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    Dyeing cellulosic textiles with vat and sulfur dyes using sodium dithionite and an aldehyde-bisulfite addition product stabilizer
    71.
    发明授权
    Dyeing cellulosic textiles with vat and sulfur dyes using sodium dithionite and an aldehyde-bisulfite addition product stabilizer 失效
    带有增值税的染色纺织品和使用二氧化钛和二异氰酸酯添加剂的硫化染料产品稳定剂

    公开(公告)号：US3645665A

    公开(公告)日：1972-02-29

    申请号：US3645665D

    申请日：1969-05-26

    申请人： DAN RIVER INC

    发明人： ETTERS JAMES N

    IPC分类号： D06P1/22 ,  D06P1/62 ,  D06P1/30

    CPC分类号： D06P1/623 ,  D06P1/221 ,  D06P1/622 ,  D06P1/628 ,  Y10S8/918

    摘要： An improved process for dyeing cellulosic textiles with vat or sulfur dyes using sodium dithionite as reducing agent, using as a stabilizer for the reducing agent a stabilizer of the formula WHEREIN M is a monovalent cation selected from the class consisting of alkali metal and ammonium cations, R is a monovalent group selected from the class consisting of hydrogen, alkyl, alkenyl and furyl, n is an integer of 1 to 3, X is a group having a valence of n and is selected from the class consisting of hydroxyl and substituents having the formula R''3 n N and R'' is a monovalent radical selected from the class consisting of hydrogen and monovalent hydrocarbon, said stabilizer being used in an amount providing about 0.01 to about 2 mols of UNIT OF SAID STABILIZER PER MOL OF SAID REDUCING AGENT. Also, the stabilizer as defined above in dry particulate form and novel mixtures of reducing agent and stabilizer.

    摘要翻译： 使用连二亚硫酸钠作为还原剂使用大瓮或硫化染料染色纤维素织物的改进方法，使用还原剂的稳定剂，式WHEREIN M是选自碱金属和铵阳离子的一价阳离子， R是选自氢，烷基，烯基和呋喃基的一价基团，n为1〜3的整数，X为n价的基团，选自羟基和具有 式R'3-nN和R'是选自氢和一价烃的一价基团，所述稳定剂以提供约0.01至约2摩尔的减压剂每单位的单位使用的量使用 。 此外，如上定义的稳定剂以干燥颗粒形式和还原剂和稳定剂的新型混合物。

    Process for the production of reduced sulfur dyes
    72.
    发明授权
    Process for the production of reduced sulfur dyes 失效
    生产减少硫磺染色体的方法

    公开(公告)号：US3640803A

    公开(公告)日：1972-02-08

    申请号：US3640803D

    申请日：1970-02-04

    申请人： CASSELLA FARBWERKE MAINKUR AG

    发明人： FRIND HORST ,  HEID CHRISTIAN ,  AMAN HORST

    IPC分类号： C09B49/00 ,  D06P1/30 ,  C07B29/06

    CPC分类号： C09B49/00 ,  D06P1/30

    摘要： The dyeing behavior of a sulfur dyestuff, whether water soluble or water insoluble, is improved by electrolytic reduction. This reduction is performed in a cell in which the dyestuff is used as the catholyte. An ionic agent, such as salt or lye may be used to improve the conductivity of the catholyte. The dyestuff concentration in the cell ranges from about 5 to 50 percent by weight and 10 to 20 percent by weight is particularly effective. A porous clay diaphragm separates the anolyte and catholyte. The anolyte is for example, an aqueous lye or salt solution. The cathode is a material having relatively high hydrogen overvoltage, such as lead and alloy steels. The anode is a noble metal such as platinum or graphite. The catholyte is agitated during the reduction and its temperature is maintained from about 25* to 200* C. and preferably from 50* to 80* C. A current density of about 0.005 to 0.05 A./cm.2 is employed and preferably maintained from 0.01 to 0.04 A./cm.2. The reduction has an energy demand from about 0.5 to 1 kWh./kg. The termination of the reduction of water-insoluble sulfur dyestuff is determined by a spot analysis test. The end of the reduction of water-soluble sulfur dyestuffs is determined relative to hydrogen formation. After the electrolytic reduction has been terminated, the catholyte is stabilized by adding any of a number of suitable reducing agents.

