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    Process for the manufacture of 2,3-dimethylpentanal
    44.
    发明授权
    Process for the manufacture of 2,3-dimethylpentanal 失效
    2,3-二甲基戊醛的制备方法

    公开(公告)号：US4205013A

    公开(公告)日：1980-05-27

    申请号：US891380

    申请日：1978-03-28

    Applicant: Jurgen Weber ,  Helmut Springer

    Inventor： Jurgen Weber ,  Helmut Springer

    IPC: B01J31/00 ,  C07B61/00 ,  C07C45/00 ,  C07C45/50 ,  C07C47/02 ,  C07C67/00 ,  C07C45/10

    CPC classification number: C07C45/50

    Abstract: A process for the preparation of 2,3-dimethylpentanal which comprises contacting 3-methyl-2-pentene with carbon monoxide and hydrogen in the presence of a rhodium carbonyl compound as catalyst. Rhodium carbonyl catalysts are those which contain only rhodium and carbon monoxide and in certain cases, also hydrogen. Especially contemplated are non-phosphine containing rhodium carbonyl catalysts.

    Abstract translation: 一种制备2,3-二甲基戊醛的方法，其包括在羰基铑化合物作为催化剂存在下使3-甲基-2-戊烯与一氧化碳和氢气接触。 铑羰基催化剂是仅含有铑和一氧化碳的催化剂，在某些情况下也是氢气。 特别考虑的是不含磷化氢的铑羰基催化剂。

    Incinerator
    45.
    发明授权
    Incinerator 失效

    公开(公告)号：US3552334A

    公开(公告)日：1971-01-05

    申请号：US3552334D

    申请日：1969-01-31

    Applicant: HELMUT SPRINGER

    Inventor： SPRINGER HELMUT ,  BIENICK FRITZ

    IPC: F23G5/16 ,  F23G5/00

    CPC classification number: F23G5/165

    Abstract: An incinerator has a lower combustion portion preferably equipped with a burner and an upper afterburning portion which can be swung off the lower portion. This upper portion has an upper outlet mouth. A chimney extends alongside the portions and has a lateral flue which opens just above the upper outlet mouth. A collar on the flue controls the amount of air let in at the gap between the flue''s end and the mouth and this collar can be lifted also to swing out the upper afterburning portion for loading the combustibles into the burning chamber. A flap on the chimney below where the flue is connected is biased closed by a weight and, on excessive draft, opens to control this draft.

    3(4),7(8)-Bis(aminomethyl)bicyclo[4.3.0]nonane and a process for its preparation
    46.
    发明授权
    3(4),7(8)-Bis(aminomethyl)bicyclo[4.3.0]nonane and a process for its preparation 失效
    3（4），7（8） - 双（氨基甲基）双环[4.3.0]壬烷及其制备方法

    公开(公告)号：US07342135B2

    公开(公告)日：2008-03-11

    申请号：US11657749

    申请日：2007-01-25

    Applicant: Helmut Springer ,  Paolo Bavaj

    Inventor： Helmut Springer ,  Paolo Bavaj

    IPC: C07C209/60 ,  C07C211/36 ,  C07C211/38

    CPC classification number: C07C211/19 ,  C07C2602/24

    Abstract: 3(4),7(8)-bis(aminomethyl)bicyclo[4.3.0]nonane and a process for its preparation, wherein bicyclo[4.3.0]nona-3,7-diene is reacted with synthesis gas in a homogeneous organic phase in the presence of transition metal compounds of Group VIII of the Periodic Table containing complex-bound organophosphorus compounds, and excess organophosphorus compound, at temperatures of 70 to 160° C. and pressures of 5 to 35 MPa, and the 3(4),7(8)-bisformylbicyclo[4.3.0]nonane thus obtained is reductively aminated.

    Abstract translation: 3（4），7（8） - 双（氨基甲基）双环[4.3.0]壬烷及其制备方法，其中双环[4.3.0]壬-3,7-二烯与合成气以均匀 在70至160℃的温度和5至35MPa的压力下，在含有复合结合的有机磷化合物的周期表第Ⅷ族的过渡金属化合物和过量的有机磷化合物存在下的有机相和3（4 ），7（8） - 二甲酰基双环[4.3.0]壬烷进行还原胺化。

    Process for preparing TCD-monenal
    47.
    发明授权
    Process for preparing TCD-monenal 失效
    制备TCD- monenal的方法

    公开(公告)号：US07122706B2

    公开(公告)日：2006-10-17

    申请号：US10968760

    申请日：2004-10-19

    Applicant: Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    Inventor： Peter Lappe ,  Helmut Springer ,  Rainer Lukas

    IPC: C07C45/50

    CPC classification number: C07C47/445 ,  C07C45/50 ,  C07C45/82

    Abstract: A process for selectively hydroformylating dicyclopentadiene to 8(9)-formyltricyclo-[5.2.1.02,6]dec-3-ene in a heterogeneous reaction system using an aqueous solution of transition metal compounds, containing water-soluble organic phosphorus(III) compounds in complex-bound form, of group VIII of the Periodic Table of the Elements, wherein the water-soluble organic phosphorus(III) compounds are alkali metal or alkaline earth metal salts of sulfonated arylphosphines and aryldiphosphines.

