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    Processes for preparing dianthranilate compounds and diazopyridone colorants
    2.
    发明授权
    Processes for preparing dianthranilate compounds and diazopyridone colorants 失效
    制备二邻氨基苯甲酸酯化合物和重氮吡啶酮着色剂的方法

    公开(公告)号：US06576747B1

    公开(公告)日：2003-06-10

    申请号：US10185261

    申请日：2002-06-27

    申请人： Rina Carlini ,  James M. Duff ,  Stephen G. Robinson ,  George Liebermann ,  Roger E. Gaynor ,  Tania Pereira ,  Jeffrey H. Banning ,  James D. Mayo

    发明人： Rina Carlini ,  James M. Duff ,  Stephen G. Robinson ,  George Liebermann ,  Roger E. Gaynor ,  Tania Pereira ,  Jeffrey H. Banning ,  James D. Mayo

    IPC分类号： C09B35031

    CPC分类号： C09B35/031 ,  C07C227/18 ,  C07C227/22 ,  C07C229/56 ,  C07D213/85 ,  Y10S534/02

    摘要： Disclosed is a process for preparing dianthranilate compounds which comprises (a) admixing reactants as follows: (1) a diol of the formula R1(OH)2, wherein R1 is an alkylene group having at least about 20 carbon atoms, and wherein the —OH groups are primary or secondary, (2) isatoic anhydride, present in an amount of at least, about 2 moles of isatoic anhydride per every one mole of diol, (3) a catalyst which is 1,4-diazabicyclo [2.2.2]octane, N,N,N′,N′-tetramethylethylene diamine, or a mixture thereof, said catalyst being present in an amount of at least about 0.2 mole of catalyst per every one mole of diol, and (4) a solvent; and (b) heating the mixture thus formed to form a dianthranilate compound of the formula Also disclosed is a process for preparing diazopyridone colorants which comprises (I) preparing a dianthranilate compound by the aforementioned method, (II) reacting the dianthranilate compound with nitrosylsulfuric acid to form a diazonium salt, and (III) reacting the, diazonium salt with a pyridone compound to form a diazopyridone compound.

    摘要翻译： 公开了一种制备二氨基甲酸盐化合物的方法，其包括（a）如下混合反应物：（1）式R 1（OH）2的二醇，其中R 1是具有至少约20个碳原子的亚烷基， OH基团是伯或仲，（2）丙酸酐，每1摩尔二醇存在量至少约2摩尔丙烯酸酐，（3）作为1,4-二氮杂双环[2.2.2 ]辛烷，N，N，N'，N'-四甲基乙二胺或其混合物，所述催化剂的存在量为每一摩尔二醇至少约0.2摩尔催化剂，和（4）溶剂; 和（b）加热由此形成的混合物以形成下式的二邻氨基苯甲酸酯化合物。另外公开的是一种制备重氮吡啶酮着色剂的方法，其包括（I）通过上述方法制备二氨基甲酸酯化合物，（II）使二邻氨基苯甲酸酯化合物与亚硝酰基磺酸反应 形成重氮盐，和（III）使重氮盐与吡啶酮化合物反应形成二叠氮基吡啶酮化合物。

    Process for preparing substituted pyridone compounds
    3.
    发明授权
    Process for preparing substituted pyridone compounds 有权
    取代吡啶酮化合物的制备方法

    公开(公告)号：US06696552B2

    公开(公告)日：2004-02-24

    申请号：US10185597

    申请日：2002-06-27

    申请人： James D. Mayo ,  James M. Duff ,  Rina Carlini ,  Roger E. Gaynor ,  George Liebermann

    发明人： James D. Mayo ,  James M. Duff ,  Rina Carlini ,  Roger E. Gaynor ,  George Liebermann

    IPC分类号： C09B4100

    CPC分类号： C07D213/69 ,  C07D213/85 ,  Y10S534/02

    摘要： A process which comprises admixing in the absence of a solvent an amine of the formula R1—NH2 and a first ester of the formula wherein R2 is an electron withdrawing group and R3 is an alkyl group; heating the mixture containing the amine and the first ester to form an intermediate compound of the formula admixing the intermediate compound with a base and a second ester of the formula said second ester being present in a molar excess relative to the intermediate compound, said base being present in a molar excess relative to the intermediate compound, and heating the mixture to form a pyridone compound of the formula or a salt thereof. Also disclosed is a process for preparing diazopyridone colorants which comprises preparing a pyridone compound by the above process and reacting the pyridone compound with a diazonium salt to form a diazopyridone compound.

