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公开(公告)号：US20150183697A1
公开(公告)日：2015-07-02
申请号：US14643607
申请日：2015-03-10
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Daniel C. Merkel , Konstantin A. Pokrovski , Haseh S. Tung , Haiyou Wang
CPC classification number: C07C17/395 , B01D3/009 , B01D3/10 , B01D11/04 , B01J19/123 , B01J23/44 , B01J27/10 , B01J27/138 , B01J2219/1203 , C07C17/25 , C07C17/383 , C07C21/18 , Y02P20/582 , C07C19/10
Abstract: The instant invention relates to a process and method for manufacturing 2,3,3,3-tetrafluoropropene by dehydrohalogenating a reactant stream of 2-chloro-1,1,1,2-tetrafluoropropane that is substantially free from impurities, particularly halogenated propanes, propenes, and propynes.
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公开(公告)号：US20140350309A1
公开(公告)日：2014-11-27
申请号：US14351688
申请日：2012-10-10
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Haiyou Wang , Hsueh Sung Tung , Daniel C. Merkel
IPC: C07C17/25
CPC classification number: C07C17/25 , C07C17/087 , C07C17/202 , C07C19/10 , C07C21/18
Abstract: The present invention relates, in part, to the discovery that the presence of impurities in a reactor for dehydrochlorinating HCFC-244bb to HFO-1234yf results in a reduced conversion rate and/or a selectivity changeover from HFO-1234yf to HCFO-1233xf. By substantially removing such impurities, it is shown that the conversion rate may be improved and selectivity to HFO-C 1234yf via dehydrochlorination of HCFC-244bb is also improved.
Abstract translation: 本发明部分涉及以下发现，即将HCFC-244bb脱氯化氢反应成HFO-1234yf的反应器中的杂质的存在导致从HFO-1234yf到HCFO-1233xf的转化率和/或选择性转换率降低。 通过基本上除去这些杂质，可以看出可以提高转化率，并且还提高了通过HCFC-244bb的脱氯化氢对HFO-C 1234yf的选择性。
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公开(公告)号：US20140303409A1
公开(公告)日：2014-10-09
申请号：US14348804
申请日：2012-09-29
Applicant: HONEYWELL INTERNATIONAL INC.
Inventor： Haiyou Wang , Hsueh Sung Tung
IPC: C07C17/25
CPC classification number: C07C19/12 , B01J27/10 , B01J27/12 , B01J27/138 , B01J35/0006 , C07B35/06 , C07C17/25 , C07C21/18
Abstract: The present invention relates, in part, to the discovery that the presence of HF in a HCFC-244bb feedstream in a reaction for the preparation of HFO-1234yf results in selectivity changeover from HFO-1234yf to HCFO-1233xf. By substantially removing HF, it is shown that the selectivity to HFO-1234yf via dehydrochlorination of HCFC-244bb is improved.
Abstract translation: 本发明部分地涉及在用于制备HFO-1234yf的反应中在HCFC-244bb原料流中存在HF导致从HFO-1234yf到HCFO-1233xf的选择性转换的发现。 通过基本上去除HF，显示了通过HCFC-244bb的脱氯化氢对HFO-1234yf的选择性得到改善。
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公开(公告)号：US20140275647A1
公开(公告)日：2014-09-18
申请号：US14206088
申请日：2014-03-12
Applicant: Honeywell International, Inc.
Inventor： Daniel C. Merkel , Hsueh Sung Tung , Haiyou Wang , Haluk Kopkalli , Yuon Chiu
CPC classification number: B01J19/24 , B01J4/002 , C07C17/206 , C07C17/25 , C07C21/18
Abstract: The invention relates to a process to prepare tetrahalopropenes, such as 2-chloro-3,3,3-trifluoropropene (1233xf). The process comprises atomizing a feed material, such as 1,1,2,3-tetrachloropropene (1230xa) and the like, and mixing it with superheated HF to form a vaporized composition of feed material and HF with substantially instantaneous contact with a vapor phase fluorination catalyst. The invention extends catalyst life and forestalls catalyst deactivation.
Abstract translation: 本发明涉及制备四卤代丙烯的方法，例如2-氯-3,3,3-三氟丙烯（1233xf）。 该方法包括将原料如1,1,2,3-四氯丙烯（1230xa）等进行雾化，并与过热HF混合以形成与气相基本上瞬时接触的原料和HF的蒸发组合物 氟化催化剂。 本发明延长了催化剂的寿命并阻止了催化剂的失活。
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公开(公告)号：US20140147343A1
公开(公告)日：2014-05-29
申请号：US14168475
申请日：2014-01-30
Applicant: Honeywell International Inc.
Inventor： Daniel C. Merkel , Hsueh Sung Tung , Konstantin A. Pokrovski , Haiyou Wang , Selma Bektesevic
IPC: B01D3/00
CPC classification number: B01D3/009 , C07C17/206 , C07C17/25 , C07C17/383 , Y02P20/582 , C07C21/18
Abstract: Disclosed is a method for the production of 1233xf comprising the continuous low temperature liquid phase reaction of 1,1,1,2,3-pentachloropropane and anhydrous HF, without the use of a catalyst, wherein the reaction takes place in one or more reaction vessels, each one in succession converting a portion of the original reactants fed to the lead reaction vessel and wherein the reactions are run in a continuous fashion.
