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    Preparation of polyamide thermoplastic adhesive from polyoxypropylene polyamine and piperazine
    62.
    发明授权
    Preparation of polyamide thermoplastic adhesive from polyoxypropylene polyamine and piperazine 失效
    由聚氧丙烯多胺和哌嗪制备聚酰胺热塑性粘合剂

    公开(公告)号：US4182845A

    公开(公告)日：1980-01-08

    申请号：US920903

    申请日：1978-06-29

    Applicant: Ernest L. Yeakey ,  Harold G. Waddill

    Inventor： Ernest L. Yeakey ,  Harold G. Waddill

    IPC: C08G69/40 ,  C09J177/00 ,  C08G69/28

    CPC classification number: C08G69/40 ,  C09J177/00

    Abstract: Novel thermoplastic adhesive components, prepared from inexpensive and readily available synthetic materials, having melting points between about 20.degree. C. to about 180.degree. C. and broad ranges of hardness, flexibility and compatibility are disclosed. The novel thermoplastic compounds useful in adhesive formulations are comprised of a resinous polyamide reaction product of a polyoxypropylene polyamine having an average molecular weight of from about 190 to about 3,000 and being selected from diamines, triamines, or mixtures thereof, piperazine and an aliphatic or aromatic dicarboxylic acid, ester or anhydride having from about 4 to about 20 carbon atoms per molecule. The resinous polyamide reaction product is prepared by mixing and reacting the polyoxypropylene polyamine, piperazine, and dicarboxylic acid materials in a total amine:acid molar ratio within the range of from about 0.25:1.0 to about 4.0:1.0 at a temperature of from about 175.degree. C. to about 270.degree. C. The inventive thermoplastic polyamides can be formulated with compatible plasticizing agents to prepare a useful adhesive to which can also be added other components, such as a minor amount of a polyepoxide resin having an epoxide equivalent weight of about 150 to about 600, fillers and the like to produce thermoplastic adhesive formulations having desired hardness, flexibility and compatibility that are capable of bonding together a variety of substrates.

    Abstract translation: 公开了由廉价且容易获得的合成材料制备的具有约20℃至约180℃的熔点和宽范围的硬度，柔性和相容性的新型热塑性粘合剂组分。 用于粘合剂制剂的新型热塑性化合物由平均分子量为约190至约3,000的聚氧丙烯多胺的树脂聚酰胺反应产物组成，并且选自二胺，三胺或其混合物，哌嗪和脂族或芳族 每个分子具有约4-约20个碳原子的二羧酸，酯或酸酐。 树脂聚酰胺反应产物是通过将聚氧丙烯多胺，哌嗪和二羧酸材料在总的胺：酸摩尔比在约0.25:1.0至约4.0:1.0的范围内，在约175℃ 本发明的热塑性聚酰胺可以用相容的增塑剂配制以制备可用的粘合剂，也可以向其中加入其它成分，例如少量的环氧当量重量约为 150至约600，填料等，以生产具有能够将各种基材粘合在一起的所需硬度，柔性和相容性的热塑性粘合剂制剂。

    Polyether dihydroxyalkyl carbamate epoxy additive for epoxy resins
    66.
    发明授权
    Polyether dihydroxyalkyl carbamate epoxy additive for epoxy resins 失效
    用于环氧树脂的聚醚二羟基烷基氨基甲酸酯环氧添加剂

    公开(公告)号：US4122069A

    公开(公告)日：1978-10-24

    申请号：US786751

    申请日：1977-04-11

    Applicant: Lee G. Meyer

    Inventor： Lee G. Meyer

    IPC: C08G59/40 ,  C08G59/56 ,  C08G71/04

    CPC classification number: C08G59/4057 ,  C08G59/56 ,  C08G71/04

    Abstract: The adhesion properties of amine-cured epoxy resins are unexpectedly enhanced by addition of certain di-hydroxyalkyl carbamate terminated polyether additives. The adhesively superior epoxy resin composition comprises a vicinal polyepoxide, a curing amount of an amine curing agent, and an effective amount of a polyether dicarbamate having terminal hydroxyalkyl carbamate groups and a molecular weight of from about 2000 to about 3000.

