METHOD FOR PREPARING HETEROATOM-DOPED CNHS
    61.
    发明公开

    公开(公告)号:US20230286805A1

    公开(公告)日:2023-09-14

    申请号:US18304316

    申请日:2023-04-20

    CPC classification number: C01B32/18 B01J21/18 B01J23/42 B01J35/0013 B01J37/08

    Abstract: A method includes the following steps: a first step: the material containing heteroatom and graphite powder are mixed for a preset time by grinding, and the molar ratio of heteroatom to carbon atom is 1%-10%, then the heteroatom precursors are obtained; a second contact step: the heteroatom precursor is filled into a graphite rod with holes and compacted, then the graphite rod is dried for a preset time to obtain a plasma anode and using a DC arc plasma device to prepare the graphite anode into heteroatom-doped CNHs; a third contact step: the heteroatom-doped CNHs are dispersed in a reducing solution, a platinum salt is added to stir evenly, the reduction reaction is carried out by heating and stirring, and after centrifugation, washing and drying, a catalyst with platinum loading is obtained.

    Opening-closing type microwave catalytic reaction apparatus

    公开(公告)号:US11571676B2

    公开(公告)日:2023-02-07

    申请号:US17492140

    申请日:2021-10-01

    Abstract: The present disclosure provides an opening-closing type microwave catalytic reaction apparatus, including a microwave system, a microwave cavity, a protective cover, a cooling system, and a vertical furnace tube, where two ends of the furnace tube are respectively stretched out of the microwave cavity, the microwave system includes a plurality of microwave transmitting units, and the microwave transmitting unit includes a microwave transmitter; the furnace tube is provided with a gas inlet on a top and a gas outlet on a bottom; a compression hinge and a cavity cover capable of being opened or closed are arranged on the microwave cavity, a convex edge plate is disposed at an edge of the cavity cover, the compression hinge can compress the cavity cover such that the convex edge plate is tightly attached to a concave edge plate on the microwave cavity, and the protective cover can cover the entire cavity cover.

    OPENING-CLOSING TYPE MICROWAVE CATALYTIC REACTION APPARATUS

    公开(公告)号:US20220314190A1

    公开(公告)日:2022-10-06

    申请号:US17492140

    申请日:2021-10-01

    Abstract: The present disclosure provides an opening-closing type microwave catalytic reaction apparatus, including a microwave system, a microwave cavity, a protective cover, a cooling system, and a vertical furnace tube, where two ends of the furnace tube are respectively stretched out of the microwave cavity, the microwave system includes a plurality of microwave transmitting units, and the microwave transmitting unit includes a microwave transmitter; the furnace tube is provided with a gas inlet on a top and a gas outlet on a bottom; a compression hinge and a cavity cover capable of being opened or closed are arranged on the microwave cavity, a convex edge plate is disposed at an edge of the cavity cover, the compression hinge can compress the cavity cover such that the convex edge plate is tightly attached to a concave edge plate on the microwave cavity, and the protective cover can cover the entire cavity cover.

    HIGH ENTROPY ALLOY POWDER FOR LASER CLADDING AND APPLICATION METHOD THEREOF

    公开(公告)号:US20220097133A1

    公开(公告)日:2022-03-31

    申请号:US17486062

    申请日:2021-09-27

    Abstract: The present disclosure discloses a high-entropy alloy powder for laser cladding and a use method thereof. The alloy powder is CoCrFeMnNiCx, and x has a value of 0.1-0.15. The specific method includes: subjecting a 45 steel substrate to surface pretreatment, mixing the weighed CoCrFeMnNi high-entropy alloy powder with different content of a nano-C powder uniformly and pre-placed on the pre-treated substrate surface to form a prefabricated layer, then placing the prefabricated layer at 80-90° C. for constant temperature treatment for 8-12 h, and under a protective atmosphere, subjecting the cladding powder to laser cladding on the surface of the 45 steel. The method of the present disclosure prepares a CoCrFeMnNiCx high-entropy alloy coating with performance superior to the CoCrFeMnNi high-entropy alloy coating.

    Method for simultaneously removing SO2 and NOX in flue gas

    公开(公告)号:US10814273B2

    公开(公告)日:2020-10-27

    申请号:US16601661

    申请日:2019-10-15

    Abstract: The invention discloses a method for simultaneously removing SO2 and NOx in flue gas: uniformly mixing a water-soluble ruthenium salt with ammonia water to obtain an aqueous solution of a ruthenium-amine complex; subjecting the flue gas and the aqueous solution of the ruthenium-amine complex to a countercurrent contact reaction under the temperature of 5-60° C., pH of 7.5-12 to obtain a solution A and purified gas; discharging the solution A of the step (2) into a crystallization tank to crystallize and separate an ammonium salt to obtain a solution B, returning the solution B to replace the aqueous solution of the ruthenium-amine complex. The invention utilizes the ruthenium-amine complex having a strong capability of complexing with NO as well as residual oxygen in the flue gas to carry out liquid phase catalytic oxidation to convert the NOx into ammonium nitrate, and the removal efficiency of the NOx and the SO2 is high.

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