Abstract translation: 公开了一种制备1233xf的方法，其包括1,1,1,2,3-五氯丙烷和无水HF的连续低温液相反应，不使用催化剂，其中反应在一个或多个反应 容器，每个连续地将一部分原始反应物转化成铅反应容器，其中反应以连续的方式运行。
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Patent Agency Ranking
公开(公告)号：US12281053B2
公开(公告)日：2025-04-22
申请号：US18534092
申请日：2023-12-08
Applicant: Honeywell International Inc.
Inventor： Haridasan K. Nair , Glenn Matthies , Rajiv Ratna Singh , Terris Yang , Haiyou Wang , Ryan J. Hulse , Rajiv Banavali
IPC: C07C17/20 , B01J27/224 , C07C17/35 , C07C19/16
Abstract: The present disclosure provides a process for producing trifluoroiodomethane, the process comprising providing a reactant stream comprising hydrogen iodide and at least one trifluoroacetyl halide selected from the group consisting of trifluoroacetyl chloride, trifluoroacetyl fluoride, trifluoroacetyl bromide, and combinations thereof, reacting the reactant stream in the presence of a first catalyst at a first reaction temperature from about 25° C. to about 400° C. to produce an intermediate product stream comprising trifluoroacetyl iodide, and reacting the intermediate product stream in the presence of a second catalyst at a second reaction temperature from about 200° C. to about 600° C. to produce a final product stream comprising the trifluoroiodomethane.
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公开(公告)号：US20250122136A1
公开(公告)日：2025-04-17
申请号：US18889319
申请日：2024-09-18
Applicant: Honeywell International Inc.
Inventor： Haiyou Wang , Gustavo Cerri , Jinhua Yao , Jennifer W. McClaine
IPC: C07C17/23 , B01J27/132 , C07C17/383
Abstract: The present disclosure provides a method for conversion of a mixture of high-boiling fluorinated components comprising 1,1,3,3-tetrachloro-1-fluoropropane (HCFC-241fa), 1,3,3-trichloro-1,1-difluoropropane (HCFC-242sfa), 1,1,3-trichloro-1,3-difluoropropane (HCFC-242fb), 3,3-dichloro-1,1,1-trifluoropropane (HCFC-243fa), 1,3-dichloro-1,1,3-trifluoropropane (HCFC-243fb), 3-chloro-1,1,1,3-tetrafluoropropane (HCFC-244fa), their isomers, and combinations thereof, to 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd). Heavy impurities, such as oligomers and other high boiling impurities, that are present may be purged during the process to prevent yield loss and reduction of catalyst efficacy.
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公开(公告)号：US12258357B2
公开(公告)日：2025-03-25
申请号：US18400050
申请日：2023-12-29
Applicant: Honeywell International Inc.
Inventor： Haiyou Wang , Haridasan K. Nair , Daniel C. Merkel , Selma Bektesevic , Terris Yang
IPC: C07F13/00
Abstract: The present disclosure provides a composition including trifluoroacetyl iodide, at least one organic impurity and at least one inorganic impurity. The at least one organic impurity includes at least one of: difluoroiodomethane, pentafluoroiodoethane, iodomethane, iodopropane, dichlorotetrafluoroethane, dichlorotrifluoroethane, trichlorotrifluoroethane, methyltrifluoroacetate, trifluoroacetic anhydride, difluorobutane and methyl propane. The at least one inorganic impurity includes at least one of: hydrogen iodide, hydrogen chloride, iodine and hydrogen triiodide.
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公开(公告)号：US20240376032A1
公开(公告)日：2024-11-14
申请号：US18660212
申请日：2024-05-09
Applicant: Honeywell International Inc.
Inventor： Richard D. Horwath , Gustavo Cerri , Benson May , Haiyou Wang
IPC: C07C17/25 , B01J23/26 , C07C17/383
Abstract: A method for reducing 1,1,1,2,2-pentafluoropropane (HFC-245cb) in a trans-1,3,3,3-tetrafluoropropene (HFO-1234ze(E)) manufacturing process including catalyst conditioning, temperature reduction, and contact time reduction. The method includes dehydrofluorinating 1,1,1,3,3-pentafluoropropane (HFC-245fa) with a catalyst mixture to produce a product mixture with HFO-1234ze(E) and HFC-245cb, and either incorporating a conditioned catalyst, using a lower temperature for the dehydrofluorination, or reducing the contact time for the dehydrofluorination to reduce the formation of HFC-245cb.
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公开(公告)号：US20240376031A1
公开(公告)日：2024-11-14
申请号：US18658341
申请日：2024-05-08
Applicant: Honeywell International Inc.
Inventor： Joshua Close , Pramod K.W. Harikumar Warrier , Justin Howard , Terris Yang , Haiyou Wang , Akbar Mahdavi-Shakib
IPC: C07C17/25 , C07C17/383 , C07C19/08 , C07C19/12
Abstract: An azeotrope or azeotrope-like composition consisting essentially of effective amounts of 1-chloro-1,1,2-trifluoroethane (HCFC-133b) and 1,1,2-trifluoroethane (HFC-143). Methods for separating the azeotrope or azeotrope-like composition and/or exploiting the composition in extractive and pressure swing distillation are also disclosed in connection with methods of manufacturing 1,1,2-trifluoroethane (HFC-143).
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