    摘要翻译： 包括在不存在溶剂的情况下混合式R 1 -NH 2的胺和式R 2的第一酯的方法是吸电子基团，并且R 3是烷基; 加热含有胺和第一酯的混合物以形成中间体化合物，该中间体化合物将中间体化合物与碱和第二酯的第二酯相对于中间体化合物以摩尔过量存在，所述碱存在于 相对于中间体化合物的摩尔过量，并加热该混合物以形成式的吡啶酮化合物或其盐。 还公开了制备重氮吡啶酮着色剂的方法，其包括通过上述方法制备吡啶酮化合物并使吡啶酮化合物与重氮盐反应以形成重氮吡啶酮化合物。

    Arylamine processes
    5.
    发明授权
    Arylamine processes 失效
    芳胺方法

    公开(公告)号：US5902901A

    公开(公告)日：1999-05-11

    申请号：US74620

    申请日：1998-05-07

    申请人： H. Bruce Goodbrand ,  George Liebermann ,  Roger E. Gaynor

    发明人： H. Bruce Goodbrand ,  George Liebermann ,  Roger E. Gaynor

    IPC分类号： C07C209/10 ,  C07C211/54

    CPC分类号： C07C209/10

    摘要： A process for the preparation of N,N-bis(3,4-dimethylphenyl)-4-biphenylamine which comprises the reaction of N,N-bis(3,4-dimethylphenyl)amine and an iodobiphenyl in the presence of a ligand copper catalyst, and wherein the ligand is selected from the group consisting of monodentate tertiary amines and bidentate tertiary amines, and which reaction is accomplished at a temperature of, for example, from about 120.degree. C. to about 150.degree. C.

    摘要翻译： 一种制备N，N-双（3,4-二甲基苯基）-4-联苯胺的方法，其包括在配体铜的存在下N，N-双（3,4-二甲基苯基）胺和碘代联苯的反应 催化剂，并且其中所述配体选自单齿叔胺和二齿叔胺，并且该反应在例如约120℃至约150℃的温度下进行。

    Process for making titanyl phthalocyanine
    7.
    发明授权
    Process for making titanyl phthalocyanine 有权
    制备钛氧基酞菁的方法

    公开(公告)号：US07947825B2

    公开(公告)日：2011-05-24

    申请号：US11706892

    申请日：2007-02-13

    申请人： Marko D. Saban ,  George Liebermann ,  Roger E. Gaynor ,  Sandra Gardner ,  Cuong Vong ,  Evelyn Juandi

    发明人： Marko D. Saban ,  George Liebermann ,  Roger E. Gaynor ,  Sandra Gardner ,  Cuong Vong ,  Evelyn Juandi

    IPC分类号： C07B47/00 ,  C07D487/22

    CPC分类号： C07D487/22

    摘要： Processes for making organic pigments useful in imaging members, specifically for pigments that after further polymorphic conversion may be used in a charge generating layer of an imaging member. More specifically, there are described processes for producing titanyl phthalocyanine (TiOPc) in high yields using tetrahydronaphthalene as reaction solvent, such as TiOPc Type I. This pigment can be successfully converted to a high sensitivity crystal form useful as charge generating pigment in an imaging member.

    摘要翻译： 用于制备用于成像构件的有机颜料的方法，特别是用于进一步多晶型转化后的颜料的方法可用于成像构件的电荷产生层。 更具体地，描述了使用四氢化萘作为反应溶剂，例如TiOPc I型，以高产率生产钛酞菁（TiOPc）的方法。该颜料可以成功地转化成用作成像构件中的电荷产生颜料的高灵敏度晶体形式 。

    Process for making titanyl phthalocyanine
    8.
    发明申请
    Process for making titanyl phthalocyanine 有权
    制备钛氧基酞菁的方法

    公开(公告)号：US20080194814A1

    公开(公告)日：2008-08-14

    申请号：US11706892

    申请日：2007-02-13

    申请人： Marko D. Saban ,  George Liebermann ,  Roger E. Gaynor ,  Sandra Gardner ,  Cuong Vong ,  Evelyn Juandi

    发明人： Marko D. Saban ,  George Liebermann ,  Roger E. Gaynor ,  Sandra Gardner ,  Cuong Vong ,  Evelyn Juandi

    IPC分类号： C07D487/22

    CPC分类号： C07D487/22

    摘要： Processes for making organic pigments useful in imaging members, specifically for pigments that after further polymorphic conversion may be used in a charge generating layer of an imaging member. More specifically, there are described processes for producing titanyl phthalocyanine (TiOPc) in high yields using tetrahydronaphthalene as reaction solvent, such as TiOPc Type I. This pigment can be successfully converted to a high sensitivity crystal form useful as charge generating pigment in an imaging member.

