Process for producing arylsulfur pentafluorides

    公开(公告)号:US07820864B2

    公开(公告)日:2010-10-26

    申请号:US12473109

    申请日:2009-05-27

    申请人: Teruo Umemoto

    发明人: Teruo Umemoto

    IPC分类号: C07C315/00

    CPC分类号: C07C381/00

    摘要: Novel processes for preparing arylsulfur pentafluorides are disclosed. Processes include reacting at least one aryl sulfur compound with a halogen and a fluoro salt to form an arylsulfur halotetrafluoride. The arylsulfur halotetrafluoride is reacted with a fluoride source to form a target arylsulfur pentafluoride.

    Process for Producing Arylsulfur Pentafluorides
    3.
    发明申请
    Process for Producing Arylsulfur Pentafluorides 有权
    生产丙烯基五氟化硫的方法

    公开(公告)号:US20090287024A1

    公开(公告)日:2009-11-19

    申请号:US12473129

    申请日:2009-08-04

    申请人: Teruo Umemoto

    发明人: Teruo Umemoto

    IPC分类号: C07C381/00

    CPC分类号: C07C381/00

    摘要: Novel processes for preparing arylsulfur pentafluorides are disclosed. Processes include reacting at least one aryl sulfur compound with a halogen and a fluoro salt to form an arylsulfur halotetrafluoride. The arylsulfur halotetrafluoride is reacted with a fluoride source to form a target arylsulfur pentafluoride.

    摘要翻译: 公开了制备芳基五氟化硫的新方法。 方法包括使至少一种芳基硫化合物与卤素和氟盐反应形成芳基卤四氟化硫。 芳基卤四氟化物与氟化物源反应形成目标芳基五氟化硫。

    Process for producing arylsulfur pentafluorides
    4.
    发明授权
    Process for producing arylsulfur pentafluorides 有权
    芳基五氟化硫的制备方法

    公开(公告)号:US07592491B2

    公开(公告)日:2009-09-22

    申请号:US12053775

    申请日:2008-03-24

    申请人: Teruo Umemoto

    发明人: Teruo Umemoto

    IPC分类号: C07C315/00

    CPC分类号: C07C381/00

    摘要: Novel processes for preparing arylsulfur pentafluorides are disclosed. Processes include reacting at least one aryl sulfur compound with a halogen and a fluoro salt to form an arylsulfur halotetrafluoride. The arylsulfur halotetrafluoride is reacted with a fluoride source to form a target arylsulfur pentafluoride.

    摘要翻译: 公开了制备芳基五氟化硫的新方法。 方法包括使至少一种芳基硫化合物与卤素和氟盐反应形成芳基卤四氟化硫。 芳基卤四氟化物与氟化物源反应形成目标芳基五氟化硫。

    Tetraketopiperazine unit-containing compound as an active material in batteries
    5.
    发明申请
    Tetraketopiperazine unit-containing compound as an active material in batteries 失效
    含四氯哌嗪单元的化合物作为电池中的活性物质

    公开(公告)号:US20030148188A1

    公开(公告)日:2003-08-07

    申请号:US10028064

    申请日:2001-12-20

    发明人: Teruo Umemoto

    IPC分类号: H01M006/18

    摘要: Compounds containing at least one tetraketopiperazine-1,4-diyl unit are disclosed as active materials in the positive electrodes of batteries. Novel methods for preparing the tetraketopiperazine unit-containing compounds include: (i) reacting an oxalyl halide and an oxamide, and adding water or an aqueous alkali solution to the reaction mixture, (ii) reacting an oxalyl halide and a silylamine, (iii) reacting an oximidyl halide and an amine, (iv) reacting an oxalyl halide and a silylamine, and reacting with an amine, (v) reacting an oxalyl halide and a dioxamide, (vi) reacting an oximidyl halide and a diamine, and (vii) reacting an oxalyl halide and a silylamine, and reacting with a diamine. A novel method for preparing an oximidyl halide is also disclosed.

    摘要翻译: 公开了含有至少一种四硒代哌嗪-1,4-二基单元的化合物作为电池正极中的活性材料。 用于制备含有四取代哌嗪单元的化合物的新方法包括:(ⅰ)使草酰卤和草酰胺反应,并向反应混合物中加入水或碱式水溶液,(ⅱ)使草酰卤和甲硅烷基胺反应,(iii) 使肟酰卤和胺反应,(iv)使草酰卤和甲硅烷基胺反应,并与胺反应,(v)使草酰卤和二氧杂环己烷反应,(vi)使肟基卤和二胺反应,和(vii )使草酰卤和甲硅烷基胺反应,并与二胺反应。 还公开了一种制备肟基卤化物的新方法。

    Method for preparing polymers containing cyclopentanone structures
    10.
    发明授权
    Method for preparing polymers containing cyclopentanone structures 失效
    制备含有环戊酮结构的聚合物的方法

    公开(公告)号:US07182850B2

    公开(公告)日:2007-02-27

    申请号:US10845839

    申请日:2004-05-14

    申请人: Teruo Umemoto

    发明人: Teruo Umemoto

    IPC分类号: C25B3/00 C25B3/02

    摘要: A method to electrolytically polymerize aromatic hydrocarbons and oxidize cyclopentane structures within the hydrocarbons into cyclopentanone structures is disclosed including a method to electrolyze fluorene in the presence of an ester to produce poly(9-fluorenone). A method to electrolytically oxidize polymers having cyclopentane structures to polymers having cyclopentanone structures is also disclosed including a method to electrolyze poly(fluorene) to produce poly(9-fluorenone). In addition, a method to chemically oxidize polymers containing cyclopentane structures into polymers containing cyclopentanone structures is disclosed, including a method to oxidize poly(fluorene), with a chemically prepared oxidizing agent, to produce poly(9-fluroenone).

    摘要翻译: 公开了一种使芳族烃电解聚合并将烃内的环戊烷结构氧化为环戊酮结构的方法,包括在酯存在下电解芴以产生聚(9-芴酮)的方法。 还公开了一种将具有环戊烷结构的聚合物电解氧化成具有环戊酮结构的聚合物的方法,其包括电解聚(芴)以产生聚(9-芴酮)的方法。 此外,公开了一种将含有环戊烷结构的聚合物化学氧化成含有环戊酮结构的聚合物的方法,包括用化学制备的氧化剂氧化聚(芴)的方法以产生聚(9-氟酮酮)。