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公开(公告)号：US20240150267A1
公开(公告)日：2024-05-09
申请号：US18534092
申请日：2023-12-08
发明人： Haridasan K. Nair , Glenn Matthies , Rajiv Ratna Singh , Terris Yang , Haiyou Wang , Ryan J. Hulse , Rajiv Banavali
IPC分类号： C07C17/20 , B01J27/224 , C07C17/35
CPC分类号： C07C17/20 , B01J27/224 , C07C17/35 , C07C19/16
摘要： The present disclosure provides a process for producing trifluoroiodomethane, the process comprising providing a reactant stream comprising hydrogen iodide and at least one trifluoroacetyl halide selected from the group consisting of trifluoroacetyl chloride, trifluoroacetyl fluoride, trifluoroacetyl bromide, and combinations thereof, reacting the reactant stream in the presence of a first catalyst at a first reaction temperature from about 25° C. to about 400° C. to produce an intermediate product stream comprising trifluoroacetyl iodide, and reacting the intermediate product stream in the presence of a second catalyst at a second reaction temperature from about 200° C. to about 600° C. to produce a final product stream comprising the trifluoroiodomethane.
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公开(公告)号：US20230159415A1
公开(公告)日：2023-05-25
申请号：US17997262
申请日：2021-05-19
申请人： ZEON CORPORATION
发明人： Go MATSUURA
IPC分类号： C07C17/35
CPC分类号： C07C17/35
摘要： Provided is a production method that enables production of monofluoromethane by a gas phase flow method without using a catalyst. The method of producing monofluoromethane includes causing electrical discharge of a feedstock gas containing a fluorine-containing inorganic compound, a compound represented by formula 1: CH3—R (R is a hydrogen atom, a chlorine atom, a bromine atom, an iodine atom, or an organic group other than a hydrocarbon group), and an inert gas, while in a continuous flow state, and then causing continuous release to outside of an electrical discharge zone.
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公开(公告)号：US20220396536A1
公开(公告)日：2022-12-15
申请号：US17889496
申请日：2022-08-17
发明人： Haridasan K. Nair , Glenn Matthies , Rajiv Ratna Singh , Terris Yang , Haiyou Wang , Ryan J. Hulse , Rajiv Banavali
IPC分类号： C07C17/20 , C07C17/35 , B01J27/224
摘要： The present disclosure provides a process for producing trifluoroiodomethane, the process comprising providing a reactant stream comprising hydrogen iodide and at least one trifluoroacetyl halide selected from the group consisting of trifluoroacetyl chloride, trifluoroacetyl fluoride, trifluoroacetyl bromide, and combinations thereof, reacting the reactant stream in the presence of a first catalyst at a first reaction temperature from about 25° C. to about 400° C. to produce an intermediate product stream comprising trifluoroacetyl iodide, and reacting the intermediate product stream in the presence of a second catalyst at a second reaction temperature from about 200° C. to about 600° C. to produce a final product stream comprising the trifluoroiodomethane.
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公开(公告)号：US11440861B2
公开(公告)日：2022-09-13
申请号：US17295102
申请日：2019-11-25
申请人： BASF SE
发明人： Karsten Koerber , Michael Rack , Pascal Bindschaedler , Martin John McLaughlin , Birgit Gockel , Devendra Vyas , Sebastian Soergel
IPC分类号： C07C17/35 , B01J21/18 , B01J23/44 , C07C25/08 , C07C245/20 , C07C37/045 , C07C39/30 , C07C17/093
摘要： The invention relates to a process for the preparation of 5-bromo-1,3-dichloro-2-fluoro-benzene by diazotization and reduction of 6-bromo-2,4-dichloro-3-fluoro-aniline, which is obtained by bromination of 2,4-dichloro-3-fluoro-aniline, which is obtained by reduction of 1,3-dichloro-2-fluoro-4-nitro-benzene, and a process for preparing active compounds of formula V (Formula V) wherein the variables are defined in the specification by further transforming 5-bromo-1,3-dichloro-2-fluoro-benzene obtained from 2,4-dichloro-3-fluoro-aniline by the process according to the invention.
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公开(公告)号：US20220033330A1
公开(公告)日：2022-02-03
申请号：US17245459
申请日：2021-04-30
发明人： Emma Jayne HODGSON , Clare Mary Skae , Gary Lloyd , Claire Elizabeth McGuinness , Clive Robert Giddis , James Henry Murray
摘要： The present invention provides a process for preparing 3,3,3-trifluoropropene (1243zf), the process comprising: (a) fluorinating CCl3CH2CH2Cl (250fb) to produce a reaction product comprising CF3CH2CH2Cl (253fb) in the liquid phase in a first reactor, using HF as the fluorinating agent; and (b) (i) dehydrohalogenating 253fb to produce 1243zf in the vapour phase in the present of a catalyst in a second reactor; or (b)(ii) dehydrohalogenating 253fb to produce 1243zf in a second reactor, wherein the reaction product comprising 253fb produced in step (a) has subjected to one or more purification steps before step (b). The present invention also provides an azeotropic or near-azeotropic composition comprising HF and 253fb.
