Process and apparatus for air separation by rectification
    4.
    发明授权
    Process and apparatus for air separation by rectification 失效
    通过整流进行空气分离的方法和装置

    公开(公告)号:US4824453A

    公开(公告)日:1989-04-25

    申请号:US217516

    申请日:1988-07-11

    IPC分类号: F25J3/04

    摘要: In a process and apparatus for air separation by rectification air 1 is preliminarily separated in a first rectification stage 2 of a two-stage rectification column to obtain a nitrogen-rich fraction 4 and an oxygen-rich fraction 8. These two fractions are fed to the second rectification stage 6 and separated into oxygen and nitrogen fractions. An argon-enriched fraction, containing essentially oxygen and argon, is removed from the second rectification stage at an intermediate point and is separated in a raw argon column 10 by rectification into an argon-rich fraction 18 and a liquid fraction 19 containing essentially oxygen. The liquid fraction 19 is fed back into the second rectification stage. Another fraction 22 is removed from the raw argon column above the bottom thereof and is separated in a high-purity oxygen column 23 to produce a high-purity oxygen fraction 25, 26 and a lighter residual fraction 24. An additional nitrogen-rich fraction is removed from the head of the first rectification stage and separated in a high-purity nitrogen column 31 producing a bottom liquid fraction 29, which is fed back to the head of the first rectification stage, and a residual gas fraction 33. A high-purity nitrogen fraction 34 is removed at a point several plates below the head of the first rectification stage.

    摘要翻译: 在二级精馏塔的第一精馏阶段2中,通过精馏空气1进行空气分离的方法和装置预先分离,得到富氮馏分4和富氧馏分8.将这两个馏分进料至 第二精馏段6并分离成氧和氮馏分。 在中间点从第二精馏阶段除去基本上含有氧和氩的富氩馏分,并通过精馏将其在原氩塔10中分离成富氩馏分18和基本上含氧的液体馏分19。 液体馏分19反馈回第二精馏段。 另一部分22从其底部的原氩塔中除去,并在高纯氧塔23中分离,以产生高纯氧分数25,26和较轻的残余馏分24.另外的富氮馏分为 从第一精馏段的头部除去,并在高纯氮塔31中分离,产生反馈到第一精馏段的头部的底部液体馏分29和残余气体馏分33.高纯度 氮馏分34在第一整流段的头部下方的几个板上被去除。

    Multistory bath condenser
    5.
    发明授权
    Multistory bath condenser 失效
    多层浴冷凝器

    公开(公告)号:US07152432B2

    公开(公告)日:2006-12-26

    申请号:US10296883

    申请日:2001-05-31

    IPC分类号: F25J5/00 F25J3/00

    摘要: The invention relates to a bath condenser with a condenser block (1) that has evaporation passages (8) for a liquid and liquefaction passages (2) for a heating medium and at least two circulation sections (7) that are located vertically on top of one another. The evaporation passages (8) each have on the lower end of a circulation section (7) at least one entry opening (9) for the liquid and on the upper end of a circulation section (7) at least one exit opening (10), for each circulation section (7) there being a liquid storage tank (15) that is flow-connected to the entry opening (9) and the exit opening (10) of the circulation section (7) and that has a gas offtake (18). The inlet into the gas offtake (18) is not located in the area in front of the side (12) of the circulation section (7) in which the exit opening (10) of the circulation section (7) is located.

