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公开(公告)号：US08575405B2
公开(公告)日：2013-11-05
申请号：US13197737
申请日：2011-08-03
申请人： David Lee , Adam Orosco , Lincoln Sarager , R. Jay Warner , Radmila Jevtic , Victor J. Johnston
发明人： David Lee , Adam Orosco , Lincoln Sarager , R. Jay Warner , Radmila Jevtic , Victor J. Johnston
IPC分类号： C07C29/149
CPC分类号： B01D3/40 , B01D3/148 , C07C29/149 , C07C29/80 , C07C29/88 , C07C51/12 , C07C31/08 , C07C53/08
摘要： To reduce acetal concentrations when separating ethanol from a crude product in one or more distillation column, at least one of the columns is operated at a higher pressure to increase the equilibrium constant that favors hydrolysis of the acetal. The crude product may comprise ethanol, acetaldehyde, water and one or more acetals, such as diethyl acetal. The acetal concentration may be reduced thus reducing the need to separate acetal from the crude product.
摘要翻译： 为了减少在一个或多个蒸馏塔中从粗产物中分离乙醇时的乙缩醛浓度，至少一个塔在较高的压力下运行以增加有利于缩醛水解的平衡常数。 粗产物可以包括乙醇，乙醛，水和一种或多种缩醛，例如二乙缩醛。 缩醛浓度可能会降低，从而减少了从粗产物分离乙缩醛的需要。
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公开(公告)号：US20130035523A1
公开(公告)日：2013-02-07
申请号：US13197737
申请日：2011-08-03
申请人： David Lee , Adam Orosco , Lincoln Sarager , R. Jay Warner , Radmila Jevtic , Victor J. Johnston
发明人： David Lee , Adam Orosco , Lincoln Sarager , R. Jay Warner , Radmila Jevtic , Victor J. Johnston
IPC分类号： C07C29/149 , B01D3/00
CPC分类号： B01D3/40 , B01D3/148 , C07C29/149 , C07C29/80 , C07C29/88 , C07C51/12 , C07C31/08 , C07C53/08
摘要： To reduce acetal concentrations when separating ethanol from a crude product in one or more distillation column, at least one of the columns is operated at a higher pressure to increase the equilibrium constant that favors hydrolysis of the acetal. The crude product may comprise ethanol, acetaldehyde, water and one or more acetals, such as diethyl acetal. The acetal concentration may be reduced thus reducing the need to separate acetal from the crude product.
摘要翻译： 为了减少在一个或多个蒸馏塔中从粗产物中分离乙醇时的乙缩醛浓度，至少一个塔在较高的压力下运行以增加有利于缩醛水解的平衡常数。 粗产物可以包括乙醇，乙醛，水和一种或多种缩醛，例如二乙缩醛。 缩醛浓度可能会降低，从而减少了从粗产物分离乙缩醛的需要。
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公开(公告)号：US20130035517A1
公开(公告)日：2013-02-07
申请号：US13273054
申请日：2011-10-13
IPC分类号： C07C29/143 , C07C31/08
CPC分类号： C07C29/149 , C07C29/145 , C07C45/48 , C07C31/10 , C07C31/08 , C07C49/08
摘要： A process is described for producing an alcohol product, in which (a) a first feed composition comprising acetic acid is converted to a product comprising acetone; and (b) a second feed composition comprising at least part of the acetone produced in (a) is hydrogenated in the presence of a catalyst to produce a hydrogenation effluent comprising isopropanol.
