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    Ultrasound enhanced process for extracting metal species in supercritical fluids
    41.
    发明申请
    Ultrasound enhanced process for extracting metal species in supercritical fluids 失效
    用于超临界流体萃取金属物质的超声增强方法

    公开(公告)号：US20030183043A1

    公开(公告)日：2003-10-02

    申请号：US10397862

    申请日：2003-03-25

    发明人： Chien M. Wai ,  Youichi Enokida

    IPC分类号： C22B009/02

    CPC分类号： B01D11/0203 ,  B01D11/0219 ,  B01D11/0261 ,  B01D11/0265 ,  B01D11/028 ,  C22B3/0005 ,  C22B60/0239 ,  G21C19/48 ,  G21F9/06 ,  G21F9/30 ,  Y02P10/234 ,  Y02W30/884 ,  Y10S210/912

    摘要： Improved methods for the extraction or dissolution of metals, metalloids or their oxides, especially lanthanides, actinides, uranium or their oxides, into supercritical solvents containing an extractant are disclosed. The disclosed embodiments specifically include enhancing the extraction or dissolution efficiency with ultrasound. The present methods allow the direct, efficient dissolution of UO2 or other uranium oxides without generating any waste stream or by-products.

    摘要翻译： 公开了将金属，准金属或其氧化物，特别是镧系元素，锕系元素，铀或其氧化物提取或溶解到含有萃取剂的超临界溶剂中的改进方法。 所公开的实施方案具体包括用超声波增强提取或溶解效率。 本方法允许直接，有效地溶解UO2或其他铀氧化物，而不产生任何废物流或副产物。

    Treatment of carbonaceous materials
    42.
    发明授权
    Treatment of carbonaceous materials 失效
    碳质材料的处理

    公开(公告)号：US5017281A

    公开(公告)日：1991-05-21

    申请号：US358636

    申请日：1989-05-30

    申请人： Mohammad-Ali Sadeghi ,  Kazem Sadeghi ,  Jih-Fen Kuo ,  Long-Kuan Jang ,  Teh F. Yen

    发明人： Mohammad-Ali Sadeghi ,  Kazem Sadeghi ,  Jih-Fen Kuo ,  Long-Kuan Jang ,  Teh F. Yen

    IPC分类号： B01D11/02 ,  C10G1/04

    CPC分类号： B01D11/0265 ,  C10G1/04 ,  C10G1/047

    摘要： Hydrocarbon liquids are recovered from carbonaceous materials such as tar sands utilizing a separation reagent formed in situ by reacting polar resin components of tar sands with an inorganic base such as sodium silicate in sonicated aqueous solution in absence of an organic solvent to form a surfactant. Under the influence of sonication a microemulsion of polar-external micelles forms. The polar groups can associate with anions, especially polyanions such as silicate and act in a membrane mimetic manner to form vesicles. Cavities can form in the surfactant resin molecule that complex with guest cations such as titanium or other metals from the tar sand.When tar sands are added to the sonicated separation reagent, the surfactant penetrates the bitumen. Metal ions complex with the polar groups and aid in removing the bitument from the sand particles. The polarorganic asphaltene materials are carried into the aqueous phase by the anion and stabilized within the micelle structure. The lighter, non-polar hydrocarbon oil fraction separate from the emulsion and rise to the top and are recovered by skimming. The heavier asphaltenes and preasphaltenes complex with the polyvalent metals to form charcoal-like agglomerates which settle to the bottom of the treatment tank. The separation reagent forms during the reaction and can reach a concentration capable of dissolving bitumen. The separation reagent can be recovered and used in other processes after removal and recovery of the clay. The separation reagent must be substantially diluted after being recycled and reused to reduce solvation properties.

    摘要翻译： 烃类液体是从含碳物质如沥青砂中回收的，利用在无有机溶剂的条件下，将超临界水溶液中的焦油砂的极性树脂成分与无机碱如硅酸钠在原位形成的分离剂一起回收，形成表面活性剂。 在超声处理的影响下，形成极性 - 外部胶束的微乳液。 极性基团可以与阴离子，特别是聚阴离子如硅酸盐结合，并以膜模拟方式起作用以形成囊泡。 可以在表面活性剂树脂分子中形成空穴，其与来自焦油砂的客体阳离子如钛或其它金属络合。 当沥青砂添加到超声处理的分离试剂中时，表面活性剂渗透沥青。 金属离子与极性基团复合，有助于从砂粒中除去废料。 极性有机沥青质材料通过阴离子进入水相并稳定在胶束结构内。 较轻的非极性烃油馏分与乳液分离并升至顶部，并通过撇去回收。 较重的沥青质和预沥青质与多价金属复合，形成沉淀到处理槽底部的类似炭的附聚物。 在反应过程中形成分离剂，并能达到能够溶解沥青的浓度。 在除去和回收粘土之后，分离试剂可以被回收并用于其它工艺中。 分离试剂在回收再利用后必须基本稀释，以降低溶剂化性能。

