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公开(公告)号:US20200270519A1
公开(公告)日:2020-08-27
申请号:US16801626
申请日:2020-02-26
Applicant: NICHIA CORPORATION
Inventor: Takayuki SHINOHARA , Hiroyuki WATANABE , Shoji HOSOKAWA
Abstract: Provided is a method for producing a nitride fluorescent material including: preparing a raw material mixture including a hydride containing at least one first alkaline earth metal element, at least one compound containing at least one second alkaline earth metal element and selected from an amide compound and an imide compound, a compound containing europium, a compound containing aluminum, and a compound containing silicon, wherein at least one of the compound containing europium, the compound containing aluminum, and the compound containing silicon is a nitride; and subjecting the raw material mixture to a heat treatment to obtain the nitride fluorescent material.
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32.
公开(公告)号:US20190330526A1
公开(公告)日:2019-10-31
申请号:US16508974
申请日:2019-07-11
Applicant: NICHIA CORPORATION
Inventor: Shozo TAKETOMI , Shoji HOSOKAWA , Tomokazu YOSHIDA , Kazuya NISHIMATA
Abstract: Provided are a method of producing an aluminate fluorescent material, an aluminate fluorescent material and a light emitting device. The production method includes heat-treating a mixture prepared by mixing a compound containing at least one alkaline earth metal element selected from the group consisting of Ba, Sr and Ca, a Mg-containing compound not acting as a flux, a Mn-containing compound, an Al-containing compound, a first flux containing at least one alkali metal element selected from the group consisting of Na, K, Rb and Cs, and a Mg-containing second flux to give an aluminate fluorescent material.
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公开(公告)号:US20190305193A1
公开(公告)日:2019-10-03
申请号:US16369046
申请日:2019-03-29
Applicant: NICHIA CORPORATION
Inventor: Kenichi AOYAGI , Takashi KAIDE , Takuya NAKABAYASHI , Tetsuya ISHIKAWA , Shoji HOSOKAWA
Abstract: A wavelength converting member comprising a first wavelength converting layer containing: a first fluorescent material having a light emission peak wavelength in a range of 620 nm or more and 660 nm or less; a second fluorescent material having a light emission peak wavelength in a range of 510 nm or more and 560 nm or less; and a resin, wherein the average particle diameter, as measured according to a Fisher Sub-Sieve Sizer method, of the first fluorescent material is in a range of 2 μm or more and 30 μm or less, wherein the second fluorescent material comprises a β-SiAlON fluorescent material, the circularity of the β-SiAlON fluorescent material is 0.7 or more, and the volume average particle diameter, as measured according to a laser diffraction scattering particle size distribution measuring method, of the β-SiAlON fluorescent material is in a range of 2 μm or more and 30 μm or less, and wherein the thickness of the first wavelength converting layer is in a range of 50 μm or more and 200 μm or less.
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34.
公开(公告)号:US20190153311A1
公开(公告)日:2019-05-23
申请号:US16233545
申请日:2018-12-27
Applicant: NICHIA CORPORATION
Inventor: Tomokazu YOSHIDA , Kazuya NISHIMATA , Shoji HOSOKAWA
Abstract: Provided is an aluminate fluorescent material having a high emission intensity and having a composition containing a first element that contains one or more of Ba and Sr, and a second element that contains Mg and Mn. In the composition, when a molar ratio of Al is 10, a total molar ratio of the first element is a parameter a, a total molar ratio of the second element is a parameter b, a molar ratio of Sr is a product of a parameter m and the parameter a, a molar ratio of Mn is a product of a parameter n and the parameter b. The parameters a and b satisfy 0.5
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公开(公告)号:US20190109266A1
公开(公告)日:2019-04-11
申请号:US16201141
申请日:2018-11-27
Applicant: NICHIA CORPORATION
Inventor: Shoji HOSOKAWA , Kazuya NISHIMATA , Tomokazu YOSHIDA
IPC: H01L33/50 , G02F1/13357 , C09K11/64 , C09K11/77 , C09K11/08
Abstract: Provided is a light-emitting device including a light-emitting element having a peak emission wavelength in a range of from 400 nm to 470 nm, and a fluorescent member including a first fluorescent material including an aluminate that contains Mg, Mn, and at least one alkali earth metal selected from the group consisting of Ba, Sr, and Ca, a second fluorescent material having a different composition from the first fluorescent material, and a third fluorescent material. The first, second and third fluorescent materials have a peak emission wavelength in a range of from 510 nm to 525 nm, from 510 nm to 550 nm, and from 620 nm to 670 nm, respectively.
