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11.发明授权Process for producing hexamethylenediamine and aminocapronitrile from adiponitrile, wherein the hexamethylenediamine contains less than 100 ppm tetrahydroazepine 失效从己二腈生产六亚甲基二胺和氨基己腈的方法，其中六亚甲基二胺含有小于100ppm的四氢氮杂公开(公告)号：US07060819B2
公开(公告)日：2006-06-13
申请号：US10663479
申请日：2003-09-15
IPC分类号： C07D201/16 , C07D223/02
CPC分类号： C07C253/30 , C07C209/48 , C07C209/84 , C07C211/12 , C07C255/24
摘要： Process for making both ACN and HMD from partial hydrogenation of ADN by using a combination of distillations resulting in the formation of a mixture of HMD and THA that can be hydrogenated to produce a mixture of HMD and HMI that can be separated easily by simple distillation.
摘要翻译： 通过使用蒸馏组合形成ACN和HMD来制备HMD和THA的混合物，可以被氢化以产生可通过简单蒸馏容易地分离的HMD和HMI的混合物来制备ADN的部分氢化的方法。
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12.发明授权[Hexakis(pentenenitrilo)nickel II]bis-[.mu.-(cyano) bis(triphenylborane) (I)], its method of preparation and its use 失效[Hexakis（pentenenitrilo）nickel II] bis- [ - （氰基）双（三苯基硼烷）（I）]，其制备方法及其用途
公开(公告)号：US4749801A
公开(公告)日：1988-06-07
申请号：US870739
申请日：1986-06-04
IPC分类号： C07C67/00 , C07C253/00 , C07C253/10 , C07C253/30 , C07C255/04 , C07F15/04
CPC分类号： C07F15/04 , C07C253/10
摘要： Process for preparing a new compound: [hexakis(pentenenitrilo)nickel II]bis[.mu.-(cyano)bis(triphenylborane)(I)] which is useful as a promoter in the hydrocyanation of 3 or 4-pentenenitrile.
摘要翻译： 制备新化合物的方法：可用作3或4-戊烯腈的氢化氰化促进剂的[六（五烯基三烯）镍II]双[ - （氰基）双（三苯基硼烷）（I）]。
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13.发明授权Nickel metal compositions and nickel complexes derived from basic nickel carbonates 有权镍金属组合物和衍生自碱式碳酸镍的镍络合物公开(公告)号：US09371343B2
公开(公告)日：2016-06-21
申请号：US12968341
申请日：2010-12-15
申请人： John J. Ostermaier
发明人： John J. Ostermaier
IPC分类号： B01J31/18 , C01G53/06 , C07C253/10 , C07C255/04 , C07C255/07 , C07F9/145 , C22B23/00
CPC分类号： C07F9/145 , B01J31/185 , B01J2231/322 , B01J2531/847 , C01G53/06 , C07C253/10 , C07C255/07 , C07C255/04
摘要： Nickel-metal-containing solids for use in manufacturing nickel metal complexes are disclosed. The nickel-metal-containing solids are made by reducing basic nickel carbonates. By varying the molar ratios of carbonates and bicarbonates to nickel salts, the methods provide basic nickel carbonates that produce superior nickel metal-containing solids that react more effectively with phosphorous-containing ligands. The phosphorous containing ligands can be both monodentate and bidentate phosphorous-containing ligands.
摘要翻译： 公开了用于制造镍金属络合物的含镍金属固体。 含镍金属的固体是通过还原碱式碳酸镍制成的。 通过改变碳酸盐和碳酸氢盐与镍盐的摩尔比，该方法提供碱式镍碳酸盐，其产生优异的含有镍金属的固体，其与含磷配体更有效地反应。 含磷配体可以是单齿和二齿含磷配体。
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公开(公告)号：US08101790B2
公开(公告)日：2012-01-24
申请号：US12137925
申请日：2008-06-12
IPC分类号： C07C253/34
CPC分类号： C07C253/34 , C07C255/04
摘要： A process and apparatus for reacting deleterious impurities contained in adiponitrile (ADN) comprises feeding ADN and an ozone containing gas into a co-current plug flow reactor containing static mixer elements, to oxidize at least a portion of the impurities, thereby producing a reactor discharge, which is processed to produce an ozone-treated ADN product.
摘要翻译： 用于使己二腈（ADN）中所含的有害杂质反应的方法和装置包括将ADN和含臭氧气体进料到含有静态混合器元件的并流活塞流反应器中，以氧化至少一部分杂质，从而产生反应器排放 ，其被处理以产生经臭氧处理的ADN产物。
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公开(公告)号：US07678906B2
公开(公告)日：2010-03-16
申请号：US12027432
申请日：2008-02-07
申请人： John J. Ostermaier
发明人： John J. Ostermaier
IPC分类号： C07F5/02
CPC分类号： C07F5/027
摘要： A process for improving the recovery of solid triphenylboron-pyridine compound (TPBP), while retaining desirable particle characteristics comprises the addition of an acid to neutralize at least a portion of the alkali contained in the aqueous mother liquor. By adjusting the pH of the product slurry to between about 8.5 and about 12, it is possible to increase product recovery by more than 10%, while maintaining desirable particle characteristics.
摘要翻译： 改善固体三苯基硼 - 吡啶化合物（TPBP）回收率的方法同时保留所需的颗粒特性包括加入酸以中和含水母液中的至少一部分碱。 通过将产品浆料的pH调节至约8.5至约12之间，可以在保持理想的颗粒特性的同时将产品回收率提高10％以上。
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公开(公告)号：US07517985B2
公开(公告)日：2009-04-14
申请号：US11473907
申请日：2006-06-23
IPC分类号： C07F5/02
CPC分类号： C07F5/027
摘要： A process for producing solid triphenylboron-pyridine (TPBP) spherical particles by separately feeding into a vigorously agitated reaction zone (i) a stream of pyridine and a (ii) stream comprising a solution of sodium hydroxide adduct of triphenylboron (TPBA) whereby the total concentration of TPBA in the combined feed streams is in the range of from 1 wt % to 6 wt %, and simultaneously removing a product stream from said reaction zone and recovering the triphenylboron-pyridine (TPBP) particles.