    摘要翻译: 本发明涉及一种具有冷凝器块(1)的浴冷凝器,其具有用于液体的液体和液化通道(2)和用于加热介质的至少两个循环部分(7)的蒸发通道(8),所述循环部分垂直地位于 另一个。 蒸发通道(8)各自在循环部分(7)的下端具有用于液体的至少一个入口(9)和循环段(7)的上端,至少一个出口(10) 对于每个循环部分(7),存在流体连接到循环部分(7)的入口(9)和出口(10)并且具有气体排出口(7)的液体储存罐(15) 18)。 进入气体出口(18)的入口不位于循环部分(7)的出口(10)所在的循环部分(7)的侧面(12)的前面区域。

    Method and device for obtaining nitrogen by low-temperature separation
of air
    7.
    发明授权
    Method and device for obtaining nitrogen by low-temperature separation of air 失效
    通过空气低温分离获得氮的方法和装置

    公开(公告)号:US5964104A

    公开(公告)日:1999-10-12

    申请号:US79236

    申请日:1998-05-15

    申请人: Dietrich Rottmann

    发明人: Dietrich Rottmann

    IPC分类号: F25J3/04 F25J3/00

    摘要: In the method and device, nitrogen is obtained by two-stage rectification of air in a double column. Double column contains a high-pressure column and a medium-pressure column that are in a heat-exchange relationship with each other. Entering air is compressed, purified, cooled in a main heat exchanger against separation products, and fed to rectification. At least one nitrogen product fraction is taken from high-pressure column. A nitrogen gas fraction from double column is heated, expanded, and brought into indirect heat exchange with an oxygen-enriched liquid from the lower region of medium-pressure column. In this way, the nitrogen gas fraction is at least partially condensed and the oxygen-enriched liquid is at least partially evaporated. The condensate formed in the indirect heat exchange is at least partially fed to medium-pressure column. The nitrogen gas fraction is heated upstream of expansion to an intermediate temperature that is between the temperatures at the cold end and the warm end of main heat exchanger.

    摘要翻译: 在该方法和装置中,氮气通过双塔中空气的两级精馏获得。 双柱包含彼此处于热交换关系的高压塔和中压塔。 进入空气被压缩,净化,在主热交换器中冷却分离产物,并进料进行精馏。 从高压塔取出至少一个氮气产物馏分。 来自双塔的氮气馏分被加热,膨胀,并与来自中压塔的下部区域的富氧液体进行间接热交换。 以这种方式,氮气部分至少部分冷凝,富氧液体至少部分蒸发。 在间接热交换中形成的冷凝物至少部分地供给中压塔。 将氮气馏分在膨胀的上游加热至在主热交换器的冷端和暖端之间的温度之间的中间温度。

    PROCESS AND DEVICE FOR LOW-TEMPERATURE SEPARATION OF AIR

    公开(公告)号:US20090188280A1

    公开(公告)日:2009-07-30

    申请号:US12282606

    申请日:2007-03-06

    IPC分类号: F25J3/08

    摘要: The process and the device are used for low-temperature separation of air with a distilling-column system for nitrogen-oxygen separation (20), which has at least one separation column (21, 22). A main air stream (1, 5) is compressed in an air compressor (2) and purified in a purification device (4). A first air stream (7) and a second air stream (8) are diverted from the main air stream (5). The first air stream (7) is further compressed in two secondary compressors (10, 13) that are connected in series. The further compressed first air stream (15) is cooled by indirect heat exchange (16), and at least partially liquefied or pseudo-liquefied, and then introduced into the distilling-column system for nitrogen-oxygen separation (20). The second air stream (8) is cooled by indirect heat exchange (16) and then, divided into two partial streams (24, 27), is actively depressurized in two expanders (25, 28), whereby the two expanders have essentially the same inlet pressure. The actively depressurized partial streams (26, 29) of the second air stream are introduced (30, 129) at least in part into the distilling-column system for nitrogen-oxygen separation (20). The mechanical energy that is produced in the active depressurization (25, 28) of the second air stream is used at least partially in the driving of the two secondary compressors (10, 13) that are connected in series. A liquid product stream (31) is removed from the distilling-column system for nitrogen-oxygen separation (20), brought to an elevated pressure in the liquid state (32), and evaporated or pseudo-evaporated under this elevated pressure by indirect heat exchange (16) with the first air stream (15), and finally removed as a gaseous product stream (34). Both secondary compressors (10, 13) are operated with an inlet temperature that is higher than 250 K, in particular higher than 270 K.