摘要翻译： 描述了用于生产醇产物的方法，其中（a）包含乙酸的第一进料组合物转化为包含丙酮的产物; 和（b）包含（a）中生产的至少一部分丙酮的第二进料组合物在催化剂存在下氢化以产生包含异丙醇的氢化流出液。
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公开(公告)号：US08754267B2
公开(公告)日：2014-06-17
申请号：US13078754
申请日：2011-04-01
申请人： R. Jay Warner , Heiko Weiner , Nathan Bower , Josefina T. Chapman , Gerald Grusendorf , Radmila Jevtic , Victor J. Johnston
发明人： R. Jay Warner , Heiko Weiner , Nathan Bower , Josefina T. Chapman , Gerald Grusendorf , Radmila Jevtic , Victor J. Johnston
IPC分类号： C07C29/149
CPC分类号： C07C29/149 , C07C29/80 , C07C31/08
摘要： Purifying and/or recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of crude ethanol mixture are employed to allow recovery of ethanol and remove impurities. In particular, light ends are separated in an acetaldehyde removal column operating at a pressure greater than atmospheric pressure to recover acetaldehyde that may be returned to the reactor and reduce acetaldehyde concentrations in an ethyl acetate stream.
摘要翻译： 从乙酸氢化获得的粗乙醇产物中纯化和/或回收乙醇。 使用粗乙醇混合物的分离和纯化方法来回收乙醇并除去杂质。 特别地，轻馏分在以大于大气压的压力下操作的乙醛除去塔中分离以回收乙醛，其可以返回到反应器中并降低乙酸乙酯流中的乙醛浓度。
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公开(公告)号：US20120010448A1
公开(公告)日：2012-01-12
申请号：US13178861
申请日：2011-07-08
IPC分类号： C07C29/147
CPC分类号： C07C29/141 , C07C29/149 , C07C29/78 , C07C29/80 , C07C29/86 , C07C29/88 , C07C29/90 , C07C67/08 , C07C31/08 , C07C69/14
摘要： A process for purifying ethanol by using a finishing reactor to remove impurities, such as ethyl acetate, acetaldehyde, acetic acid, and diethyl acetal, present in ethanol after distilling a crude product from a hydrogenation reactor. The finishing reactor may reduce the impurities in the presence of hydrogen and a catalyst or may hydrolyze the impurities.
摘要翻译： 在从氢化反应器中蒸馏出粗产物后，使用精整反应器来净化乙醇的方法，以除去乙醇中的杂质，如乙酸乙酯，乙醛，乙酸和二乙基缩醛。 精加工反应器可以在氢和催化剂存在下减少杂质，或者可能水解杂质。
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公开(公告)号：US20110275865A1
公开(公告)日：2011-11-10
申请号：US13078754
申请日：2011-04-01
申请人： R. Jay Warner , Heiko Weiner , Nathan Bower , Josefina T. Chapman , Gerald Grusendorf , Radmila Jevtic , Victor J. Johnston
发明人： R. Jay Warner , Heiko Weiner , Nathan Bower , Josefina T. Chapman , Gerald Grusendorf , Radmila Jevtic , Victor J. Johnston
IPC分类号： C07C29/149 , C07C29/80
CPC分类号： C07C29/149 , C07C29/80 , C07C31/08
摘要： Purifying and/or recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of crude ethanol mixture are employed to allow recovery of ethanol and remove impurities. In particular, light ends are separated in an acetaldehyde removal column operating at a pressure greater than atmospheric pressure to recover acetaldehyde that may be returned to the reactor and reduce acetaldehyde concentrations in an ethyl acetate stream.
摘要翻译： 从乙酸氢化获得的粗乙醇产物中纯化和/或回收乙醇。 使用粗乙醇混合物的分离和纯化方法来回收乙醇并除去杂质。 特别地，轻馏分在以大于大气压的压力下操作的乙醛除去塔中分离以回收乙醛，其可以返回到反应器中并降低乙酸乙酯流中的乙醛浓度。
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公开(公告)号：US20110275862A1
公开(公告)日：2011-11-10
申请号：US12889813
申请日：2010-09-24
申请人： Victor J. Johnston , Josefina T. Chapman , Radmila Jevtic , Heiko Weiner , Tianshu Pan , R. Jay Warner , Gerald Grusendorf , Nathan Bower , Lincoln M. Sarager
发明人： Victor J. Johnston , Josefina T. Chapman , Radmila Jevtic , Heiko Weiner , Tianshu Pan , R. Jay Warner , Gerald Grusendorf , Nathan Bower , Lincoln M. Sarager
IPC分类号： C07C29/80
CPC分类号： C07C29/149 , C07C29/88 , C07C31/08
摘要： Recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of the crude ethanol products are employed to allow recovery of ethanol and remove acetal impurities.
