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公开(公告)号：US4206481A
公开(公告)日：1980-06-03
申请号：US870527
申请日：1978-01-18
CPC分类号： H01J29/826 , H01J29/762
摘要： A front extended portion, a pair of facing extending segments, and a rear extended portion mounted on the extending segments, which compose a coil separator, are integrally molded. Saddle-type horizontal coil is inserted in a rear extended portion through an opening between the pair of facing extending segments. In this state the horizontal coil are fixed to the rear extended portion of the coil separator by means of spacers.
摘要翻译： 整体模制了前延伸部分，一对相对的延伸段和安装在延伸段上的后延伸部分，其构成线圈分离器。 鞍形水平线圈通过一对相对的延伸段之间的开口插入到后延伸部分中。 在这种状态下，水平线圈通过间隔件固定到线圈分离器的后延伸部分。
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公开(公告)号：USD574737S1
公开(公告)日：2008-08-12
申请号：US29280006
申请日：2007-05-14
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公开(公告)号：US07289233B2
公开(公告)日：2007-10-30
申请号：US10798785
申请日：2004-03-12
CPC分类号： G01B11/0633
摘要： Light emitted from a light source (22) is used through a light projection optical system (23) to perform coaxial down-emission lighting on a measurement target (36). Light reflected by the measurement target (36) is formed on a photo-detector (26) through an image formation optical system (24). Along its optical path, a spectroscope (25) is provided for converting an image impinging on the photo-detector (26) into a spectroscopic image having a predetermined wavelength band. A measurement point extraction portion (32) in a signal processing portion (28) determines a predeterm film thickness measurement point from an image picked up by the photo-detector (26), extracts an image signal at the film thickness measurement point, and transmits t to film thickness operation portion (33). The film thickness operation portion (33) measured film thickness of a thin film, which is the measurement target (36), from this signal.
摘要翻译： 从光源（22）发射的光通过光投射光学系统（23）使用，以在测量目标（36）上执行同轴向下发射照明。 通过成像光学系统（24）在光检测器（26）上形成由测量对象（36）反射的光。 沿着其光路，设置分光镜（25），用于将照射在光检测器（26）上的图像转换为具有预定波长带的分光图像。 信号处理部分（28）中的测量点提取部分（32）从由光电检测器（26）拾取的图像中确定预制薄膜厚度测量点，在薄膜厚度测量点处提取图像信号， t到膜厚度操作部分（33）。 膜厚度运算部33根据该信号测定作为测定对象36的薄膜的膜厚。
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公开(公告)号：US5900491A
公开(公告)日：1999-05-04
申请号：US934638
申请日：1997-09-22
IPC分类号： C07D319/12 , C07D319/06
CPC分类号： C07D319/12
摘要： A process for preparing a cyclic ester by reacting an .alpha.-hydroxycarboxylic acid or an .alpha.-hydroxycarboxyliclic acid ester with an orthoester. A process for purifying a cyclic ester by containing water and acid as impurities by adding an orthoester to a cyclic ester obtained by reaction of a reaction mixture including an .alpha.-hydrocarboxylic acid or an .alpha.-hydroxycarboxyliclic acid ester. According to the present invention, a high-purity cyclic ester containing small amounts of impurities such as water and an acid component can be provided.
摘要翻译： 通过使α-羟基羧酸或α-羟基羧酸酯与原酸酯反应制备环酯的方法。 通过向通过包含α-羟基羧酸或α-羟基羧酸酯的反应混合物反应获得的环状酯中加入原酸酯，通过将水和酸作为杂质来含有水和酸来纯化环状酯的方法。 根据本发明，可以提供含有少量杂质如水和酸成分的高纯度环状酯。
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公开(公告)号：US5183539A
公开(公告)日：1993-02-02
申请号：US793958
申请日：1991-11-15
申请人： Akihiro Honma , Masahiro Kurokawa
发明人： Akihiro Honma , Masahiro Kurokawa
IPC分类号： C07D301/32 , C07D303/16
CPC分类号： C07D303/16 , Y10S203/06 , Y10S203/22
摘要： A method of purifying a crude glycidyl (meth)acrylate, by (1) subjecting a crude glycidyl (meth)acrylate containing epichlorohydrin and other chlorine compounds as impurities to a stripping treatment with a mixed gas containing oxygen gas in the presence of a quaternary ammonium salt, and then (2) distilling the treated product to obtain a purified glycidyl (meth)acrylate.