    摘要翻译： 用于制备用于成像构件的有机颜料的方法，特别是用于进一步多晶型转化后的颜料的方法可用于成像构件的电荷产生层。 更具体地，描述了使用四氢化萘作为反应溶剂，例如TiOPc I型，以高产率生产钛酞菁（TiOPc）的方法。该颜料可以成功地转化成用作成像构件中的电荷产生颜料的高灵敏度晶体形式 。

    Hydroxygallium phthalocyanine photoconductive imaging members
    9.
    发明授权
    Hydroxygallium phthalocyanine photoconductive imaging members 失效
    羟基镓酞菁光导成像构件

    公开(公告)号：US5563261A

    公开(公告)日：1996-10-08

    申请号：US469240

    申请日：1995-06-06

    申请人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao Murti ,  Sandra J. Gardner

    发明人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao Murti ,  Sandra J. Gardner

    IPC分类号： C07D487/22 ,  C09B67/16 ,  C09B67/50 ,  G03G5/06 ,  C09B67/12

    CPC分类号： G03G5/0696

    摘要： A process for the preparation of hydroxygallium phthalocyanines which comprises hydrolyzing a gallium phthalocyanine precursor pigment by dissolving said hydroxygallium phthalocyanine in a strong acid and then reprecipitating the resulting dissolved pigment in basic aqueous media; removing any ionic species formed by washing with water, concentrating the resulting aqueous slurry comprised of water and hydroxygallium phthalocyanine to a wet cake; removing water from said slurry by azeotropic distillation with an organic solvent, and subjecting said resulting pigment slurry to mixing with the addition of a second solvent to cause the formation of said hydroxygallium phthalocyanine polymorphs.

    摘要翻译： 一种制备羟基镓酞菁的方法，其包括通过将所述羟基镓酞菁溶解在强酸中，然后将所得溶解的颜料再沉淀在碱性水性介质中来水解镓酞菁前体颜料; 去除通过用水洗涤形成的任何离子物质，将由水和羟基镓酞菁组成的所得水性浆料浓缩到湿饼; 通过与有机溶剂共沸蒸馏从所述浆料中除去水，并将所得颜料浆料加入第二溶剂进行混合，形成所述羟基镓酞菁多晶型物。

    Method of making hydroxygallium phthalocyanine type V photoconductive imaging members
    10.
    发明授权
    Method of making hydroxygallium phthalocyanine type V photoconductive imaging members 失效
    羟基镓酞菁V型感光成像剂的制备方法

    公开(公告)号：US5482811A

    公开(公告)日：1996-01-09

    申请号：US332304

    申请日：1994-10-31

    申请人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao K. Murti ,  Sandra J. Gardner

    发明人： Barkev Keoshkerian ,  George Liebermann ,  Cheng-Kuo Hsiao ,  James D. Mayo ,  Dasarao K. Murti ,  Sandra J. Gardner

    IPC分类号： C07D487/22 ,  C09B67/16 ,  C09B67/50 ,  G03G5/06 ,  G03G5/047

    CPC分类号： G03G5/0696

    摘要： A process for the preparation of hydroxygallium phthalocyanines which comprises hydrolyzing a gallium phthalocyanine precursor pigment by dissolving said hydroxygallium phthalocyanine in a strong acid and then reprecipitating the resulting dissolved pigment in basic aqueous media; removing any ionic species formed by washing with water, concentrating the resulting aqueous slurry comprised of water and hydroxygallium phthalocyanine to a wet cake; removing water from said slurry by azeotropic distillation with an organic solvent, and subjecting said resulting pigment slurry to mixing with the addition of a second solvent to cause the formation of said hydroxygallium phthalocyanine polymorphs.

    摘要翻译： 一种制备羟基镓酞菁的方法，其包括通过将所述羟基镓酞菁溶解在强酸中，然后将所得溶解的颜料再沉淀在碱性水性介质中来水解镓酞菁前体颜料; 去除通过用水洗涤形成的任何离子物质，将由水和羟基镓酞菁组成的所得水性浆料浓缩到湿饼; 通过与有机溶剂共沸蒸馏从所述浆料中除去水，并将所得颜料浆料加入第二溶剂进行混合，形成所述羟基镓酞菁多晶型物。