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89 条记录 (耗时 0.022 秒)

    Process for the preparation of acyloxybenzenesulfonic acids and their salts
    33.
    发明授权
    Process for the preparation of acyloxybenzenesulfonic acids and their salts 失效
    制备乙酰苯二酚酸及其盐的方法

    公开(公告)号：US5100588A

    公开(公告)日：1992-03-31

    申请号：US154057

    申请日：1988-02-09

    申请人： Fritz-Feo Grabley ,  Gerd Reinhardt ,  Roland Steinl

    发明人： Fritz-Feo Grabley ,  Gerd Reinhardt ,  Roland Steinl

    IPC分类号： C07C309/42 ,  C07C20060101 ,  C07C67/00 ,  C07C301/00 ,  C07C303/02 ,  C07C303/04 ,  C07C303/06 ,  C07C303/14 ,  C07C303/30 ,  C07C303/32 ,  C07C309/58 ,  C11D1/22 ,  C11D3/34

    CPC分类号： C07C309/00

    摘要： The process for the preparation of acyloxybenzenesulfonic acids of the general formula ##STR1## in which R denotes a (C.sub.1 -C.sub.17)-alkyl or (C.sub.2 -C.sub.17)-alkenyl radical, or alkali metal, alkaline earth metal or ammonium salts thereof, is carried out in the following stages: (a) sulfonation of phenol, (b) heat treatment of the phenolsulfonic acid formed as the intermediate product, (c) esterification of the phenolsulfonic acid and, if appropriate, (d) neutralization of the resulting (C.sub.2 -C.sub.18)-acyloxybenzenesulfonic acid. As a result of the incorporation of stage (b), the process affords products in which the proportion of the 1,4-isomer compared with the 1,2-isomer is markedly increased, as a result of which these products can be used, in particular, as perborate activators in detergents.

    摘要翻译： 其中R表示（C1-C17） - 烷基或（C2-C17） - 烯基或其碱金属，碱土金属或铵盐的通式为“IMAGE”的酰氧基苯磺酸的制备方法为 在以下阶段进行：（a）苯酚的磺化，（b）作为中间产物形成的酚磺酸的热处理，（c）苯酚磺酸的酯化，如果合适的话，（d）中和所得的（ C2-C18） - 酰氧基苯磺酸。 作为阶段（b）的结合，该方法提供了与1,2-异构体相比的1,4-异构体的比例显着增加的产物，由此可以使用这些产物， 特别是作为洗涤剂中的过硼酸盐活化剂。

    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane metal complexes
    34.
    发明授权
    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane metal complexes 有权
    制备3,7-二氮杂双环[3.3.1]壬烷金属络合物的方法

    公开(公告)号：US08846921B2

    公开(公告)日：2014-09-30

    申请号：US13877567

    申请日：2011-10-06

    申请人： Christian Sidot ,  Audrey Caron ,  Miriam Ladwig ,  Gerd Reinhardt

    发明人： Christian Sidot ,  Audrey Caron ,  Miriam Ladwig ,  Gerd Reinhardt

    IPC分类号： C07F15/02 ,  C07F13/00

    CPC分类号： C07F15/02 ,  C07F13/00 ,  C07F13/005 ,  C07F15/025

    摘要： The invention relates to a method for producing metal complexes of formula (2) [MaLxXn]Ym (2), where M is a metal from the group consisting of Mn(II), Mn(III), Mn(IV), Fe(II), Fe(III) or Fe(IV), X is a coordinating compound selected from mono-, bi- or tri-charged anions or neutral molecules which can coordinate to a metal in mono-, bi- or tri-dentate form, Y represents a non-coordinating counter-ion which ensures charge equalization of the complex, L represents a ligand of formula (1) or the protonized or de-protonized form thereof, and a, x, n, m, R, R1, R2, R3 and z have the meanings described in claim 1. Said method is characterized in that the reaction of one or more ligands of formula (1) with an iron salt or manganese salt is carried out in an acetone/water mixture in a temperature range from 0 to 50° C. and for this purpose a solution or a suspension of the one or more ligands of formula (1) in acetone is brought in contact with an aqueous metal salt solution of the iron salt or manganese salt in the temperature range in which the reaction takes place.

    摘要翻译： 本发明涉及一种制备式（2）[MaLxXn] Ym（2）的金属配合物的方法，其中M是由Mn（II），Mn（III），Mn（IV），Fe（ II），Fe（III）或Fe（IV），X是选自单，双或三电荷阴离子或中性分子的配位化合物，其可以以单，双或三齿形式与金属配位 ，Y表示非配位抗衡离子，其确保络合物的电荷均衡，L表示式（1）的配体或其质子化或去质子化形式，和a，x，n，m，R，R 1， R2，R3和z具有权利要求1所述的含义。所述方法的特征在于，式（1）的一种或多种配体与铁盐或锰盐的反应在丙酮/水混合物中在温度 范围为0至50℃，为此目的，将式（1）的一种或多种配体在丙酮中的溶液或悬浮液与铁盐水溶液的金属盐溶液接触 r锰盐在发生反应的温度范围内。

