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21.发明授权Automated on-line evaporating light scattering detection to quantify isolated fluid sample compounds in microtiter plate format 失效自动在线蒸发光散射检测，以微量滴定板格式定量分离的液体样品化合物公开(公告)号：US06426006B1
公开(公告)日：2002-07-30
申请号：US09710363
申请日：2000-11-08
IPC分类号： B01D1508
CPC分类号： G01N30/82 , B01J2219/00315 , B01J2219/00587 , B01J2219/00707 , C40B60/14 , G01N30/7266 , G01N30/74 , G01N30/78 , G01N21/4133 , G01N30/84 , G01N30/10
摘要： Single pass methods and systems for measuring the total masses of individual compounds present in fluid samples in real time, and particularly for fluid samples prepared in microtiter plate format are provided. Individual compounds are isolated by fluid separation column (14). Portions of the individual compounds isolated by column (14) are analyzed by mass spectrometer (16), which determines their concentration on the basis of their molecular weights, and an evaporative light scattering detector (24), (which determines the total masses of each of the isolated compounds passing therethrough). Total collected masses of the individual compounds are calculated by determining the amount and portion of the isolated compounds diverted into evaporative light scattering detector (24) during a period of fraction collection.
摘要翻译： 提供用于实时测量流体样品中存在的各种化合物的总质量的单程方法和系统，特别是用于以微量滴定板形式制备的流体样品。 单独的化合物通过流体分离柱（14）分离。 通过柱（14）分离的各个化合物的部分通过质谱仪（16）进行分析，质谱仪（16）根据其分子量确定其浓度，以及蒸发光散射检测器（24）（其确定每个化合物的总质量 的分离的化合物通过）。 通过确定在馏分收集期间转移到蒸发光散射检测器（24）中的分离化合物的量和部分来计算单个化合物的总收集质量。
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22.发明授权Automated on-line evaporating light scattering detection to quantify isolated fluid sample compounds in microtiter plate format 失效自动在线蒸发光散射检测，以微量滴定板格式定量分离的液体样品化合物公开(公告)号：US06210571B1
公开(公告)日：2001-04-03
申请号：US09415541
申请日：1999-10-08
IPC分类号： B01D1508
CPC分类号： G01N30/82 , B01J2219/00315 , B01J2219/00587 , B01J2219/00707 , C40B60/14 , G01N30/7266 , G01N30/74 , G01N30/78 , G01N21/4133 , G01N30/84 , G01N30/10
摘要： Single pass methods and systems for measuring the total masses of individual compounds present in fluid samples in real time, and particularly for fluid samples prepared in microtiter plate format are provided. Individual compounds are isolated by fluid separation column (14). Portions of the individual compounds isolated by column (14) are analyzed by mass spectrometer (16), which determines their concentration on the basis of their molecular weights, and an evaporative light scattering detector (24), (which determines the total masses of each of the isolated compounds passing therethrough). Total collected masses of the individual compounds are calculated by determining the amount and portion of the isolated compounds diverted into evaporative light scattering detector (24) during a period of fraction collection.
摘要翻译： 提供用于实时测量流体样品中存在的各种化合物的总质量的单程方法和系统，特别是用于以微量滴定板形式制备的流体样品。 单独的化合物通过流体分离柱（14）分离。 通过柱（14）分离的各个化合物的部分通过质谱仪（16）进行分析，质谱仪（16）根据其分子量确定其浓度，以及蒸发光散射检测器（24）（其确定每个化合物的总质量 的分离的化合物通过）。 通过确定在馏分收集期间转移到蒸发光散射检测器（24）中的分离化合物的量和部分来计算单个化合物的总收集质量。
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23.发明授权Automated on-line evaporation light scattering detection to quantify isolated fluid sample compounds in microtiter plate format 失效自动在线蒸发光散射检测，以微量滴定板格式定量分离的液体样品化合物
公开(公告)号：US06077438A
公开(公告)日：2000-06-20
申请号：US219083
申请日：1998-12-22
IPC分类号： G01N27/62 , B01D15/08 , B01J3/00 , C40B60/14 , G01N30/02 , G01N30/72 , G01N30/74 , G01N30/78 , G01N30/80 , G01N30/82 , G01N30/84 , G01N37/00
CPC分类号： G01N30/82 , B01J2219/00315 , B01J2219/00587 , B01J2219/00707 , C40B60/14 , G01N30/7266 , G01N30/74 , G01N30/78
摘要： Single pass methods and systems for measuring the total masses of individual compounds present in fluid samples in real time, and particularly for fluid samples prepared in microtiter plate format are provided. Individual compounds are isolated by fluid separation column (14). Portions of the individual compounds isolated by column (14) are analyzed by mass spectrometer (16), which determines their concentration on the basis of their molecular weights, and an evaporative light scattering detector (24), (which determines the total masses of each of the isolated compounds passing therethrough). Total collected masses of the individual compounds are calculated by determining the amount and portion of the isolated compounds diverted into evaporative light scattering detector (24) during a period of fraction collection.
摘要翻译： 提供用于实时测量流体样品中存在的各种化合物的总质量的单程方法和系统，特别是用于以微量滴定板形式制备的流体样品。 单独的化合物通过流体分离柱（14）分离。 通过柱（14）分离的各个化合物的部分通过质谱仪（16）进行分析，质谱仪（16）根据其分子量确定其浓度，以及蒸发光散射检测器（24）（其确定每个化合物的总质量 的分离的化合物通过）。 通过确定在馏分收集期间转移到蒸发光散射检测器（24）中的分离化合物的量和部分来计算单个化合物的总收集质量。
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公开(公告)号：US5348940A
公开(公告)日：1994-09-20
申请号：US936434
申请日：1992-09-03
CPC分类号： C07K7/56 , A61K38/00 , Y10S930/27
摘要： Certain propionitrile compounds which have a cyclohexapeptidyl nucleus and which are found to have antibiotic activity with physical properties suitable for use in therapeutic compositions are described. A novel process for their preparation is also described. ##STR1##
摘要翻译： 描述了具有环己肽基核并且被发现具有适合用于治疗组合物的物理性质的抗生素活性的某些丙腈化合物。 还描述了其制备的新方法。 （一）
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