摘要翻译： 从乙酸氢化得到的粗乙醇产物中回收乙醇。 使用粗乙醇产物的分离和纯化方法以回收乙醇并除去缩醛杂质。
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公开(公告)号：US08304586B2
公开(公告)日：2012-11-06
申请号：US12852269
申请日：2010-08-06
申请人： Radmila Jevtic , Victor J. Johnston , R. Jay Warner , Heiko Weiner , Nathan Bower , Josefina T. Chapman , Gerald Grusendorf
发明人： Radmila Jevtic , Victor J. Johnston , R. Jay Warner , Heiko Weiner , Nathan Bower , Josefina T. Chapman , Gerald Grusendorf
IPC分类号： C07C29/149
CPC分类号： C07C29/149 , C07C29/141 , C07C29/80 , C07C31/08
摘要： Purifying and/or recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of crude ethanol mixture are employed to allow recovery of ethanol and remove impurities. In addition, the process involves returning acetaldehyde separated from the crude ethanol product to the reactor.
摘要翻译： 从乙酸氢化获得的粗乙醇产物中纯化和/或回收乙醇。 使用粗乙醇混合物的分离和纯化方法来回收乙醇并除去杂质。 此外，该方法包括将从粗乙醇产物分离的乙醛返回到反应器中。
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公开(公告)号：US20110190548A1
公开(公告)日：2011-08-04
申请号：US12852269
申请日：2010-08-06
申请人： Radmila Jevtic , Victor J. Johnston , R. Jay Warner , Heiko Weiner , Nathan Bower , Josefina Chapman , Gerald Grusendorf
发明人： Radmila Jevtic , Victor J. Johnston , R. Jay Warner , Heiko Weiner , Nathan Bower , Josefina Chapman , Gerald Grusendorf
CPC分类号： C07C29/149 , C07C29/141 , C07C29/80 , C07C31/08
摘要： Purifying and/or recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of crude ethanol mixture are employed to allow recovery of ethanol and remove impurities. In addition, the process involves returning acetaldehyde separated from the crude ethanol product to the reactor.
摘要翻译： 从乙酸氢化获得的粗乙醇产物中纯化和/或回收乙醇。 使用粗乙醇混合物的分离和纯化方法来回收乙醇并除去杂质。 此外，该方法包括将从粗乙醇产物分离的乙醛返回到反应器中。
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公开(公告)号：US08318988B2
公开(公告)日：2012-11-27
申请号：US12889813
申请日：2010-09-24
申请人： Victor J. Johnston , Josefina T. Chapman , Radmila Jevtic , Heiko Weiner , Tianshu Pan , R. Jay Warner , Gerald Grusendorf , Nathan Bower , Lincoln M. Sarager
发明人： Victor J. Johnston , Josefina T. Chapman , Radmila Jevtic , Heiko Weiner , Tianshu Pan , R. Jay Warner , Gerald Grusendorf , Nathan Bower , Lincoln M. Sarager
IPC分类号： C07C29/149
CPC分类号： C07C29/149 , C07C29/88 , C07C31/08
摘要： Recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of the crude ethanol products are employed to allow recovery of ethanol and remove acetal impurities.
摘要翻译： 从乙酸氢化得到的粗乙醇产物中回收乙醇。 使用粗乙醇产物的分离和纯化方法以回收乙醇并除去缩醛杂质。
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