    摘要翻译： 通过电解还原改善了硫化染料的染色行为，无论是水溶性还是水不溶性的。 该还原在使用染料作为阴极电解液的电池中进行。 可以使用离子剂，例如盐或碱液来改善阴极电解液的导电性。 细胞中的染料浓度为约5〜50重量％，10〜20重量％特别有效。 多孔粘土隔膜分离阳极电解液和阴极电解液。 阳极电解液是例如碱水溶液或盐水溶液。 阴极是具有相对高的氢过电压的材料，例如铅和合金钢。 阳极是贵金属如铂或石墨。 在还原过程中搅动阴极电解液，其温度保持在约25℃至200℃，优选50℃至80℃。使用约0.005至0.05A / cm 2的电流密度，并优选保持 从0.01到0.04 A./cm.2。 减少的能量需求约为0.5至1kWh./kg。 通过点分析测试来确定水不溶性硫色素的还原的终止。 水溶性硫色素的还原结束相对于氢的形成来确定。 电解还原终止后，通过添加多种合适的还原剂来稳定阴极电解液。

    Printed textile fibers and method for producing same
    73.
    发明授权
    Printed textile fibers and method for producing same 失效
    印刷纺织纤维及其生产方法

    公开(公告)号：US3625642A

    公开(公告)日：1971-12-07

    申请号：US3625642D

    申请日：1967-08-01

    申请人： MARTIN MARIETTA CORP

    发明人： TRIBBLE FEASTER V

    IPC分类号： C09B62/443 ,  D06P1/12 ,  D06P1/30 ,  D06P3/66 ,  C09B27/00

    CPC分类号： D06P3/666 ,  C09B62/443 ,  D06P1/127 ,  D06P1/305 ,  Y10S8/918 ,  Y10S534/01

    摘要： THERE ARE DISCLOSED HEREIN COTTON AND REGENERATED CELLULOSE TEXTILE FIBERS HAVING PRINTED THEREON A MIXTURE OF AZOIC DYE AND THE DYESTUFF RESULTING FROM REACTING NA2S2-4 WITH CERTAIN THIOSULFATE DYES. THERE IS ALSO DISCLOSED A PRINTING METHOD CMPRISING THE STEPS OF APPLYING TO COTTON OR REGENERATED CELLULOSE TEXTILE FIBERS AN ALKALINE PRINTING PASTE COMPRISING WATER, THICKENER, DYESTUFF SELECTED FROM THE GROUP CONSISTING OF AZO, SULFUR, PHTHALOCYANINE, METAL PHTHALOCYANINE, PERYLENE, DIOXAZINE, ANTHRAQUINONE, AND ISODIBENZANTHRONE DYES HAVING PER DYE MOLECULE AT LEAST ONE PENDANT - SSO3NA1 .-SSO3K, -SSO3NH4 OR -SSO3H GROUP, SOLUBILIZED TRIAZENE FORM OF STABILIZED DIAZO COMPOUND, AND A SOLUBILIZED NAPHTHOL COUPLING COMPONENT; DRYING THE FIBERS; ACID AGEING THE FIBERS WITH VOLATILIZED ACID AND AQUEOUS STEAM; APPLYING AQUEOUS NA2S2-4 AND EITHER SODA ASH OR SODIUM BORAX TO THE FIBERS; OPTIONALLY EXPOSING THE FIBERS TO AIR; AND WASHING THE FIBERS.

    Permanent press process
    74.
    发明授权
    Permanent press process 失效
    永久新闻稿

    公开(公告)号：US3573858A

    公开(公告)日：1971-04-06

    申请号：US3573858D

    申请日：1969-07-25

    申请人： CELANESE CORP

    发明人： MOUSSALLI FRANCIS S ,  BROWNE COLIN L

    IPC分类号： D06M15/00 ,  D06M15/423 ,  D06M15/507 ,  D06M23/00 ,  D06M101/00 ,  D06M101/02 ,  D06M101/06 ,  D06M101/08 ,  D06M101/16 ,  D06M101/30 ,  D06M101/32 ,  D06P1/22 ,  D06P1/30 ,  D06P3/54 ,  D06P3/62 ,  D06P3/82 ,  D06F71/00 ,  D06C29/00

    CPC分类号： D06P3/62 ,  D06M15/423 ,  D06M23/00 ,  D06P1/22 ,  D06P1/30 ,  D06P3/54 ,  D06P3/8238

    摘要： There is provided a novel process for the production of flatdrying, dimensionally stable, durable press garments with good abrasion resistance properties. In such process there is no requirement that the textile material from which said garments are made be impregnated with a fiber-setting reagent and precured or postcured in order to obtain a permanent press; rather, said press is obtained by the more economical and desirable method of heating the textile material to a temperature and for a time of from about 180* Fahrenheit for about 6 hours to about 440* Fahrenheit for about 1 second, cutting patterned pieces of fabric, sewing said pieces into a unitary shaped body, and pressing said shaped body for from about 10 to about 90 seconds at a head temperature of from about 300* to about 350* Fahrenheit and an air supply pressure of from about 20 to about 100 pounds per square inch. This process works especially well with fabrics comprised of from about 50 to about 95 percent of polyester. Since the fabrics used in this process contain substantially no fiber-setting reagent, the garments produced via the process of this invention possess excellent abrasion resistance properties.