摘要翻译： 通过分别进料到剧烈搅拌的反应区（i）吡啶流和包含三苯基硼（TPBA）的氢氧化钠加合物溶液的（ⅱ）流），生产固体三苯基硼 - 吡啶（TPBP）球形颗粒的方法，其中总共 组合进料流中TPBA的浓度在1重量％至6重量％的范围内，同时从所述反应区除去产物流并回收三苯基硼 - 吡啶（TPBP）颗粒。
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17.发明授权Recovery of hexamethylenediamine (HMD) with low polarographically reducible impurities (PRI) from mixtures of HMD, aminocapronitirle and PRI 有权从HMD，氨基己腈和PRI的混合物中回收具有低极谱降解杂质（PRI）的六亚甲基二胺（HMD）公开(公告)号：US06248926B1
公开(公告)日：2001-06-19
申请号：US09697691
申请日：2000-10-26
申请人： John J. Ostermaier , Leon S. Scott
发明人： John J. Ostermaier , Leon S. Scott
IPC分类号： C07C20948
CPC分类号： C07C209/86 , C07C211/12
摘要： A method for separating a mixture of hexamethylenediamine, aminocapronitile and polarographically reducible impurities using fractional distillation in which the temperature in the rectifying zone of a distillation column varies sigmoidally along its length to force a major portion of the PRI to co-distill with the aminocapronitrile.
摘要翻译： 使用分馏法分离六亚甲基二胺，氨基己内酯和极谱可还原杂质的混合物的方法，其中蒸馏塔的精馏区中的温度沿着其长度乙酰乙腈地改变，迫使大部分PRI与氨基己腈共蒸馏。
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公开(公告)号：US08815186B2
公开(公告)日：2014-08-26
申请号：US12968373
申请日：2010-12-15
申请人： John J. Ostermaier
发明人： John J. Ostermaier
IPC分类号： C01G1/00
CPC分类号： C07F9/145 , B01J31/185 , B01J2231/322 , B01J2531/847 , C01G53/06 , C07C253/10 , C07C255/07 , C07C255/04
摘要： Nickel compositions for use in manufacturing nickel metal compositions, and specifically to methods of making basic nickel carbonates used to produce nickel metal compositions are disclosed. By varying the molar ratios of carbonates and bicarbonates to nickel salts, the methods provide basic nickel carbonates that produce superior nickel-containing solids that react more effectively with phosphorous-containing ligands. The phosphorous containing ligands can be both monodentate and bidentate phosphorous-containing ligands.
摘要翻译： 公开了用于制造镍金属组合物的镍组合物，具体涉及用于制备镍金属组合物的制备碱式镍碳酸盐的方法。 通过改变碳酸盐和碳酸氢盐与镍盐的摩尔比，该方法提供碱式碳酸镍，产生与含磷配体更有效反应的优异的含镍固体。 含磷配体可以是单齿和二齿含磷配体。
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公开(公告)号：US20110311428A1
公开(公告)日：2011-12-22
申请号：US12968373
申请日：2010-12-15
申请人： John J. Ostermaier
发明人： John J. Ostermaier
IPC分类号： C01G53/06
CPC分类号： C07F9/145 , B01J31/185 , B01J2231/322 , B01J2531/847 , C01G53/06 , C07C253/10 , C07C255/07 , C07C255/04
摘要： Nickel compositions for use in manufacturing nickel metal compositions, and specifically to methods of making basic nickel carbonates used to produce nickel metal compositions are disclosed. By varying the molar ratios of carbonates and bicarbonates to nickel salts, the methods provide basic nickel carbonates that produce superior nickel-containing solids that react more effectively with phosphorous-containing ligands. The phosphorous containing ligands can be both monodentate and bidentate phosphorous-containing ligands.
摘要翻译： 公开了用于制造镍金属组合物的镍组合物，具体涉及用于制备镍金属组合物的制备碱式镍碳酸盐的方法。 通过改变碳酸盐和碳酸氢盐与镍盐的摩尔比，该方法提供碱式碳酸镍，产生与含磷配体更有效反应的优异的含镍固体。 含磷配体可以是单齿和二齿含磷配体。
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公开(公告)号：US20070299259A1
公开(公告)日：2007-12-27
申请号：US11473907
申请日：2006-06-23
IPC分类号： C07F5/02
CPC分类号： C07F5/027
摘要： A process for producing solid triphenylboron-pyridine (TPBP) spherical particles by separately feeding into a vigorously agitated reaction zone (i) a stream of pyridine and a (ii) stream comprising a solution of sodium hydroxide adduct of triphenylboron (TPBA) whereby the total concentration of TPBA in the combined feed streams is in the range of from 1 wt % to 6 wt %, and simultaneously removing a product stream from said reaction zone and recovering the triphenylboron-pyridine (TPBP) particles.
摘要翻译： 通过分别进料到剧烈搅拌的反应区（i）吡啶流和包含三苯基硼（TPBA）的氢氧化钠加合物溶液的（ⅱ）流），生产固体三苯基硼 - 吡啶（TPBP）球形颗粒的方法，其中总共 组合进料流中TPBA的浓度在1重量％至6重量％的范围内，同时从所述反应区除去产物流并回收三苯基硼 - 吡啶（TPBP）颗粒。
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