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公开(公告)号:US20180171222A1
公开(公告)日:2018-06-21
申请号:US15843544
申请日:2017-12-15
Inventor: Naoto HIROSAKI , Takashi TAKEDA , Shiro FUNAHASHI , Takayuki SHINOHARA , Shoji HOSOKAWA
CPC classification number: C09K11/7734 , C01B21/0821 , C01F17/0012 , C01P2002/72 , C01P2002/76 , C01P2002/77 , C01P2004/61 , C01P2006/60 , C09K11/0883 , H01L33/502
Abstract: Provided are a fluorescent material including a high light emission intensity and a light emitting device using the same. The present fluorescent material includes at least an A element, a M element, a D element, a E element, and an X element, wherein the A element is at least one element selected from the group consisting of Sr, Mg, Ca, and Ba; the M element is at least one element selected from the group consisting of Eu, Mn, Ce, Pr, Nd, Sm, Tb, Dy, and Yb; the D element is at least one element selected from the group consisting of Si, Ge, Sn, Ti, Zr, and Hf, the E element is at least one element selected from the group consisting of Al, B, Ga, In, Sc, Y, and La; the X element is at least one element selected from the group consisting of O, N, and F; and a molar ratio of the M element to the sum of the A element and the M element [M/(A+M)] is 0.06 or less.
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公开(公告)号:US20180090647A1
公开(公告)日:2018-03-29
申请号:US15715841
申请日:2017-09-26
Applicant: NICHIA CORPORATION
Inventor: Shoji HOSOKAWA , Kazuya NISHIMATA , Tomokazu YOSHIDA
IPC: H01L33/50 , G02F1/1335
CPC classification number: H01L33/504 , G02F1/133603 , H01L33/502
Abstract: Provided is a light emitting device capable of realizing color reproducibility in a broad range. The light emitting device contains a light emitting element having an emission peak wavelength in a range of 430 nm or more and 470 nm or less, a first fluorescent material having a composition represented by formula (I), which has an emission peak wavelength in a range of 510 nm or more and 525 nm or less and has an average particle diameter that is 10.0 μm or more and 30.0 μm or less, and a second fluorescent material having an emission peak wavelength in a range of 620 nm or more and 670 nm or less: X1aMgbMncAldOa+b+c+1.5d (I) wherein X1 represents at least one element selected from the group consisting of Ba, Sr and Ca, and a, b, c and d satisfy 0.5≦a≦1.0, 0.0≦b≦0.7, 0.3≦c≦0.7, and 8.5≦d≦13.0.
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公开(公告)号:US20180086977A1
公开(公告)日:2018-03-29
申请号:US15717232
申请日:2017-09-27
Applicant: NICHIA CORPORATION
Inventor: Shoji HOSOKAWA , Daiki KURAMOTO
CPC classification number: C09K11/7734 , C09K11/0883
Abstract: A method of producing a nitride fluorescent material including a step of first heat-treating a first compound containing at least one alkaline earth metal element selected from the group consisting of Ba, Sr, Ca and Mg, a second compound containing at least one element selected from the group consisting of Eu, Ce, Tb and Mn, and a Si-containing compound, in an atmosphere containing nitrogen to obtain a calcined product of raw materials, and a step of second heat-treating the calcined product of raw materials, a Ba-containing compound, a Si-containing compound, and optionally a third compound containing at least one element selected from the group consisting of Eu, Ce, Tb and Mn, and optionally a fourth compound containing at least one alkaline earth metal element selected from the group consisting of Sr, Ca and Mg, in an atmosphere containing nitrogen to obtain a nitride fluorescent material is provided, wherein the ratio of the charge-in molar amount of Ba to the total charge-in molar amount of at least one alkaline earth metal element to be contained in the calcined product of raw materials in the step of obtaining the calcined product of raw materials is smaller than the ratio of the charge-in molar amount of Ba to the total charge-in molar amount of at least one alkaline earth metal element to be contained in the nitride fluorescent material in the step of obtaining the nitride fluorescent material.
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公开(公告)号:US20180002600A1
公开(公告)日:2018-01-04
申请号:US15635751
申请日:2017-06-28
Applicant: NICHIA CORPORATION
Inventor: Shoji HOSOKAWA , Daiki KURAMOTO
CPC classification number: C09K11/7734 , C09K11/0883
Abstract: A method of producing a nitride fluorescent material having relatively high light emission intensity is provided. The method of producing a nitride fluorescent material includes preparing a calcined product having a composition containing at least one first element selected from the group consisting of Ba, Sr, Ca, and Mg, at least one second element selected from the group consisting of Eu, Ce, Tb, and Mn, and Si and N, and bringing the calcined product into contact with a fluorine-containing substance at a temperature in a range of −20° C. or higher and lower than 150° C.
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公开(公告)号:US20170342321A1
公开(公告)日:2017-11-30
申请号:US15606153
申请日:2017-05-26
Applicant: NICHIA CORPORATION
Inventor: Kenichi AOYAGI , Takashi KAIDE , Motoharu MORIKAWA , Shoji HOSOKAWA
CPC classification number: C09K11/7734 , C09K11/0883
Abstract: Provided is a method of producing a β-sialon fluorescent material having a high light emission intensity and an excellent light emission luminance. The method includes preparing a calcined product having a composition of β-sialon containing an activating element; grinding the calcined product to obtain a ground product; and heat-treating the ground product to obtain a heat-treated product. A specific surface area of the ground product is 0.2 m2/g or more.
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