单酰胺; （e）在加入单酰胺后，将所得混合物进行高剪切混合; 和（f）在混合物进行高剪切混合之后，任选地向混合物中加入另外的油墨成分。

    Processes for the preparation of titanium-phthalocyanine Type X
    13.
    发明授权
    Processes for the preparation of titanium-phthalocyanine Type X 失效
    X型钛酞菁的制备方法

    公开(公告)号：US5189156A

    公开(公告)日：1993-02-23

    申请号：US673506

    申请日：1991-04-01

    申请人： James D. Mayo ,  Sandra J. Gardner

    发明人： James D. Mayo ,  Sandra J. Gardner

    IPC分类号： C09B67/16 ,  C09B67/50

    CPC分类号： C09B67/0026 ,  C09B67/0019

    摘要： A process for the preparation of titanyl phthalocyanine which comprises the reaction of a titanium tetraalkoxide and diiminoisoindolene in the presence of a halonaphthalene solvent; dissolving the resulting Type I titanyl phthalocyanine in a haloacetic acid and an alkylene halide; adding the resulting mixture slowly to a cold alcohol solution; and thereafter isolating the resulting Type X titanyl phthalocyanine with an average volume particle size diameter of from about 0.02 to about 0.5 micron.

    摘要翻译： 一种制备钛酞菁的方法，其包括在卤代萘溶剂存在下四烷氧基钛和二亚氨基异吲哚啉的反应; 将得到的I型氧钛酞菁溶解在卤代乙酸和卤化烯中; 将所得混合物缓慢加入到冷的醇溶液中; 然后分离得到的X型氧钛酞菁的平均体积粒径直径为约0.02至约0.5微米。

    Processes for the preparation of titanyl phthalocyanines
    14.
    发明授权
    Processes for the preparation of titanyl phthalocyanines 失效
    制备钛酞菁的方法

    公开(公告)号：US5350844A

    公开(公告)日：1994-09-27

    申请号：US24145

    申请日：1993-03-01

    申请人： Trevor I. Martin ,  James D. Mayo ,  Nancy A. Listigovers ,  Cheng K. Hsiao ,  Terry L. Bluhm ,  Sharon E. Normandin ,  Kathleen M. Carmichael

    发明人： Trevor I. Martin ,  James D. Mayo ,  Nancy A. Listigovers ,  Cheng K. Hsiao ,  Terry L. Bluhm ,  Sharon E. Normandin ,  Kathleen M. Carmichael

    IPC分类号： C09B67/12 ,  C09B67/16 ,  C09B67/50

    CPC分类号： C09B67/0016 ,  C09B67/0019 ,  C09B67/0026

    摘要： A process for the preparation of a more perfect crystalline form of the Type I polymorph of titanyl phthalocyanine which comprises dissolving a precursor titanyl phthalocyanine Type I in a solution of trihaloacetic acid and alkylene chloride; adding the resultant solution to a solvent thereby enabling precipitation of Type X titanyl phthalocyanine; separating the titanyl phthalocyanine Type X from the solution; followed by a first washing with an organic solvent and a second washing with water; slurrying the resulting Type X titanyl phthalocyanine in an organic solvent enabling conversion of said Type X to Type IV titanyl phthalocyanine; and thereafter, subjecting the Type IV titanyl phthalocyanine obtained to treatment with an organic solvent to enable said crystalline form of titanyl phthalocyanine Type I.

    摘要翻译： 制备氧化钛酞菁的I型多晶型物的更完美结晶形式的方法，其包括将前体氧钛酞菁I溶解在三卤代乙酸和亚烷基氯的溶液中; 将所得溶液加入到溶剂中，从而使X型氧钛酞菁沉淀; 从溶液中分离X型氧钛酞菁; 然后用有机溶剂进行第一次洗涤，并用水洗涤第二次; 将得到的X型氧钛酞菁在有机溶剂中制浆，使所述X型转化为IV型氧钛酞菁; 然后，将得到的IV型钛酞菁用有机溶剂进行处理，得到所述晶型的钛氧酞菁I型。