Process for the manufacture of polycarboxylic acids using phosphorous containing reducing agents
    63.
    发明授权
    Process for the manufacture of polycarboxylic acids using phosphorous containing reducing agents 失效
    使用含磷还原剂制造多元羧酸的方法

    公开(公告)号:US07169742B2

    公开(公告)日:2007-01-30

    申请号:US10267296

    申请日:2002-10-09

    IPC分类号: C11D11/00 C11D3/36 C11D3/37

    CPC分类号: C08F20/04

    摘要: A method for the production of polycarboxylic acids is provided via the present invention. The novel method herein comprises the steps of i) mixing a phosphorous containing reducing agent with at least one carboxylic acid monomer to form a reaction mixture; ii) adding an equivalent of base to the reaction mixture to provide a partially neutralized reaction mixture; and iii) adding a free radical generator to the partially neutralized reaction mixture under polymerization conditions to form a phospho/carboxylic acid polymer containing solution. Preferred monomers, reducing agents and free radical generators are also disclosed.

    摘要翻译: 通过本发明提供了制备多元羧酸的方法。 本发明的新方法包括以下步骤:i)将含磷还原剂与至少一种羧酸单体混合以形成反应混合物; ii)向反应混合物中加入等量的碱以提供部分中和的反应混合物; 和iii)在聚合条件下向部分中和的反应混合物中加入自由基发生剂以形成含磷/羧酸聚合物的溶液。 还公开了优选的单体,还原剂和自由基发生剂。

    Durable press treatment of fabric
    66.
    发明授权
    Durable press treatment of fabric 失效
    织物的耐久压力处理

    公开(公告)号:US06841198B2

    公开(公告)日:2005-01-11

    申请号:US10267267

    申请日:2002-10-09

    摘要: A post mill or post manufacturing process for reducing wrinkle and crease problems in fabric articles is provided. The process involves the domestic or commercial laundry application of a phosphonate- and phosphinate-containing polycarboxylate cross-linking agent followed by at least partial curing of the cross-linking agent via the application of heat to the article. The present invention also includes an article of manufacture or product comprising the treatment composition, at least one container for the treatment composition and accompanying text instructing the user of the product on application of the treatment.

    摘要翻译: 提供了一种用于减少织物制品中的皱纹和折痕问题的后磨或后制造工艺。 该方法涉及含磷酸盐和次膦酸盐的多羧酸盐交联剂的家用或商业洗衣应用,然后通过向制品施加热至少部分固化交联剂。 本发明还包括一种制品或包含该处理组合物的产品,用于处理组合物的至少一个容器和在施加该处理时指示该产品的使用者的随附文本。

    Method for enhancing suds volume and suds duration using liquid detergent compositions comprising polymeric suds enhancers
    68.
    发明授权
    Method for enhancing suds volume and suds duration using liquid detergent compositions comprising polymeric suds enhancers 失效
    使用包含聚合物增泡剂的液体洗涤剂组合物提高泡沫体积和泡沫持续时间的方法

    公开(公告)号:US06825157B2

    公开(公告)日:2004-11-30

    申请号:US10650019

    申请日:2003-08-27

    IPC分类号: C11D100

    摘要: A method for providing enhanced suds volume and suds duration in dishwashing using liquid detergent compositions comprising a polymeric material which is a suds enhancer and a suds volume extender, said compositions having increased effectiveness for preventing re-deposition of grease during hand washing are provided. The polymeric material which are suitable as suds volume and suds endurance enhancers comprise an effective amount of a quaternary nitrogen-containing monomeric unit and/or zwitterionic monomeric unit-containing polymeric suds enhancer comprise: i) units capable of having a cationic charge at a pH of from about 4 to about 12; provided that said suds enhancer has an average cationic charge density of 2.8 or less units per 100 daltons molecular weight at a pH of from about 4 to about 12; b) an effective amount of a detersive surfactant; and c) the balance carriers and other adjunct ingredients; provided that a 10% aqueous solution of said detergent composition has a pH of from about 4 to about 12.

    摘要翻译: 提供了使用液体洗涤剂组合物提供增强的泡沫体积和泡沫持续时间的方法,所述液体洗涤剂组合物包含聚合物材料,其为增泡剂和泡沫体积增长剂,所述组合物具有增强的用于防止洗手时油脂再沉积的效果。 适合作为泡沫体积和泡沫耐久性增强剂的聚合物材料包含有效量的含季氮的单体单元和/或两性离子单体单元的聚合物泡沫增强剂包括:i)能够在pH值下具有阳离子电荷的单元 约4至约12; 条件是所述泡沫增强剂在约4至约12的pH下具有2.8或更少单位/ 100道尔顿分子量的平均阳离子电荷密度; b)有效量的去污表面活性剂; 和c)平衡载体和其它辅助成分;条件是所述洗涤剂组合物的10%水溶液具有约4至约12的pH。