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    Thermochemical production of hydrogen and oxygen from water
    32.
    发明授权
    Thermochemical production of hydrogen and oxygen from water 失效
    从水中热和生成氢气和氧气

    公开(公告)号：US4027003A

    公开(公告)日：1977-05-31

    申请号：US627246

    申请日：1975-10-30

    Applicant: William H. Dorrance ,  Rane L. Curl

    Inventor： William H. Dorrance ,  Rane L. Curl

    IPC: C01B3/06 ,  C01B7/00 ,  C01B7/01 ,  C01B7/03 ,  C01B7/09 ,  C01B7/19 ,  C01B13/02 ,  C01B13/00 ,  C01B1/00

    CPC classification number: C01B13/0207 ,  C01B3/068 ,  C01B7/01 ,  C01B7/03 ,  C01B7/096 ,  C01B7/191 ,  Y02E60/36 ,  Y02P20/134

    Abstract: A process is disclosed which produces hydrogen and oxygen from water by means of a multi-step, closed, thermochemical cycle. Hydrogen and oxygen are produced at separate stations. Hydrogen and a halogen are produced by a sub-cycle involving transition metal or lanthanide compounds (depending on the halogen) and a hydrogen halide. Oxygen and the hydrogen halide are produced in a sub-cycle involving magnesium or transition metal compounds (depending on the halogen), the halogen and water. When the halogen is chlorine the transition metals in the oxygen producing sub-cycle can be nickel, cobalt, or yttrium and the lanthanide metals in the hydrogen producing sub-cycle can be samarium, europium, or ytterbium. When the halogen is bromine, the metals in the oxygen producing sub-cycle can be manganese or cobalt and the metals in the hydrogen producing sub-cycle can be vanadium or chromium.

    Abstract translation: 公开了一种通过多步骤，封闭的热化学循环从水产生氢和氧的方法。 氢和氧在不同的工作站产生。 氢和卤素通过涉及过渡金属或镧系元素化合物（取决于卤素）和卤化氢的亚循环产生。 氧和卤化氢在涉及镁或过渡金属化合物（取决于卤素），卤素和水的亚循环中产生。 当卤素是氯时，产氧子循环中的过渡金属可以是镍，钴或钇，并且在产氢子循环中的镧系金属可以是钐，铕或镱。 当卤素为溴时，氧生成亚循环中的金属可以是锰或钴，并且产氢子循环中的金属可以是钒或铬。

    Solar hydrogen generator
    33.
    发明授权
    Solar hydrogen generator 失效
    太阳能发电机

    公开(公告)号：US4019868A

    公开(公告)日：1977-04-26

    申请号：US669928

    申请日：1976-03-24

    Applicant: Daniel I. Sebacher ,  Alexander P. Sabol

    Inventor： Daniel I. Sebacher ,  Alexander P. Sabol

    IPC: C01B3/04 ,  F24S20/20 ,  F24S23/71 ,  B01J7/00 ,  C01B1/00

    CPC classification number: F24J2/12 ,  C01B3/045 ,  F24J2/07 ,  Y02E10/41 ,  Y02E10/42 ,  Y02E60/364 ,  Y02P20/134

    Abstract: An apparatus for using solar energy to manufacture hydrogen by dissociating water molecules into hydrogen and oxygen molecules. Solar energy is concentrated on a globe containing water thereby heating the water to its dissociation temperature. The globe is pervious to hydrogen molecules permitting them to pass through the globe while being essentially impervious to oxygen molecules. The hydrogen molecules are collected after passing through the globe and the oxygen molecules are removed from the globe.

    Abstract translation: 一种使用太阳能通过将水分子分解成氢和氧分子来制造氢的装置。 太阳能集中在含有水的地球上，从而将水加热至其解离温度。 地球是透过氢分子，允许它们通过地球，而基本上不透氧分子。 在通过球体后收集氢分子，氧分子从地球上去除。

    Closed-cycle thermochemical process for the decomposition of water
    35.
    发明授权
    Closed-cycle thermochemical process for the decomposition of water 失效
    用于水分解的封闭循环热化学工艺

    公开(公告)号：US3839550A

    公开(公告)日：1974-10-01

    申请号：US37453673

    申请日：1973-06-28

    Applicant: GEN ELECTRIC

    Inventor： WENTORF R

    IPC: C01B3/06 ,  C01B3/10 ,  C01B13/02 ,  C01D3/12 ,  C01D15/02 ,  C01D15/04 ,  G21D9/00 ,  C01B1/00 ,  C01B13/00

    CPC classification number: G21D9/00 ,  C01B3/061 ,  C01B3/068 ,  C01B3/10 ,  C01B13/0207 ,  C01D3/12 ,  C01D15/02 ,  C01D15/04 ,  Y02E60/36

