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公开(公告)号：US3101369A
公开(公告)日：1963-08-20
申请号：US13410761
申请日：1961-08-28
Applicant: UNITED STATES BORAX CHEM
Inventor： BROTHERTON ROBERT J , MCCLOSKEY ALLEN L
CPC classification number: C07F5/022 , C07F5/02 , C07F5/025 , C08G59/4078
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公开(公告)号：US3028368A
公开(公告)日：1962-04-03
申请号：US83243059
申请日：1959-08-10
Applicant: UNITED STATES BORAX CHEM
Inventor： DAVID ENGLISH WILLIAM , MCCLOSKEY ALLEN L , HOWARD STEINBERG
CPC classification number: C08G79/08 , C08G18/3897 , Y10S528/906
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公开(公告)号：US3139453A
公开(公告)日：1964-06-30
申请号：US77641058
申请日：1958-11-26
Applicant: UNITED STATES BORAX CHEM
Inventor： HOWARD STEINBERG , MCCLOSKEY ALLEN L
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公开(公告)号：US3082252A
公开(公告)日：1963-03-19
申请号：US10901961
申请日：1961-05-10
Applicant: UNITED STATES BORAX CHEM
Inventor： NEWSOM HERBERT C , WOODS WILLIAM C , MCCLOSKEY ALLEN L
IPC: C07F5/02
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公开(公告)号：US3082234A
公开(公告)日：1963-03-19
申请号：US6693060
申请日：1960-11-03
Applicant: UNITED STATES BORAX CHEM
Inventor： KIYOSHI KITASAKI , MCCLOSKEY ALLEN L , WOODS WILLIAM G
CPC classification number: C11B5/0078 , C07F5/066 , C07F5/069 , C08K5/36 , C08K5/37 , C10L1/2406 , C08L21/00
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Patent Agency Ranking
公开(公告)号：US3079432A
公开(公告)日：1963-02-26
申请号：US15694461
申请日：1961-12-04
Applicant: UNITED STATES BORAX CHEM
Inventor： PETTERSON LOWELL L , BROTHERTON ROBERT J , WIILCOCKSON GEORGE W , MCCLOSKEY ALLEN L
CPC classification number: C10M3/00 , C07F5/006 , C07F5/025 , C10L1/303 , C10M2227/08 , C10N2210/03 , C10N2240/08
Abstract: An amino(phenyl) borane of the formula R1(3-n)B(NR2)n is made by the interaction of an aminohaloborane of the formula (R2N)nBX(3-n), an aromatic halide of the formula R1X and, in a state capable of providing a continuously available active surface, a metal consisting of sodium, lithium, potassium, a sodium-potassium alloy or sodium amalgam, X being chlorine or bromine, R1 being phenyl, m- or p-tolyl, R being an alkyl group of from 1 to 6 carbon atoms, cyclohexyl, benzyl, unsubstituted phenyl or an alkyl-substituted phenyl in which the alkyl substitutent contains from 1 to 4 carbon atoms, and n being 1 or 2. The metal is either dispersed in a very small particle size or in a liquid or molten condition and the reaction is conducted with agitation. Examples of reactants are given and detailed examples describe the preparation of bis(dimethylamino)phenylborane, dimethylamino(diphenyl)borane, bis(diphenylamino) phenylborane and bis(dimethylamino)-p-tolylborane.
Abstract translation: 式R 1（3-n）B（NR 2）n的氨基（苯基）硼烷是通过式（R2N）nBX（3-n）的氨基卤代硼烷，式R1X的芳族卤化物， 在能够提供连续可用的活性表面的状态下，由钠，锂，钾，钠 - 钾合金或钠汞齐组成的金属，X为氯或溴，R1为苯基，间或对甲苯基，R为 1至6个碳原子的烷基，环己基，苄基，未取代的苯基或烷基取代的苯基，其中烷基取代基含有1至4个碳原子，n为1或2.金属分散在 非常小的粒度或液体或熔融状态，反应在搅拌下进行。 给出了反应物的实例，详细的实施例描述了双（二甲基氨基）苯基硼烷，二甲基氨基（二苯基）硼烷，双（二苯基氨基）苯基硼烷和双（二甲基氨基）对甲苯基硼烷的制备。
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公开(公告)号：US2974165A
公开(公告)日：1961-03-07
申请号：US79104359
申请日：1959-02-04
Applicant: UNITED STATES BORAX CHEM
Inventor： BROTHERTON ROBERT J , HOWARD STEINBERG , MCCLOSKEY ALLEN L
IPC: C01B21/082 , C01B21/092 , C01B35/16 , C07F5/02
CPC classification number: C07F5/022 , C01B21/082 , C01B21/0923
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公开(公告)号：US3255153A
公开(公告)日：1966-06-07
申请号：US6860160
申请日：1960-11-14
Applicant: UNITED STATES BORAX CHEM
Inventor： MCCLOSKEY ALLEN L , COLLINS GROVER G , DAVID ENGLISH WILLIAM
IPC: C08G59/40
CPC classification number: C08G59/4078
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公开(公告)号：US3072718A
公开(公告)日：1963-01-08
申请号：US10950361
申请日：1961-05-12
Applicant: UNITED STATES BORAX CHEM
Inventor： NEWSON HERBERT C , WOODS WILLIAM G , MCCLOSKEY ALLEN L
IPC: C07F5/02
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公开(公告)号：US3068182A
公开(公告)日：1962-12-11
申请号：US83541459
申请日：1959-08-24
Applicant: UNITED STATES BORAX CHEM
Inventor： DAVID ENGLISH WILLIAM , MCCLOSKEY ALLEN L
CPC classification number: H01B3/30 , C07F5/02 , C07F5/022 , C08G73/00 , C08G79/08 , C10L1/303 , C10M1/08 , C10M2227/06 , C10M2227/08 , C10N2210/03
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