    Ultrasonic composite acidic water extraction method for cordyceps polysaccharide and cordycepin in
    44.
    发明授权
    Ultrasonic composite acidic water extraction method for cordyceps polysaccharide and cordycepin in 有权

    公开(公告)号：US12109509B2

    公开(公告)日：2024-10-08

    申请号：US17419718

    申请日：2019-12-06

    申请人： JIANGNAN UNIVERSITY

    发明人： Min Zhang ,  Hao Shi ,  Sifu Yi ,  Xiaoling Guo ,  Lihua Hou ,  Wuxiong Yang

    IPC分类号： A23L31/00 ,  A01G18/70 ,  B01D11/02 ,  C08B37/00

    CPC分类号： B01D11/0265 ,  A01G18/70 ,  A23L31/00 ,  C08B37/00

    摘要： Disclosed is an ultrasonic composite acidic water extraction method for a Cordyceps polysaccharide and cordycepin in Cordyceps militaris, which falls within the technical field of food processing. The method comprises: picking, washing, drying, pulverizing and degreasing Cordyceps militaris fruiting bodies to obtain a Cordyceps militaris dry powder; then immersing same in a prepared diluted hydrochloric acid solution to perform three cycles of ultra-low temperature freezing and microwave defrosting, and at the same time using low-frequency ultrasonic waves to carry out assisted stirring and extraction; then subjecting an extract to evaporation and concentration treatments; and finally, performing freeze-drying on the extract to collect a dry powder of a water extraction product. The amount of an additive used in the method meets domestic and foreign usage requirements of food additives, and the operation is simple, practical and uses a combination of chemical and physical methods, thereby saving time and being highly efficient.

    EXTRACTION METHODS AND APPARATUS
    45.
    发明公开
    EXTRACTION METHODS AND APPARATUS 审中-公开

    公开(公告)号：US20240261701A1

    公开(公告)日：2024-08-08

    申请号：US18564676

    申请日：2022-05-27

    申请人： PUREPLANTE BIOSCIENCE INC.

    发明人： Jie QI ,  Harry LIU

    IPC分类号： B01D11/02

    CPC分类号： B01D11/0265

    摘要： Methods for extracting one or more compounds from a plant or fungal material feedstock include immersing the plant or fungal material feedstock in a liquid, subjecting the immersed plant or fungal material and/or the liquid to ultrasonic vibrations, and subsequently extracting one or more compounds from the plant or fungal material. Also disclosed are methods for treating one or more compounds extracted from a plant or fungal material feedstock. Such methods include providing the extracted compounds and a liquid to an emulsification vessel, subjecting the extracted compounds and the liquid to ultrasonic vibrations using a circulating agitator to create an emulsion of the extracted compounds and the liquid. The methods for extracting one or more compounds from a plant or fungal material feedstock and the methods for treating one or more compounds extracted from a plant or fungal material feedstock may be used separately or in conjunction with each other.

    Flow Cell Horn And Method Of Tuning
    50.
    发明公开
    Flow Cell Horn And Method Of Tuning 审中-公开

    公开(公告)号：US20230264116A1

    公开(公告)日：2023-08-24

    申请号：US17677342

    申请日：2022-02-22

    申请人： Sonics & Materials, Inc.

    发明人： Andrew Rushton ,  Jeffrey Meyer ,  Daniel Grise

    IPC分类号： B01D11/02 ,  B01J19/10 ,  G01H13/00

    CPC分类号： B01D11/0265 ,  B01D11/0288 ,  B01J19/10 ,  G01H13/00 ,  B01J2219/0877

    摘要： An ultrasonic horn includes a generally cylindrical input section having an energy input end, a generally cylindrical output section having an energy output end, and a throat section disposed between the input section and the output section, the throat section being defined by a side wall having a continuous curve and having a diameter tapering down from a diameter generally equal to a diameter of the input section on a side connected to the input section, and tapering down from a diameter generally equal to a diameter of the output section on a side connected to the output section, to a minimum throat diameter. The minimum throat diameter is smaller than the diameter of the output section and the diameter of the output section is smaller than the diameter of the input section. The side wall of the throat section has a constant radius of curvature.