    Abstract: 1. THE PROCESS FOR THE GENERATION OF HYDROGEN AND OXYGEN FROM WATER COMPRISING THE STEPS OF: (A) HYDROLYZING LITHIUM IODIDE TO PRODUCE LITHIUM HYDROXIDE AND HYDROIODIC ACID; (B) REMOVING THE HYDROIDIC ACID FROM THE HYDROLYSIS REACTION ZONE, (C) REACTING AQUEOUS LITHIUM HYDROXIDE FROM TEP (A) WITH IODINE TO PRODUCE AN AQUEOUS MIXTURE OF LITHIUM IODIDE AND LITHIUM IODATE, (D) SEPARATING THE LITHIUM IODIDE FROM THE LITHIUM IODATE, SAID LITHIUM IODIDE BEING USED FOR STEP (A), (E) REACTING THE LITHIUM IODATE IN THE PRESENCE OF WATER WITH THE IODIDE OF A METAL SELECTED FROM THE GROUP CONSISTING OF POTASSIUM, RUBIDIUM AND CESIUM, (F) SEPARATING IODATE OF THE METAL SELECTED FROM THE LITHIUM IODIDE AND WATER, (G) THERMALLY DECOMPOSING THE METAL OXIDE OIDATE SO SEPARATED TO YEILED OXYGEN AND THE IODIDE OF THE SELECTED METAL, AT LEAST SOME OF THE OXYGEN BEING CONTINOUSLU REMOVED FROM THE SYSTEM AND THE METAL IODIDE BEING USED IN STEP (E), (H) CONVERTING THE HYDROIDIC ACID TO HYDROGEN AND IODINE, THE HYDROGEN BEING CONTINOUSLY REMOVED FROM THE SYSTEM AND COLLECTED AND THE IODINE BEING USED IN STEP (C) AND (I) CONTINOUSLY INTRODUCING WATER INTO THE SYSTEM.

    Process for the recovery of deuterium from hydrogen-rich gas
    36.
    发明授权
    Process for the recovery of deuterium from hydrogen-rich gas 失效
    从富含氢气中恢复氘代的方法

    公开(公告)号：US3821361A

    公开(公告)日：1974-06-28

    申请号：US15824171

    申请日：1971-06-30

    Applicant: UHDE GMBH FRIEDRICH

    Inventor： WALTER S ,  SCHINDEWOLF U

    IPC: B01D53/34 ,  C01B4/00 ,  C01B1/00

    CPC classification number: B01D53/34 ,  C01B4/00

    Abstract: A process for the recovery of deuterium from a gas having deuterium values and oxygen bearing impurities by contacting the gas with a solution of sodium or lithium in ammonia to eliminate oxygen-bearing impurities as sparingly soluble reaction products. The NH3-Na or Li solution contacts the synthesis gas saturated with NH3 having oxygen impurities and deuterium values therein and the deuterium rich ammonia gases from a deuterium enrichment unit in order to achieve saturation of higher deuterium concentration. The ammonia gases saturated with deuterium values are finally passed on to the deuterium enrichment unit to recover deuterium values and to produce ammonia depleted of deuterium. The preparation and/or stock tank for the Na -or Li- solution in NH3 is provided with a lining material selected from the group consisting of copper, non-ferrous metal and plastics because the NH3-Na solution resides in these containers for an extended period of time.

    A process for preparing lithium aluminum hydride-aluminum hydride complexes
    37.
    发明授权
    A process for preparing lithium aluminum hydride-aluminum hydride complexes 失效
    一种制备氢氧化铝 - 氢化铝复合物的方法

    公开(公告)号：US3816192A

    公开(公告)日：1974-06-11

    申请号：US7543960

    申请日：1960-12-12

    Applicant: DOW CHEMICAL CO

    Inventor： BROWER F ,  DANIELS A ,  FUJIOKA G

    IPC: C01B6/24 ,  C01B1/00

    CPC classification number: C01B6/243

    Abstract: A complex of Li AlH4 and AlH3 is prepared by mixing substantially anhydrous ether solution of AlCl3 and LiAlH4 in a dry inert atmosphere. By-product LiCl is removed and the complex hydride is subsequently recovered.

    Abstract translation: 通过在干燥的惰性气氛中混合基本上无水的AlCl 3和LiAlH 4的醚溶液来制备LiAlH 4和AlH 3的络合物。 副产物LiCl被除去，随后回收复合氢化物。

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