PROCESS FOR PRODUCING HEXAHYDRO 1,3,5-TRINITRO-1,3,5-TRIAZINE AND OCTAHYDRO-1,3,5,7-TETRANITRO-1,3,5,7-TETRAZOCINE

    公开(公告)号:US20240132454A1

    公开(公告)日:2024-04-25

    申请号:US18348763

    申请日:2023-07-06

    申请人: James E. Phillips

    发明人: James E. Phillips

    IPC分类号: C07D257/02

    CPC分类号: C07D257/02

    摘要: Formation of methanoic acid, during the production of Hexahydro-1,3,5-trinitro-1,3,5-triazine and Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine via the legacy Bachmann nitrolysis process, is avoided when the workup is performed under neutralized, anhydrous conditions. The recovered anhydrous spent acid is used directly in successive nitrolysis batches with minimal processing. The yield and quality of the hexahydro-1,3,5-trinitro-1,3,5-triazine and octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine thus produced is equal to the yield and quality of the legacy process hexahydro-1,3,5-trinitro-1,3,5-triazine and octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine employing aqueous workup conditions.

    Execute at commit state update instructions, apparatus, methods, and systems
    23.
    发明授权
    Execute at commit state update instructions, apparatus, methods, and systems 有权
    在提交状态更新指令,设备,方法和系统上执行

    公开(公告)号:US09052890B2

    公开(公告)日:2015-06-09

    申请号:US12924311

    申请日:2010-09-25

    IPC分类号: G06F9/30 G06F9/40 G06F9/38

    摘要: An apparatus including an execution logic that includes circuitry to execute instructions, and an instruction execution scheduler logic coupled with the execution logic. The instruction execution scheduler logic is to receive an execute at commit state update instruction. The instruction execution scheduler logic includes at commit state update logic that is to wait to schedule the execute at commit state update instruction for execution until the execute at commit state update instruction is a next instruction to commit. Other apparatus, methods, and systems are also disclosed.

    摘要翻译: 一种包括执行逻辑的装置,包括执行指令的电路以及与执行逻辑耦合的指令执行调度器逻辑。 指令执行调度器逻辑是在提交状态更新指令下接收执行。 指令执行调度器逻辑包括提交状态更新逻辑,等待在提交状态更新指令执行执行,直到执行提交状态更新指令是下一个提交指令。 还公开了其他装置,方法和系统。

    DYNAMIC SELECTION OF EXECUTION STAGE
    24.
    发明申请
    DYNAMIC SELECTION OF EXECUTION STAGE 有权
    动态选择执行阶段

    公开(公告)号:US20110078486A1

    公开(公告)日:2011-03-31

    申请号:US12571379

    申请日:2009-09-30

    IPC分类号: G06F9/30 G06F1/04 G06F12/02

    CPC分类号: G06F9/3836 G06F9/3873

    摘要: Methods and apparatus relating to dynamic selection of execution stage are described. In some embodiments, logic may determine whether to execute an instruction at one of a plurality of stages in a processor. In some embodiments, the plurality of stages are to at least correspond to an address generation stage or an execution stage of the instruction. Other embodiments are also described and claimed.

    摘要翻译: 描述与执行阶段的动态选择相关的方法和装置。 在一些实施例中,逻辑可以确定是否在处理器中的多个级中的一个处执行指令。 在一些实施例中,多个阶段至少对应于该指令的地址生成阶段或执行阶段。 还描述和要求保护其他实施例。

    Method for depositing and etching ruthenium layers
    26.
    发明授权
    Method for depositing and etching ruthenium layers 失效
    沉积和蚀刻钌层的方法

    公开(公告)号:US07129170B2

    公开(公告)日:2006-10-31

    申请号:US11200073

    申请日:2005-08-10

    IPC分类号: H01L21/44

    摘要: The present invention provides a method for purifying ruthenium sources to obtain high purity ruthenium metal and form a ruthenium metal pattern on a semiconductor substrate without the need for high temperature processing or a complex series of wet processes. A gas stream including ozone (O3) is brought into contact with a ruthenium source in one or more reaction vessels to form ruthenium tetraoxide (RuO4), a compound that is a gas at the reaction conditions. The ruthenium tetraoxide, along with unreacted ozone and the remainder of the gas stream is then fed into a collection vessel where the gaseous ruthenium tetraoxide is reduced to form a ruthenium dioxide (RuO2) layer on a semiconductor substrate. The deposited ruthenium dioxide is then reduced, preferably with hydrogen, to produce highly pure ruthenium metal that may be, in turn, patterned and dry etched using ozone as an etchant gas.

