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    Processes for preparing dianthranilate compounds and diazopyridone colorants
    2.
    发明授权
    Processes for preparing dianthranilate compounds and diazopyridone colorants 失效
    制备二邻氨基苯甲酸酯化合物和重氮吡啶酮着色剂的方法

    公开(公告)号：US06576747B1

    公开(公告)日：2003-06-10

    申请号：US10185261

    申请日：2002-06-27

    申请人： Rina Carlini ,  James M. Duff ,  Stephen G. Robinson ,  George Liebermann ,  Roger E. Gaynor ,  Tania Pereira ,  Jeffrey H. Banning ,  James D. Mayo

    发明人： Rina Carlini ,  James M. Duff ,  Stephen G. Robinson ,  George Liebermann ,  Roger E. Gaynor ,  Tania Pereira ,  Jeffrey H. Banning ,  James D. Mayo

    IPC分类号： C09B35031

    CPC分类号： C09B35/031 ,  C07C227/18 ,  C07C227/22 ,  C07C229/56 ,  C07D213/85 ,  Y10S534/02

    摘要： Disclosed is a process for preparing dianthranilate compounds which comprises (a) admixing reactants as follows: (1) a diol of the formula R1(OH)2, wherein R1 is an alkylene group having at least about 20 carbon atoms, and wherein the —OH groups are primary or secondary, (2) isatoic anhydride, present in an amount of at least, about 2 moles of isatoic anhydride per every one mole of diol, (3) a catalyst which is 1,4-diazabicyclo [2.2.2]octane, N,N,N′,N′-tetramethylethylene diamine, or a mixture thereof, said catalyst being present in an amount of at least about 0.2 mole of catalyst per every one mole of diol, and (4) a solvent; and (b) heating the mixture thus formed to form a dianthranilate compound of the formula Also disclosed is a process for preparing diazopyridone colorants which comprises (I) preparing a dianthranilate compound by the aforementioned method, (II) reacting the dianthranilate compound with nitrosylsulfuric acid to form a diazonium salt, and (III) reacting the, diazonium salt with a pyridone compound to form a diazopyridone compound.

    摘要翻译： 公开了一种制备二氨基甲酸盐化合物的方法，其包括（a）如下混合反应物：（1）式R 1（OH）2的二醇，其中R 1是具有至少约20个碳原子的亚烷基， OH基团是伯或仲，（2）丙酸酐，每1摩尔二醇存在量至少约2摩尔丙烯酸酐，（3）作为1,4-二氮杂双环[2.2.2 ]辛烷，N，N，N'，N'-四甲基乙二胺或其混合物，所述催化剂的存在量为每一摩尔二醇至少约0.2摩尔催化剂，和（4）溶剂; 和（b）加热由此形成的混合物以形成下式的二邻氨基苯甲酸酯化合物。另外公开的是一种制备重氮吡啶酮着色剂的方法，其包括（I）通过上述方法制备二氨基甲酸酯化合物，（II）使二邻氨基苯甲酸酯化合物与亚硝酰基磺酸反应 形成重氮盐，和（III）使重氮盐与吡啶酮化合物反应形成二叠氮基吡啶酮化合物。

    Process for preparing substituted pyridone compounds
    3.
    发明授权
    Process for preparing substituted pyridone compounds 有权
    取代吡啶酮化合物的制备方法

    公开(公告)号：US06696552B2

    公开(公告)日：2004-02-24

    申请号：US10185597

    申请日：2002-06-27

    申请人： James D. Mayo ,  James M. Duff ,  Rina Carlini ,  Roger E. Gaynor ,  George Liebermann

    发明人： James D. Mayo ,  James M. Duff ,  Rina Carlini ,  Roger E. Gaynor ,  George Liebermann

    IPC分类号： C09B4100

    CPC分类号： C07D213/69 ,  C07D213/85 ,  Y10S534/02

    摘要： A process which comprises admixing in the absence of a solvent an amine of the formula R1—NH2 and a first ester of the formula wherein R2 is an electron withdrawing group and R3 is an alkyl group; heating the mixture containing the amine and the first ester to form an intermediate compound of the formula admixing the intermediate compound with a base and a second ester of the formula said second ester being present in a molar excess relative to the intermediate compound, said base being present in a molar excess relative to the intermediate compound, and heating the mixture to form a pyridone compound of the formula or a salt thereof. Also disclosed is a process for preparing diazopyridone colorants which comprises preparing a pyridone compound by the above process and reacting the pyridone compound with a diazonium salt to form a diazopyridone compound.

    摘要翻译： 包括在不存在溶剂的情况下混合式R 1 -NH 2的胺和式R 2的第一酯的方法是吸电子基团，并且R 3是烷基; 加热含有胺和第一酯的混合物以形成中间体化合物，该中间体化合物将中间体化合物与碱和第二酯的第二酯相对于中间体化合物以摩尔过量存在，所述碱存在于 相对于中间体化合物的摩尔过量，并加热该混合物以形成式的吡啶酮化合物或其盐。 还公开了制备重氮吡啶酮着色剂的方法，其包括通过上述方法制备吡啶酮化合物并使吡啶酮化合物与重氮盐反应以形成重氮吡啶酮化合物。