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公开(公告)号：US20090215946A1
公开(公告)日：2009-08-27
申请号：US11909923
申请日：2006-03-27
Applicant: Doetze Jakob Sikkema , David J. Rodini , Hasan Dindi , James Arnold Schultz , Georg Valentin Martin , Ralf Demuth , Michael Schelhaas
Inventor： Doetze Jakob Sikkema , David J. Rodini , Hasan Dindi , James Arnold Schultz , Georg Valentin Martin , Ralf Demuth , Michael Schelhaas
IPC: C08K3/32 , C09K3/00 , C08F226/06
CPC classification number: C07D213/73 , C08G73/18 , C08G73/22
Abstract: Disclosed are processes for preparing monomer complexes that include contacting 2,3,5,6-tetraaminopyridine free base in water with 2,5-dihydroxy terephthalic acid dipotassium salt to form an aqueous mixture, and adjusting the pH of the aqueous mixture to within the range of from about (3) to about (5) to precipitate the monomer complex. Processes of polymerizing the monomer complexes, polyareneazoles, filaments and yarns are also disclosed.
Abstract translation: 公开了制备单体络合物的方法，其包括使水中的2,3,5,6-四氨基吡啶游离碱与2,5-二羟基对苯二甲酸二钾盐接触以形成含水混合物，并将含水混合物的pH调节至 范围为约（3）至约（5）以沉淀单体络合物。 还公开了聚合单体络合物，聚芳唑，长丝和纱线的方法。
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公开(公告)号：US5667743A
公开(公告)日：1997-09-16
申请号：US651174
申请日：1996-05-21
Applicant: Tsung-Ming Tai , David J. Rodini , James C. Masson , Richard L. Leonard
Inventor： Tsung-Ming Tai , David J. Rodini , James C. Masson , Richard L. Leonard
Abstract: A process for wet spinning a meta-aramid polymer solutions having a salt content of at least 3 percent by weight produces a one step, fully wet drawable fiber that has desirable physical properties without subjecting the fiber to hot stretching.
Abstract translation: 用于湿法纺丝具有至少3重量％的盐含量的间位芳族聚酰胺聚合物溶液的方法产生具有所需物理性能而不对纤维进行热拉伸的一步完全湿拉伸纤维。
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公开(公告)号：US5300122A
公开(公告)日：1994-04-05
申请号：US955274
申请日：1992-10-01
Applicant: David J. Rodini
Inventor： David J. Rodini
CPC classification number: D06P3/004
Abstract: PEKK fiber is dyed with a disperse dye in an organic dye carrier.
Abstract translation: PEKK纤维用分散染料染色在有机染料载体中。
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公开(公告)号：US4919869A
公开(公告)日：1990-04-24
申请号：US326443
申请日：1989-03-22
Applicant: Tony D. Zatkulak , David J. Rodini , James D. Hodge
Inventor： Tony D. Zatkulak , David J. Rodini , James D. Hodge
CPC classification number: D06P3/24 , D06M11/05 , Y10S264/71 , Y10S8/925
Abstract: A process for diffusing and subliming water-soluble and water-insoluble materials into never-dried, shrinkable aromatic polyamide fibers, using steam heated at certain controlled temperatures, within a specially designed treatment chamber and a process and apparatus for treating a tow of shrinkable material.
Abstract translation: 在特殊设计的处理室内使用在特定控制温度下加热的蒸汽将水溶性和水不溶性材料扩散和升华成未干燥，可收缩的芳族聚酰胺纤维的方法和用于处理可收缩材料丝束的方法和装置 。
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公开(公告)号：US11279800B2
公开(公告)日：2022-03-22
申请号：US14371443
申请日：2012-01-11
Applicant: Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
Inventor： Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
Abstract: The present invention concerns yarn comprising polymer, the polymer comprising imidazole groups, the yarn having a sulfur content of 0.01 to 3.0 percent by weight, based on weight of the yarn, the yarn having a tenacity of 30 cN/dtex (33.3 gpd) or higher.
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Patent Agency Ranking
公开(公告)号：US10240282B2
公开(公告)日：2019-03-26
申请号：US14371760
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Abstract: The present invention concerns methods for removing sulfur from yarn comprising the steps of: a) contacting never-dried polymeric yarn with an aqueous base, the polymer comprising imidazole groups and said polymer comprising sulfur atoms characterized as being in the form of sulfate anions; b) contacting the yarn with an aqueous acid comprising a halide; and c) rinsing the yarn.
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公开(公告)号：US09988514B2
公开(公告)日：2018-06-05
申请号：US14371742
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
CPC classification number: C08K3/30 , C08K2003/309 , D01D10/06 , D01F6/74 , D01F6/805 , D01F11/08 , Y10T428/249921
Abstract: The present invention concerns fiber made from a polymer comprising imidazole groups, fiber further having: i) a halide anion, the halide anion being present in an amount of 0.05 to 20.1 weight percent, based on weight of fiber; and ii) sulfur, wherein the sulfur is present in the fiber in an amount of 0.05 to 3 weight percent.
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28.发明授权公开(公告)号：US09464380B2
公开(公告)日：2016-10-11
申请号：US14371447
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion-containing polymeric-fiber with an halide-containing acid to displace at least a portion of the sulfate ions with halide anions; and b) rinsing the fiber to remove the displaced sulfate ions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）使从未干燥的含硫酸根阴离子的聚合物纤维与含卤化物的酸接触以置换至少一部分 硫酸根离子与卤化物阴离子; 和b）冲洗纤维以除去置换的硫酸根离子。
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29.发明授权公开(公告)号：US09284665B2
公开(公告)日：2016-03-15
申请号：US14371467
申请日：2012-01-11
Applicant: Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
Inventor： Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
CPC classification number: D01F6/805 , D01D10/06 , D10B2331/021
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion containing polymeric-fiber with an aqueous salt solution comprising halide anions to displace at least a portion of the sulfate anions with halide anions; and b) rinsing the fiber to remove displaced sulfate anions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）将含有聚合物纤维的未干燥硫酸根阴离子与含有卤化物阴离子的盐水溶液接触，以使至少一部分 具有卤化物阴离子的硫酸根阴离子; 和b）漂洗纤维以除去置换的硫酸根阴离子。
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30.发明申请PROCESS FOR PREPARING YARN DERIVED FROM ARAMID COPOLYMER FIBER HAVING LOW RESIDUAL SULFUR 有权用于制备具有低残留硫磺的芳族共聚物纤维制备纱线的方法公开(公告)号：US20150021812A1
公开(公告)日：2015-01-22
申请号：US14371444
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
CPC classification number: D01F8/16 , D01D5/06 , D01D10/06 , D01F6/74 , D01F6/805 , D01F11/08 , D10B2331/14
Abstract: The present invention concerns processes for producing a yarn comprising polymer comprising imidazole groups, the process having the following steps: (a) spinning a solution of polymer in sulfuric acid to give rise to a plurality of dope filaments; (b) coagulating the plurality of dope filaments into a multi-filament as-spun yarn; and (c) washing the as-spun multi-filament yarn with an aqueous acid comprising a halide or an aqueous salt comprising a halide or combination thereof.
Abstract translation: 本发明涉及生产包含咪唑基团的聚合物的纱线的方法，该方法具有以下步骤：（a）将聚合物溶液在硫酸中纺丝以产生多个涂料丝; （b）将多根纺丝原丝凝结成纺丝纱; 和（c）用包含卤化物或包含卤化物或其组合的盐水的含水酸洗涤初纺复丝纱线。
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