APPARATUS FOR PREPARING POLYBUTADIENE
    1.
    发明申请

    公开(公告)号:US20180037683A1

    公开(公告)日:2018-02-08

    申请号:US15554554

    申请日:2016-10-18

    Applicant: LG Chem, Ltd.

    Abstract: Provided is an apparatus for preparing polybutadiene which may improve productivity by minimizing a plugging phenomenon occurred during the preparation of polybutadiene and increasing a conversion rate. The apparatus for preparing polybutadiene includes two first polymerization reactors arranged in parallel to reduce the plugging phenomenon in which butadiene (reaction raw material), a polymerization catalyst, and a solvent are respectively supplied and polymerized, at least one second polymerization reactor arranged in series with the first polymerization reactors in which a first polymerization solution containing a butadiene polymer discharged from the first polymerization reactors is supplied and a butadiene polymerization reaction is performed, and one or more condensers which condense gases discharged from the first polymerization reactors and the second polymerization reactor and supply a condensate to the first polymerization reactors and/or the second polymerization reactor.

    Horizontal High-Pressure Melamine Reactor
    2.
    发明申请
    Horizontal High-Pressure Melamine Reactor 有权
    卧式高压三聚氰胺反应器

    公开(公告)号:US20130172555A1

    公开(公告)日:2013-07-04

    申请号:US13806157

    申请日:2011-06-23

    Abstract: A high-pressure melamine reactor is provided. The high-pressure melamine reactor comprising at least one horizontal reactor body having a bottom and a top side with at least one dome integrally formed on the top side of the reactor body. The at least one horizontal reactor body comprises at least two compartments separated by at least one baffle, in particular an overflow baffle. The at least one dome is solely located above at least one of the compartments serving as melamine synthesis unit, wherein the at least one compartment serving as melamine synthesis unit comprises at least one heating element.

    Abstract translation: 提供了高压三聚氰胺反应器。 所述高压三聚氰胺反应器包括至少一个具有底部和顶侧的水平反应器主体,所述水平反应器主体具有在所述反应器主体的顶侧上整体形成的至少一个圆顶。 所述至少一个水平反应器主体包括至少两个由至少一个挡板隔开的隔室,特别是溢流挡板。 至少一个圆顶仅位于用作三聚氰胺合成单元的隔室中的至少一个之上,其中用作三聚氰胺合成单元的至少一个隔室包括至少一个加热元件。

    Cavitation Reaction Apparatus
    4.
    发明申请
    Cavitation Reaction Apparatus 有权
    空化反应装置

    公开(公告)号:US20080042305A1

    公开(公告)日:2008-02-21

    申请号:US11739149

    申请日:2007-04-24

    Applicant: Ion C. Halalay

    Inventor: Ion C. Halalay

    Abstract: An apparatus is provided for carrying out a cavitation induced reaction comprising a reaction chamber for a liquid reaction medium, means for producing cavitation in the liquid reaction medium, at least one reactant inlet to the reaction chamber, an inert gas inlet conduit with a sparger for injecting a flowing stream of dry inert gas into the reaction chamber, a venting outlet for removal of a stream of the inert gas from the reaction chamber, and a recirculation conduit for re-circulating a stream of the inert gas from the venting outlet to the inert gas inlet conduit.

    Abstract translation: 提供了一种用于进行空化诱导反应的装置,其包括用于液体反应介质的反应室,用于在液体反应介质中产生空化的装置,至少一个反应室的反应物入口,具有喷雾器的惰性气体入口导管, 将干燥惰性气体的流动流注入反应室,用于从反应室除去惰性气体流的排气口和用于将惰性气体流从排气出口再循环到再循环管道的再循环管道 惰性气体入口导管。

    Method for optimization of process by adjustment of initiator in polymerization system
    5.
    发明申请
    Method for optimization of process by adjustment of initiator in polymerization system 有权
    通过调节聚合体系中引发剂优化工艺的方法

    公开(公告)号:US20070238844A1

    公开(公告)日:2007-10-11

    申请号:US11655150

    申请日:2007-01-19

    Abstract: Disclosed herein is an optimization method in a polymerization system in which heat is generated during the polymerization with an initiator. The optimization method includes the steps of measuring the heat generation amount based on the composition of the initiator in the polymerization system to previously set the relationship between the initiator composition and the heat generation amount, measuring the heat removal amount based on the temperature of a coolant in a cooling system of the polymerization system to previously set the relationship between the coolant temperature and the heat removal amount, calculating the initiator composition allowable at a predetermined coolant temperature to previously set the relationship between the coolant temperature and the initiator composition, and measuring the temperature of the coolant before and/or during the polymerization to adjust the composition of the initiator added at the measured temperature to the optimum condition, thereby decreasing the reaction time, and therefore, improving the productivity.

    Abstract translation: 本文公开了在与引发剂聚合期间产生热量的聚合体系中的优化方法。 优化方法包括以下步骤:基于聚合体系中引发剂的组成来测定发热量,以预先设定引发剂组合物与发热量之间的关系,基于冷却剂的温度测量除热量 在聚合系统的冷却系统中,预先设定冷却剂温度和除热量之间的关系,计算在预定冷却剂温度下允许的引发剂组合物,以预先设定冷却剂温度和引发剂组合物之间的关系,并测量 在聚合之前和/或聚合期间冷却剂的温度将调节在测量温度下加入的引发剂的组成调节到最佳条件,由此减少反应时间,从而提高生产率。

    Vinyl chloride polymerization process using ball valves in recycle line
    9.
    发明授权
    Vinyl chloride polymerization process using ball valves in recycle line 失效
    氯乙烯聚合工艺在循环管线中使用球阀

    公开(公告)号:US5462998A

    公开(公告)日:1995-10-31

    申请号:US285297

    申请日:1994-08-03

    Abstract: A polymerization apparatus equipped with a circuit made up of a polymerization vessel, a heat exchanger placed outside said polymerization vessel, and a circulation pipeline extending from said polymerization vessel and returning to said polymerization vessel through said heat exchanger, a branch pipeline being connected to said circulation pipeline through a ball valve comprising a spherical valve element and a valve body for housing said spherical valve element, wherein the valve body of said ball valve is joined directly to said circulation pipeline, and a method of producing a polymer of a monomer having an ethylenically unsaturated double bond by using said apparatus. Scale and polymers in the form of blocks can be prevented from mixing with the reaction mixture. Therefore, where the obtained polymer is formed into a sheet or the like, the fish eyes can be decreased, and if the polymerization is repeated, clogging of the tubes of the heat exchanger and drop in the flow velocity of the reaction mixture can be prevented.

    Abstract translation: 一种装配有由聚合容器,置于所述聚合容器外部的热交换器和从所述聚合容器延伸的循环管道并通过所述热交换器返回所述聚合容器的回路的聚合装置,连接到所述聚合容器的分支管道 通过球阀的循环管道,该球阀包括球形阀元件和用于容纳所述球形阀元件的阀体,其中所述球阀的阀体直接连接到所述循环管道,以及制备具有 烯属不饱和双键。 可以防止垢和块状聚合物与反应混合物混合。 因此,在得到的聚合物形成为片状物等的情况下,可以减少鱼眼,如果重复聚合,则可以防止热交换器的管堵塞和反应混合物的流速下降 。

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