    Abstract translation: 胺固化的环氧树脂的粘合性能通过加入某些二羟基烷基氨基甲酸酯封端的聚醚添加剂而出人意料地增强。 粘合优异的环氧树脂组合物包含邻位聚环氧化物，固化量的胺固化剂和有效量的具有末端羟基烷基氨基甲酸酯基团并且分子量为约2000至约3000的聚醚二氨基甲酸酯。

    Boride catalyst for epoxidizing olefinic compounds
    67.
    发明授权
    Boride catalyst for epoxidizing olefinic compounds 失效
    用于环氧化烯烃化合物的硼化催化剂

    公开(公告)号：US4110352A

    公开(公告)日：1978-08-29

    申请号：US761159

    申请日：1977-01-21

    Applicant: Robert M. Gipson

    Inventor： Robert M. Gipson

    IPC: C07D301/19 ,  C07D303/04 ,  C07D301/20

    CPC classification number: C07D301/19 ,  C07D301/14 ,  C07D303/04

    Abstract: A novel catalyst material of a boron containing substance for catalyzing the liquid phase oxidation of an olefin with an organic hydroperoxide to the corresponding oxirane is disclosed. The novel catalyst materials are characterized as binary or ternary boride compounds having the general formula M.sub.x B.sub.y or M.sub.x B.sub.y R.sub.z wherein x is an integer from 1-5; y is an integer from 1-2; z is an integer from 1-4; B is boron; M is an element selected from the groups II-A, III-B, IV-B, V-B, VI-B, VII-B, VIII, III-A, IV-A, and V-A of the Periodic Table, the rare earths, and the actinides; and R is an element different from M selected from the same group of elements in the Periodic Table as M. The preferred catalyst materials are those boron containing substances which are substantially insoluble in the reaction mixture containing the organic hydroperoxides, olefins and products.Also disclosed is a method for liquid phase epoxidation of an olefinic compound with an organic hydroperoxide at lower temperatures, e.g. 25.degree. to 200.degree. C. and a pressure sufficient to maintain the mixture substantially in liquid phase in the presence of a catalytically effective amount of the novel catalyst material.

    Abstract translation: 公开了一种用于催化烯烃与有机氢过氧化物向相应环氧乙烷的液相氧化的含硼物质的新型催化剂材料。 新型催化剂材料的特征在于具有通式MxBy或MxByRz的二元或三元硼化物，其中x为1-5的整数; y是1-2的整数; z是1-4的整数; B是硼; M是选自元素周期表II-A，III-B，IV-B，VB，VI-B，VII-B，VIII，III-A，IV-A和VA中的元素，稀土 ，和锕系元素; 并且R是不同于选自元素周期表中同一组元素的M的元素。优选的催化剂材料是基本上不溶于含有机氢过氧化物，烯烃和产物的反应混合物中的含硼物质。

    Production of bis-(morpholino-N-alkyl) ethers
    70.
    发明授权
    Production of bis-(morpholino-N-alkyl) ethers 失效
    双（双（甲氧基）-N-烷基）酯的生产

    公开(公告)号：US4095022A

    公开(公告)日：1978-06-13

    申请号：US679590

    申请日：1976-04-23

    Applicant: Michael E. Brennan ,  Philip H. Moss ,  Ernest L. Yeakey

    Inventor： Michael E. Brennan ,  Philip H. Moss ,  Ernest L. Yeakey

    IPC: C07D295/023 ,  C07D295/088 ,  C08G18/20 ,  C07D265/28

    CPC classification number: C07D295/023 ,  C07D295/088 ,  C08G18/2018 ,  C08G18/2081

    Abstract: An improved process is disclosed for selectively producing a bis-(morpholino-N-alkyl) ether directly from the corresponding N-(hydroxyalkyl)morpholine compound. The improved process includes contacting the N-(hydroxyalkyl)morpholine compound with a catalytically effective amount of a silica-alumina or certain phosphorus containing substances at a temperature of about 200.degree. C to 300.degree. C under a pressure sufficient to maintain the mixture substantially in liquid phase and recovering from the resultant reaction mixture the bis-(morpholino-N-alkyl) ether.According to the preferred embodiment, N-(2-hydroxyethyl)morpholine is heated in the presence of a catalytic amount of a silica-alumina catalyst having an alumina content of from about 5 to about 50 wt. % at temperatures of from about 240.degree. C to about 290.degree. C in liquid phase to selectively produce the corresponding N,N',2,2'-dimorpholinodiethyl ether (DMDEE).

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