    摘要翻译: 本发明提供一种用于纯化钌源以获得高纯度钌金属并在半导体衬底上形成钌金属图案的方法,而不需要高温处理或复杂的一系列湿法。 使包含臭氧(O 3 3 N)的气流与一个或多个反应容器中的钌源接触以形成四氧化钌(RuO 4 S 4),其为化合物 反应条件下的气体。 然后将四氧化钌,以及未反应的臭氧和气流的其余部分进料到收集容器中,在该收集容器中,气态钌四氧化物被还原以在半导体衬底上形成二氧化钌(RuO 2 N 2)层 。 然后沉积的二氧化钌优选用氢气还原,以产生高纯度的钌金属,其可以使用臭氧作为蚀刻剂气体进行图案化和干蚀刻。

    Method for purifying ruthenium and related processes
    27.
    发明授权
    Method for purifying ruthenium and related processes 有权
    钌的纯化方法及相关工艺

    公开(公告)号:US06458183B1

    公开(公告)日:2002-10-01

    申请号:US09655307

    申请日:2000-09-05

    IPC分类号: C01G5500

    摘要: The present invention provides a method for purifying ruthenium sources to obtain high purity ruthenium metal without the need for high temperature processing, expensive reagents, complex series of wet processes, or expensive equipment. According to the present invention, a gas stream including ozone (O3) is brought into contact with a ruthenium source, such as a commercial ruthenium metal sponge, in one or more reaction vessels. The ozone reacts with the ruthenium present in the ruthenium source to form ruthenium tetraoxide (RuO4), a compound that is a gas at the reaction conditions. The ruthenium tetraoxide, along with unreacted ozone and the remainder of the gas stream is then fed into a collection vessel where a major portion of the gaseous ruthenium tetraoxide is thermally reduced to form ruthenium dioxide (RuO2) deposits within the collection vessel. The deposited ruthenium dioxide is then reduced, preferably with hydrogen, to produce highly pure ruthenium metal that is, in turn removed from the collection vessel.

    摘要翻译: 本发明提供一种用于纯化钌源以获得高纯度钌金属而不需要高温处理,昂贵的试剂,复杂系列的湿法或昂贵的设备的方法。 根据本发明,在一个或多个反应容器中,使包含臭氧(O 3)的气流与诸如市售的钌金属海绵等钌源接触。 臭氧与钌源中存在的钌反应形成四氧化钌(RuO 4),RuO 4是在反应条件下为气体的化合物。 然后将四氧化钌,以及未反应的臭氧和剩余的气流进料到收集容器中,其中大部分气态四氧化钌被热还原以在收集容器内形成二氧化钌(RuO 2)沉积物。 然后沉积的二氧化钌优选用氢气还原,以产生高纯度的钌金属,其又从收集容器中除去。

    Fourier transform molecular spectrometer
    28.
    发明授权
    Fourier transform molecular spectrometer 失效
    傅里叶变换分子光谱仪

    公开(公告)号:US5233190A

    公开(公告)日:1993-08-03

    申请号:US797462

    申请日:1991-11-22

    IPC分类号: G01R33/64 H01J49/38

    CPC分类号: G01R33/64 H01J49/38

    摘要: A molecular spectrometer is provided that performs Fourier analysis utilizing the discrete Fourier Transform on a digitized time domain waveform that relates to the composition of a sample. Digitized reference waveforms are employed to permit the instrument to limit its analysis to frequencies of interest and thereby increase the rapidity of the analysis. Data at differing frequencies can be resolved at independent resolutions, and the instrument can analyze spectroscopic data in real time.

    摘要翻译: 提供了一种分子光谱仪,其利用与样品组成相关的数字化时域波形上的离散傅里叶变换进行傅立叶分析。 数字化参考波形用于允许仪器将其分析限制到感兴趣的频率,从而增加分析的快速性。 不同频率的数据可以独立分辨率解析,仪器可以实时分析光谱数据。

    Corn unit for combine
    29.
    发明授权
    Corn unit for combine 失效
    玉米单位组合

    公开(公告)号:US4548213A

    公开(公告)日:1985-10-22

    申请号:US639940

    申请日:1984-08-13

    IPC分类号: A01F12/44 B07B1/04 B07B1/46

    CPC分类号: A01F12/44 Y02P60/142

    摘要: A device for converting a conventional combine into a unit which will crush and recover corn cobs as well as recover shelled corn comprising a flat perforated metal element which will replace the conventional chaffer and sieve in the final cleaning mechanism of the combine, the element having a plurality of fins protruding above the upper surface thereof adapted to channel and direct the flow of corn stocks and chaff thereover, the holes being of a size sufficient to allow the passage of corn cob particles therethrough.

    摘要翻译: 一种用于将常规组合物转化为将粉碎和回收玉米芯的单元的装置,以及回收包含扁平穿孔金属元素的脱壳玉米,其将替代在组合物的最终清洁机构中的常规气味和筛子,该元件具有 在其上表面上突出的多个翅片,其适于引导和引导其上的玉米块和谷壳的流动,该孔的尺寸足以允许玉米芯颗粒通过其中。