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16.发明申请公开(公告)号：US20100196794A1
公开(公告)日：2010-08-05
申请号：US12376468
申请日：2007-08-06
申请人： Masahiro Kurokawa , Yoshihiro Gocho
发明人： Masahiro Kurokawa , Yoshihiro Gocho
CPC分类号： H01M4/8807 , H01M4/8605 , H01M4/8668 , H01M4/8846 , H01M4/8882 , H01M4/8892 , H01M8/1009 , H01M8/1011 , H01M2008/1095 , Y02E60/523
摘要： Provided are: an electrode for a fuel cell, which is obtained by impregnating a supporting base with a vinyl polymer composition and a fuel cell catalyst, the vinyl polymer composition in which a vinyl polymer A having at least one kind of crosslinkable group selected from the group consisting of an epoxy group and an isocyanate group protected by a protecting group and a vinyl polymer B having at least one kind of crosslinkable group selected from the group consisting of a hydroxyl group, a carboxyl group, and an amino group are contained, and at least one of the vinyl polymer A and the vinyl polymer B has an acidic group forming a salt, reacting the crosslinkable group of the vinyl polymer A with the crosslinkable group of the vinyl polymer B, and then subjecting the salt to proton exchange; a method for producing the same; and a fuel cell including an electrolyte membrane and the electrode for a fuel cell.
摘要翻译： 提供：通过用乙烯基聚合物组合物和燃料电池催化剂浸渍支撑基底而获得的用于燃料电池的电极，其中具有至少一种可交联基团的乙烯基聚合物A选自 包含由保护基保护的环氧基和异氰酸酯基的乙烯基聚合物B和具有选自羟基，羧基和氨基的至少一种交联基团的乙烯基聚合物B， 乙烯基聚合物A和乙烯基聚合物B中的至少一种具有形成盐的酸性基团，使乙烯基聚合物A的可交联基团与乙烯基聚合物B的可交联基团反应，然后使盐进行质子交换; 其制造方法; 以及包括电解质膜和燃料电池用电极的燃料电池。
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公开(公告)号：US07056984B2
公开(公告)日：2006-06-06
申请号：US10144982
申请日：2002-05-15
IPC分类号： C08F291/02
CPC分类号： C08F291/02 , C08F265/04 , C08F265/06 , C08F279/02 , C08L51/003 , C08L51/04 , C08F220/14 , C08L2666/04
摘要： Disclosed is an acrylic syrup containing a vinyl monomer (A) of methyl methacrylate and a polymerized solid component (B) which is a high polymer of said vinyl monomer and has a weight average molecular weight of from 30,000 to 2,000,000 as measured by the GPC and a viscosity at 25° C. of from 0.1 to 50 Pa·s, wherein at least part of said polymerized solid component (B) is a grafted rubber obtained by graft-polymerizing said vinyl monomer with a rubbery polymer, and said grafted rubber has a large branching coefficient. The acrylic resin molded articles obtained from the acrylic syrup exhibit excellent impact resistance.
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公开(公告)号：US06448354B1
公开(公告)日：2002-09-10
申请号：US09696958
申请日：2000-10-27
IPC分类号： C08F2006
摘要： A methyl methacrylate syrup is produced by the steps of (1) preparing a starting material comprising methyl methacrylate or a monomer mixture mainly comprising methyl methacrylate, and dividing the starting material into 20 to 70% by weight of an initial charge and 30 to 80% by weight of an after-charge; (2) heating the initial charge in a reactor; (3) adding a whole protion of a chain transfer agent at the time when the initial charge reaches a reaction temperature; (4) adding the after-charge over 0.1 to 10 hours together with a polymerization initiator having a half-life of 10 to 300 seconds at the reaction temperature; (5) continuing the heating after the addition of the after-charge and the polymerization initiator is complete; and (6) adding a hindered phenol polymerization inhibitor at the time the heating is finished. The methyl methacrylate syrup thus produced is excellent in storage stability.