    Plate heat exchanger
    9.
    发明授权
    Plate heat exchanger 失效
    板式换热器

    公开(公告)号:US07188492B2

    公开(公告)日:2007-03-13

    申请号:US10612287

    申请日:2003-07-03

    IPC分类号: F25J3/00 F28D7/10 F28F3/00

    摘要: A plate heat exchanger for indirect heat exchange of several fluid flows (30, 40, 50) with a heat transfer medium/cooling medium (10, 20) in a heat exchanger core (9) has a plurality of heat exchange passages within the core for the heat transfer medium/cooling medium (10, 20), a first fluid flow (30, 40, 50) and a second fluid flow (30, 40, 50). All heat exchange passages for the first fluid flow (40) are located In a first component area, and all heat exchange passages for the second fluid flow (30) are located in a second component area. The first and the second component areas do not intersect and each extend over the entire height of the heat exchanger core (9). The heat exchanger is particularly suitable for use in air-separation processes.

    摘要翻译: 用于在热交换器芯(9)中具有传热介质/冷却介质(10,20)的若干流体流(30,40,50)的间接热交换的板式热交换器具有在所述芯部内的多个热交换通道 用于传热介质/冷却介质(10,20),第一流体流(30,40,50)和第二流体流(30,40,50)。 用于第一流体流(40)的所有热交换通道位于第一组分区域中,并且用于第二流体流(30)的所有热交换通道位于第二组分区域中。 第一和第二组分区域不相交并且各自延伸在热交换器芯(9)的整个高度上。 热交换器特别适用于空气分离过程。

    Process for obtaining gaseous and liquid nitrogen with a variable proportion of liquid product
    10.
    发明授权
    Process for obtaining gaseous and liquid nitrogen with a variable proportion of liquid product 失效
    用可变比例的液体产品获得气态和液氮的方法

    公开(公告)号:US06477860B2

    公开(公告)日:2002-11-12

    申请号:US09810340

    申请日:2001-03-19

    IPC分类号: F25J304

    摘要: In a single column distillation system for obtaining gaseous and liquid nitrogen with a variable proportions of liquid product by low-temperature separation from air, a first portion (12, 13) of nitrogen-rich fraction (5, 7, 8) is fed downstream of circulation compressor (9) to the liquefaction chamber of a condenser-evaporator (14) associated with the single column and condensed under a pressure higher than the operating pressure of the single column (4). A liquid oxygen-enriched fraction (228, 231) from the distillation column system is at least partially evaporated in the evaporation chamber of condenser-evaporator (14). A portion (18) of nitrogen-rich liquid (15, 16) from condenser-evaporator (14) is drawn off at least at times as liquid product. A second oxygen-enriched gas (221, 521) is removed from one of columns (546) of the distillation system and/or from the evaporation chamber of condenser-evaporator (14), machine expanded(23), and heated in main heat exchanger (2).

    摘要翻译: 在用于通过与空气进行低温分离从而获得具有不同比例的液体产物的气态和液氮的单塔蒸馏系统中,将富氮馏分(5,7,8)的第一部分(12,13)进料到下游 的循环压缩机(9)连接到与单塔相关联的冷凝器 - 蒸发器(14)的液化室,并在高于单塔(4)的操作压力的压力下冷凝。 来自蒸馏塔系统的液体富氧馏分(228,231)在冷凝器 - 蒸发器(14)的蒸发室中至少部分蒸发。 至少有时作为液体产物抽出来自冷凝器 - 蒸发器(14)的富氮液体(15,16)的一部分(18)。 第二个富氧气体(221,521)从蒸馏系统的一个塔(546)和/或从冷凝器 - 蒸发器(14)的蒸发室,机器膨胀(23)中的一个中除去,并在主热中加热 交换器(2)。