    Abstract translation: 使用含水的过渡金属化合物的水溶液在非均相反应体系中选择性地将二环戊二烯加氢甲酰化为8（9） - 甲酰基三环[5.2.1.0 2,6]癸-3-烯的方法 其中水溶性有机磷（III）化合物是磺化芳基膦和芳基二膦的碱金属或碱土金属盐，它们是复合结合形式的元素周期表第Ⅷ族的可溶性有机磷（III）化合物。

    Process for preparing aliphatic straight-chain and beta-alkyl-branched carboxylic acids
    48.
    发明申请
    Process for preparing aliphatic straight-chain and beta-alkyl-branched carboxylic acids 有权

    公开(公告)号：US20060106249A1

    公开(公告)日：2006-05-18

    申请号：US11237294

    申请日：2005-09-28

    Applicant: Helmut Springer ,  Frank Winsberg

    Inventor： Helmut Springer ,  Frank Winsberg

    IPC: C07C51/235

    CPC classification number: C07C51/235 ,  C07C53/126

    Abstract: The present invention relates to a process for preparing aliphatic straight-chain and β-alkyl-branched carboxylic acids by catalytic oxidation of aldehydes by means of oxygen or oxygen-containing gas mixtures. Alkali metal carboxylates or alkaline earth metal carboxylates or a mixture thereof in an amount, calculated as alkali metal or alkaline earth metal, of from 1 mmol each to from 10 mmol each per mole of aldehyde used and also metals or compounds of metals of groups 5 to 11 of the Periodic Table of the Elements in amounts of not more than 5 ppm, based on aldehyde used, are present as catalyst.

    Method for the synthesis of aliphatic carboxylic acids from aldehydes
    49.
    发明授权
    Method for the synthesis of aliphatic carboxylic acids from aldehydes 有权
    从醛合成脂族羧酸的方法

    公开(公告)号：US06800783B2

    公开(公告)日：2004-10-05

    申请号：US10204619

    申请日：2002-09-05

    Applicant: Helmut Springer ,  Peter Lappe

    Inventor： Helmut Springer ,  Peter Lappe

    IPC: C07C51235

    CPC classification number: C07C51/235 ,  Y02P20/582 ,  C07C53/126 ,  C07C53/124

    Abstract: The invention relates to a method for the synthesis of aliphatic carboxylic acids by the catalytic oxidation of aldehydes with oxygen, or oxygen-containing gas mixtures. Metals of groups 5 11 of the periodic table of elements, or the compounds thereof are used as catalyst, in amounts of up to 5 ppm, based upon the amount of aldehyde used.

    Abstract translation: 本发明涉及通过用氧或含氧气体混合物催化氧化醛来合成脂族羧酸的方法。 基于元素周期表的第5组11的金属或其化合物，以所使用的醛的量为基准，最多可用量为5ppm。

    Process for preparing saturated alcohols
    50.
    发明授权
    Process for preparing saturated alcohols 失效
    饱和醇的制备方法

    公开(公告)号：US06288288B1

    公开(公告)日：2001-09-11

    申请号：US09199862

    申请日：1998-11-25

    Applicant: Helmut Springer

    Inventor： Helmut Springer

    IPC: C07C2914

    CPC classification number: C07C29/175 ,  C07C45/74 ,  C07C49/203 ,  C07C31/125

    Abstract: A process for preparing saturated alcohols comprising effecting an aldol condensation of alkyl methyl ketones of 6 to 8 carbon atoms which are branched at the &bgr;-carbon atom with aldehydes of 4 to 15 carbon atoms which are branched at the &agr;-carbon atom to form &agr;,&bgr;-unsaturated ketones and subsequent hydrogenation of the &agr;,&bgr;-unsaturated ketones to obtain alcohols, wherein the aldol condensation is carried out at a temperature of 60 to 130° C. in the presence of a 30-55% strength aqueous solution of an alkali metal hydroxide resulting in very low by-product formation.

    Abstract translation: 一种制备饱和醇的方法，包括使在碳原子上分支的碳原子数为6至8的烷基甲基酮与醛原子上含有4至15个碳原子的醛进行醛醇缩合从而形成α ，β-不饱和酮和随后氢化α，β-不饱和酮以获得醇，其中醛醇缩合在60至130℃的温度下进行，在30-55％强度的 碱金属氢氧化物导致非常低的副产物形成。

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