    Method For Isolating Concentrated Paraffin Sulfonic Acids
    35.
    发明申请
    Method For Isolating Concentrated Paraffin Sulfonic Acids 有权
    分离浓缩石蜡磺酸的方法

    公开(公告)号：US20100087674A1

    公开(公告)日：2010-04-08

    申请号：US12598229

    申请日：2008-04-29

    申请人： Gerd Reinhardt ,  Peter Newmann ,  Lars Cuypers

    发明人： Gerd Reinhardt ,  Peter Newmann ,  Lars Cuypers

    IPC分类号： C07C309/00

    CPC分类号： C07C303/44 ,  C07C303/14 ,  C07C309/04

    摘要： The invention relates to a method for isolating concentrated paraffin sulfonic acids from reaction mixtures that are produced during the sulfoxidation of n-paraffins, from which a major part of the sulfuric acid and the paraffin was removed by phase separation and which contain, in addition to the free paraffin sulfonic acids, n-paraffins, water and optionally minor amounts of sulfuric acids. The method according to the invention is characterized by removing paraffin and optionally residual water by vacuum distillation. The paraffin sulfonic acids obtained by distillation have a content of more than 85% by weight of the active substance. The material is pale, odorless and low in sulfuric acid and paraffin.

    摘要翻译： 本发明涉及一种从正链烷烃的亚磺氧化反应中产生的反应混合物中分离浓缩的链烷磺酸的方法，其中大部分硫酸和石蜡通过相分离从其中除去，除了含有 游离的链烷烃磺酸，正链烷烃，水和任选的少量硫酸。 根据本发明的方法的特征在于通过真空蒸馏除去石蜡和任选的残余水。 通过蒸馏获得的链烷磺酸含量大于活性物质的85重量％。 该材料为浅灰色，无臭，硫酸和石蜡含量低。

    Use Of Aminoacetones And Salts Thereof As Bleaching Boosters For Peroxygen Compounds
    36.
    发明申请
    Use Of Aminoacetones And Salts Thereof As Bleaching Boosters For Peroxygen Compounds 审中-公开
    使用氨基丙酮及其盐作为过氧化合物的漂白助剂

    公开(公告)号：US20090289221A1

    公开(公告)日：2009-11-26

    申请号：US12376423

    申请日：2007-07-31

    申请人： Gerd Reinhardt ,  Georg Borchers ,  Michael Seebach

    发明人： Gerd Reinhardt ,  Georg Borchers ,  Michael Seebach

    IPC分类号： C11D3/395

    CPC分类号： C11D3/392 ,  C11D3/3917 ,  C11D3/3927 ,  C11D17/0034

    摘要： The use is claimed of aminoacetones or salts thereof of the general formulae (I) and (II) in which R1 and R2 are each independently hydrogen, C1-C22-alkyl, C2-C22-alkenyl, phenyl or C5-C8-cycloalkyl, or R1 and R2, together with the nitrogen atom, form a 5-, 6- or 7-membered ring system, X′ is anion, for example chloride, bromide, iodide, toluenesulfonate, benzenesulfonate, cumenesulfonate, mesitylsulfonate, sulfate, hydrogensulfate, acetate, fatty acid anion or anion of polycarboxylates, as a bleaching booster for inorganic peroxygen compounds in the pH range from 7 to 9.

    摘要翻译： 要求使用通式（I）和（II）的氨基丙酮或其盐，其中R 1和R 2各自独立地为氢，C 1 -C 22 - 烷基，C 2 -C 22 - 烯基，苯基或C 5 -C 8 - 环烷基， 或R 1和R 2与氮原子一起形成5-，6-或7-元环体系，X'是阴离子，例如氯化物，溴化物，碘化物，甲苯磺酸盐，苯磺酸盐，磺酸盐，月桂基磺酸盐，硫酸盐，硫酸氢盐， 乙酸盐，脂肪酸阴离子或多羧酸盐阴离子，作为无机过氧化合物的漂白助剂，pH范围为7至9。

    Liquid bleaching composition components comprising amphiphilic polymers
    37.
    发明授权
    Liquid bleaching composition components comprising amphiphilic polymers 有权
    包含两亲聚合物的液体漂白组合物组分

    公开(公告)号：US07109155B2

    公开(公告)日：2006-09-19

    申请号：US10727770

    申请日：2003-12-04

    申请人： Gerd Reinhardt ,  Irina Geiger ,  Matthias Loeffler ,  Roman Morschhaeuser

    发明人： Gerd Reinhardt ,  Irina Geiger ,  Matthias Loeffler ,  Roman Morschhaeuser

    IPC分类号： C11D17/08 ,  C11D9/42 ,  C11D3/37 ,  C11D3/395 ,  C11D7/54

    CPC分类号： C11D3/37 ,  C11D3/3719 ,  C11D3/3776 ,  C11D3/378 ,  C11D3/3947

    摘要： Liquid bleaching composition components are claimed which comprise 1) amphiphilic copolymers which include structural units which are derived from a) acryloyldimethyltauric acid in free, partially neutralized or completely neutralized form with mono- or divalent inorganic or organic cations and b) at least one hydrophobic comonomer based on ethylenically unsaturated polyalkylene alkoxylates and optionally c) further at least monovinylically unsaturated comonomers different from a) and b), and 2) at least one bleach activator, bleach catalyst or oxygen transfer agent.

