Method for purifying difluorophosphate

    公开(公告)号:US10112835B2

    公开(公告)日:2018-10-30

    申请号:US14419181

    申请日:2014-06-06

    Abstract: Provided is a method for purifying a difluorophosphate, in which a difluorophosphate is purified to a high purity. The method includes a method for purifying a difluorophosphate, comprising bringing hydrogen fluoride into contact with a difluorophosphate containing an impurity and subsequently heating and drying the difluorophosphate, or bringing the hydrogen fluoride into contact with the difluorophosphate containing the impurity while heating and drying the difluorophosphate containing the impurity, thereby removing the impurity.

    Method for producing difluorophosphate

    公开(公告)号:US09624107B2

    公开(公告)日:2017-04-18

    申请号:US14418720

    申请日:2014-06-06

    CPC classification number: C01B25/455 H01G11/62 H01M10/052 H01M10/0568

    Abstract: Provided is a method for producing a difluorophosphate, which can easily and industrially advantageously produce a high-purity difluorophosphate. The method includes a step of producing a difluorophosphate in the fluorophosphoric acid solution by reacting hydrofluoric acid anhydride containing no solvent with an oxoacid and/or the like of phosphorous to produce a fluorophosphoric acid solution; a step of adding a hexafluorophosphate to the fluorophosphoric acid solution in the absence of respective halides, carbonates, borates, phosphates, hydroxides, and oxides of an alkali metal and the like; and a step of heating and drying the fluorophosphoric acid solution containing the difluorophosphate to distill away a fluorophosphoric acid, or a step of depositing the difluorophosphate in the fluorophosphoric acid solution by crystallization, subsequently separating the difluorophosphate by solid-liquid separation, and distilling away a fluorophosphoric acid contained in the difluorophosphate after the solid-liquid separation.

    Method for producing hollow structural body
    45.
    发明授权
    Method for producing hollow structural body 有权
    中空结构体的制造方法

    公开(公告)号:US08668851B2

    公开(公告)日:2014-03-11

    申请号:US13739967

    申请日:2013-01-11

    Abstract: It is intended to provide a method of producing a hollow construct, which may be in various shapes such as a fiber or a film as well as in various sizes and has chemical resistance, made of a fluorinated hydrocarbon polymer, a fluorinated carbon polymer or a polymer carrying a nitrogen-containing group, a silicon-containing group, an oxygen-containing group, a phosphorus-containing group or a sulfur-containing group having been introduced into the above-described polymer; and a hollow construct obtained by this method.

    Abstract translation: 本发明提供一种中空构造体的制造方法,该中空构造体可以是各种形状,例如纤维或膜,以及各种尺寸,并且具有耐化学性,由氟化烃聚合物,氟化碳聚合物或 携带含氮基团的聚合物,含有导入到上述聚合物中的含氮基团,含氧基团,含磷基团或含硫基团; 和通过该方法获得的中空构造。

    METHOD FOR PRODUCING HOLLOW STRUCTURAL BODY
    46.
    发明申请
    METHOD FOR PRODUCING HOLLOW STRUCTURAL BODY 有权
    生产中空结构体的方法

    公开(公告)号:US20130187305A1

    公开(公告)日:2013-07-25

    申请号:US13739967

    申请日:2013-01-11

    Abstract: It is intended to provide a method of producing a hollow construct, which may be in various shapes such as a fiber or a film as well as in various sizes and has chemical resistance, made of a fluorinated hydrocarbon polymer, a fluorinated carbon polymer or a polymer carrying a nitrogen-containing group, a silicon-containing group, an oxygen-containing group, a phosphorus-containing group or a sulfur-containing group having been introduced into the above-described polymer; and a hollow construct obtained by this method.

    Abstract translation: 本发明提供一种中空构造体的制造方法,该中空构造体可以是各种形状,例如纤维或膜,以及各种尺寸,并且具有耐化学性,由氟化烃聚合物,氟化碳聚合物或 携带含氮基团的聚合物,含有导入到上述聚合物中的含氮基团,含氧基团,含磷基团或含硫基团; 和通过该方法获得的中空构造。

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