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公开(公告)号：US20210171423A1
公开(公告)日：2021-06-10
申请号：US17181479
申请日：2021-02-22
发明人： Haridasan K. Nair , Glenn Matthies , Rajiv Ratna Singh , Terris Yang , Haiyou Wang , Ryan J. Hulse , Rajiv Banavali
IPC分类号： C07C17/20 , C07C17/35 , B01J27/224
摘要： The present disclosure provides a process for producing trifluoroiodomethane, the process comprising providing a reactant stream comprising hydrogen iodide and at least one trifluoroacetyl halide selected from the group consisting of trifluoroacetyl chloride, trifluoroacetyl fluoride, trifluoroacetyl bromide, and combinations thereof, reacting the reactant stream in the presence of a first catalyst at a first reaction temperature from about 25° C. to about 400° C. to produce an intermediate product stream comprising trifluoroacetyl iodide, and reacting the intermediate product stream in the presence of a second catalyst at a second reaction temperature from about 200° C. to about 600° C. to produce a final product stream comprising the trifluoroiodomethane.
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公开(公告)号：US20200255360A1
公开(公告)日：2020-08-13
申请号：US16863026
申请日：2020-04-30
发明人： CLARE MARY SKAE , GARY LLOYD
摘要： The present invention provides a process for preparing 3,3,3-trifluoropropene (1243zf), the process comprising: (a) fluorinating CCI3CH2CH2CI (250fb) to produce a reaction product comprising CF3CH2CH2CI (253fb) in the liquid phase in a first reactor, using HF as the fluorinating agent; and (b) (i) dehydrohalogenating 253fb to produce 1243zf in the vapour phase in the presence of a catalyst in a second reactor; or (b) (ii) dehydrohalogenating 253fb to produce 1243zf in a second reactor, wherein the reaction product comprising 253fb produced in step (a) has subjected to one or more purification steps before step (b). The present invention also provides an azeotropic or near-azeotropic composition comprising HF and 253fb.
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公开(公告)号：US20200062679A1
公开(公告)日：2020-02-27
申请号：US16549412
申请日：2019-08-23
发明人： Haridasan K. Nair , Glenn Matthies , Rajiv Ratna Singh , Terris Yang , Haiyou Wang , Ryan J. Hulse , Rajiv Banavali
IPC分类号： C07C17/20 , B01J27/224 , C07C17/35
摘要： The present disclosure provides a process for producing trifluoroiodomethane, the process comprising providing a reactant stream comprising hydrogen iodide and at least one trifluoroacetyl halide selected from the group consisting of trifluoroacetyl chloride, trifluoroacetyl fluoride, trifluoroacetyl bromide, and combinations thereof, reacting the reactant stream in the presence of a first catalyst at a first reaction temperature from about 25° C. to about 400° C. to produce an intermediate product stream comprising trifluoroacetyl iodide, and reacting the intermediate product stream in the presence of a second catalyst at a second reaction temperature from about 200° C. to about 600° C. to produce a final product stream comprising the trifluoroiodomethane.
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公开(公告)号：US10454041B2
公开(公告)日：2019-10-22
申请号：US16079151
申请日：2017-01-24
申请人： Merck Patent GmbH
IPC分类号： H01L51/50 , H01L51/00 , C07D333/76 , C07C211/54 , C07C211/56 , C07C211/61 , C07D411/12 , C07D209/86 , C07D307/91 , C07C25/18 , C07C25/22 , C07C17/263 , C07C17/269 , C07C17/35
摘要： The present invention relates to a process to produce compounds of the formula (1) which are suitable for use in electronic devices, as well as to intermediate compounds of formula (Int-1) and compounds of formula (1-1) and (1-2) obtained via the process. These compounds are particularly suitable for use organic electroluminescent devices. The present invention also relate to electronic devices, which comprise these compounds.
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公开(公告)号：US20180222873A1
公开(公告)日：2018-08-09
申请号：US15946601
申请日：2018-04-05
发明人： Gary David Annis
IPC分类号： C07D261/04 , C07C17/35 , C07C45/45 , C07C45/70 , C07C49/80 , C07C49/813 , C07C67/343 , C07C205/45 , C07C209/74 , C07C231/12 , C07C231/14 , C07C235/84 , C07D213/40 , C07D231/12 , C07D231/14 , C07D231/16 , C07D249/08 , C07D249/10 , C07D277/28
CPC分类号： C07D261/04 , C07C17/35 , C07C25/13 , C07C45/455 , C07C45/70 , C07C49/80 , C07C49/813 , C07C67/343 , C07C205/45 , C07C209/74 , C07C231/12 , C07C231/14 , C07C235/84 , C07D213/40 , C07D231/12 , C07D231/14 , C07D231/16 , C07D249/08 , C07D249/10 , C07D277/28 , C07C69/94 , C07C69/76 , C07C211/56
摘要： Disclosed is a method for preparing a compound of Formula 1 wherein Q and Z are as defined in the disclosure comprising distilling water from a mixture comprising a compound of Formula 2, a compound of Formula 3, a base comprising at least one compound selected from the group consisting of alkaline earth metal hydroxides of Formula 4 wherein M is Ca, Sr or Ba, alkali metal carbonates of Formula 4a wherein M1 is Li, Na or K, 1,5-diazabicyclo[4.3.0]non-5-ene and 1,8-diazabicyclo[5.4.0]undec-7-ene, and an aprotic solvent capable of forming a low-boiling azeotrope with water. Also disclosed is a method for preparing a compound of Formula 2 comprising (1) forming a reaction mixture comprising a Grignard reagent derived from contacting a compound of Formula 5 wherein X is Cl, Br or I with magnesium metal or an alkylmagnesium halide in the presence of an ethereal solvent, and then (2) contacting the reaction mixture with a compound of Formula 6 wherein Y is OR11 or NR12R13, and R11, R12 and R13 are as defined in the disclosure. Further disclosed is a method for preparing a compound of Formula 7 wherein Q and Z are as defined in the disclosure, using a compound of Formula 1 characterized by preparing the compound of Formula 1 by the method disclosed above or using a compound of Formula 1 prepared by the method disclosed above.
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