    摘要翻译： 要求保护液体漂白组合物组分，其包含1）两亲共聚物，其包括衍生自a）丙烯酰基二甲基牛磺酸的游离，部分中和或完全中和形式的单或二价无机或有机阳离子的结构单元，和b）至少一种疏水性共聚单体 基于烯键式不饱和聚亚烷基烷氧基化物和任选地c）至少一种不同于a）和b）的单乙烯基不饱和共聚单体，和2）至少一种漂白活化剂，漂白催化剂或氧转移剂。

    Ammonium nitriles and the use thereof as hydrophobic bleaching activators
    38.
    发明授权
    Ammonium nitriles and the use thereof as hydrophobic bleaching activators 失效
    腈类腈及其作为疏水性漂白活化剂的用途

    公开(公告)号：US07015185B2

    公开(公告)日：2006-03-21

    申请号：US10486939

    申请日：2003-03-12

    申请人： Michael Seebach ,  Gerd Reinhardt

    发明人： Michael Seebach ,  Gerd Reinhardt

    IPC分类号： C11D1/00 ,  C11D3/26 ,  C11D3/395

    CPC分类号： C11D3/3925 ,  C07C255/25

    摘要： The invention relates to ammonium nitriles of general formula (I), wherein the radicals R3, R4, R5 and X− have the meaning as cited in the description and R1 and R2 respectively represent individually a straight or branched chained C5–C24-alkyl, alkenyl or alkylether group. The inventive compounds are used as bleaching activators in washing, cleaning, and disinfective agents and in textile and paper bleaching.

    摘要翻译： 本发明涉及通式（I）的铵腈，其中R 3，R 4，R 5和X 5， - 具有在说明书中引用的含义，R 1和R 2分别独立地表示直链或支链的C 5 - -C 24 - 烷基，烯基或烷基醚基。 本发明化合物用作洗涤，清洁和消毒剂以及织物和纸张漂白中的漂白活化剂。

    Use of transition metal complexes as bleach catalysts in laundry detergents and cleaning compositions
    39.
    发明申请
    Use of transition metal complexes as bleach catalysts in laundry detergents and cleaning compositions 失效
    过渡金属配合物作为漂白催化剂在衣物洗涤剂和清洁组合物中的应用

    公开(公告)号：US20050209120A1

    公开(公告)日：2005-09-22

    申请号：US11041468

    申请日：2005-01-24

    申请人： Gerd Reinhardt ,  Ekaterina Jonas

    发明人： Gerd Reinhardt ,  Ekaterina Jonas

    IPC分类号： C07D257/02 ,  C07F13/00 ,  C07F15/02 ,  C11D3/16 ,  C11D3/28 ,  C11D3/39 ,  C11D3/395 ,  C11D17/00

    CPC分类号： C11D3/168 ,  C11D3/3932

    摘要： The use is claimed of transition metal complexes of the formula (I) [M(L)Yn]Xm   (I) where M is a metal atom from the group of Mn and Fe, L is a ligand of the general formula (II) or (III) where R1, R2, R3 and R4 are the same or different and are each H, C1-C8-alkyl or C6-C12-alkaryl; X and Y are each an uncharged or anionic ligand from the group of CH3CN, chloride, bromide, nitrate, perchlorate, sulfate, citrate, hexafluorophosphate, trifluoromethanesulfonate, tetrafluoroborate, tetraphenylborate or an anion of organic acids having C1-C22 carbon atoms, n and m are each a number from 0 to 4 as bleach catalysts in laundry detergents and cleaning compositions.

    摘要翻译： 要求使用式（I）的过渡金属络合物<？in-line-formula description =“In-line Formulas”end =“lead”？> [M（L）Y （I）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中M是来自Mn和Fe，L的金属原子 是通式（II）或（III）的配体，其中R 1，R 2，R 3和R 4相同或不同，并且各自为H，C 1 -C 8 > - 烷基或C 6 -C 12 - 烷芳基; X和Y各自是来自CH 3 N，CN，氯化物，溴化物，硝酸盐，高氯酸盐，硫酸盐，柠檬酸盐，六氟磷酸盐，三氟甲磺酸盐，四氟硼酸盐，四苯基硼酸盐或有机酸阴离子的不带电荷或阴离子配体 具有C 1 -C 22碳原子，n和m各自为0至4的数，作为洗衣洗涤剂和清洁组合物中的漂白催化剂。