摘要翻译： 通过以下步骤制备甲基丙烯酸甲酯浆料：（1）制备包含甲基丙烯酸甲酯或主要包含甲基丙烯酸甲酯的单体混合物的原料，并将原料分成20至70重量％的初始电荷和30至80重量％ （重量）; （2）加热反应器中的初始装料; （3）在初始电荷达到反应温度时加入链转移剂的全部物质; （4）在反应温度下，将半衰期为10〜300秒的聚合引发剂与0.1〜10小时的后处理相加; （5）在加入后充电和聚合引发剂完成后继续加热; 和（6）在加热结束时加入受阻酚聚合抑制剂。 由此制备的甲基丙烯酸甲酯浆料的储存稳定性优异。
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公开(公告)号：US5804676A
公开(公告)日：1998-09-08
申请号：US704270
申请日：1996-08-28
CPC分类号： B01J19/1862 , C08F20/14 , B01J2219/00094 , B01J2219/00101 , B01J2219/00103 , B01J2219/00159 , B01J2219/00162 , B01J2219/00164
摘要： A process for continuously preparing a high quality methacrylic polymer with a high productivity is provided. The process comprises continuously polymerizing methyl methacrylate alone or a monomer mixture of methyl methacrylate and an alkyl acrylate by a solution polymerization using methanol as a solvent, directly feeding the resulting polymerization reaction product to an extruder having a plurality of vents, and extruding the polymer, while volatiles are removed through the vents.
摘要翻译： 提供了一种以高生产率连续制备高品质甲基丙烯酸聚合物的方法。 该方法包括通过使用甲醇作为溶剂的溶液聚合连续聚合甲基丙烯酸甲酯单独或甲基丙烯酸甲酯和丙烯酸烷基酯的单体混合物，将所得聚合反应产物直接进料到具有多个通气口的挤出机中，并挤出聚合物， 而挥发物通过通风口排出。
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20.发明授权
公开(公告)号：US5750739A
公开(公告)日：1998-05-12
申请号：US687053
申请日：1996-08-07
IPC分类号： C07D301/30 , B01J31/02 , C07B61/00 , C07D301/27 , C07D303/16
CPC分类号： C07D303/16
摘要： There is disclosed a process for producing a glycidyl ester of acrylic acid or methacrylic acid which comprises the steps of neutralizing acrylic acid or methacrylic acid with a carbonate or a bicarbonate of an alkali metal in an excess amount of epichlorohydrin while an oxygen-containing gas is blown into the liquid reaction system; subjecting water formed by the neutralization and epichlorohydrin to azeotropic distillation to discharge them outside the reaction system and to form an alkali metal salt of acrylic acid or methacrylic acid; adding a quaternary ammonium salt as a catalyst to the reaction system to react the alkali metal salt of the acid with the epichlorohydrin and thus synthesize the glycidyl ester of the acid; cooling the liquid reaction product while recovering part of the excess epichlorohydrin under reduced pressure; adding aqueous solution of an alkali hydroxide to the liquid reaction product to separate into aqueous layer and organic layer; adding a catalyst deactivator to the organic phase; and subsequently distilling the organic layer to separate the glycidyl ester of the acid while blowing an oxygen-containing gas into the organic layer. The above process makes it possible to efficiently produce a highly pure glycidyl ester of acrylic acid or methacrylic acid in high yield with minimized contents of impurities.
摘要翻译： 公开了一种制备丙烯酸或甲基丙烯酸的缩水甘油酯的方法，该方法包括以下步骤：用过量表氯醇的碱金属的碳酸盐或碳酸氢盐中和丙烯酸或甲基丙烯酸，同时含氧气体为 吹入液体反应系统; 将由中和产生的水和表氯醇进行共沸蒸馏，将其排出反应体系外，形成丙烯酸或甲基丙烯酸的碱金属盐; 向反应体系中加入季铵盐作为催化剂，使酸的碱金属盐与表氯醇反应，合成酸的缩水甘油酯; 冷却液体反应产物，同时在减压下回收部分过量表氯醇; 将碱性氢氧化物的水溶液加入到液体反应产物中以分离成水层和有机层; 向有机相中加入催化剂失活剂; 随后蒸出有机层以分离酸的缩水甘油酯，同时将含氧气体吹入有机层。 上述方法使得可以以最小化的杂质含量以高产率有效地制备丙烯酸或甲基丙烯酸的高纯度缩水甘油酯。
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