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公开(公告)号：US4260651A
公开(公告)日：1981-04-07
申请号：US747002
申请日：1976-12-02
申请人： Harold E. Wixon
发明人： Harold E. Wixon
CPC分类号： C11D17/0039 , C11D1/66 , C11D1/72 , C11D17/065 , C11D3/10 , C11D3/128
摘要： A free flowing phosphate-free particulate heavy duty laundry detergent is comprised of particles of a mixture of sodium carbonate and sodium bicarbonate having nonionic detergent in the interior and on the surface thereof, to which is adhered a coating of smaller particles of ion exchanging zeolite. The product made is exceptionally free flowing and, although the particles are relatively large, is also of high bulk density (over 0.6 g./cc.). Also within the invention is a method of making such products by contacting the particles of mixed sodium carbonate and sodium bicarbonate with a normally liquid or pasty nonionic detergent in the liquid state so that the detergent is largely absorbed by the particles and coats the surfaces thereof, which are then coated with powdered zeolite which adheres to the surface nonionic of the particles and makes them free flowing.
摘要翻译： 自由流动的无磷酸盐颗粒重垢洗衣洗涤剂由其内部和表面上具有非离子洗涤剂的碳酸钠和碳酸氢钠的混合物的颗粒组成，附着有较小离子交换沸石颗粒的涂层。 所制造的产品是非常自由流动的，尽管颗粒相对较大，但其堆积密度也高（超过0.6g / cc）。 本发明还有一种通过使混合碳酸钠和碳酸氢钠的颗粒与液态的常规液体或糊状非离子洗涤剂接触使得洗涤剂被颗粒大量吸收并涂覆其表面的方法， 然后用粉末状沸石涂覆，该粉末沸石粘附在非离子表面上并使其自由流动。
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公开(公告)号：US4248911A
公开(公告)日：1981-02-03
申请号：US746900
申请日：1976-12-02
申请人： Harold E. Wixon
发明人： Harold E. Wixon
CPC分类号： C11D1/66 , C11D17/065 , C11D3/06 , C11D3/128
摘要： A free flowing particulate heavy duty laundry detergent containing no more than 8.7% of phosphorus (from phosphate) is comprised of sodium tripolyphosphate particles having nonionic detergent in the interior and on the surface thereof, which adheres a coating of smaller particles of ion-exchanging zeolite to the phosphate. Also within the invention is a method of making such a product by pre-mixing spray dried sodium tripolyphosphate particles and smaller zeolite particles and admixing with them, as by spraying, in liquid form, onto moving particles, a normally liquid or pasty nonionic detergent, such as a higher fatty alcohol polyethylene oxide condensation product, which penetrates the sodium tripolyphosphate particles and adheres zeolite particles to the surfaces thereof.
摘要翻译： 含有不超过8.7％的磷（来自磷酸盐）的自由流动的颗粒重型洗衣洗涤剂由其内部和表面上具有非离子洗涤剂的三聚磷酸钠颗粒组成，其粘附较小颗粒的离子交换沸石 到磷酸盐。 本发明还有一种通过将喷雾干燥的三聚磷酸钠颗粒和较小的沸石颗粒预先混合并与其混合的方法，通过以液体形式喷洒到移动的颗粒，常规液体或糊状非离子洗涤剂上， 例如高级脂肪醇聚氧乙烯缩合产物，其渗透三聚磷酸钠颗粒并将沸石颗粒粘附到其表面。
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公开(公告)号：US4224250A
公开(公告)日：1980-09-23
申请号：US802933
申请日：1977-06-02
申请人： Harold E. Wixon
发明人： Harold E. Wixon
IPC分类号： D06M13/385 , C07C83/00 , C07C87/16 , D06M13/38
CPC分类号： D06M13/385
摘要： Novel fabric conditioning compounds are formed by reacting a higher alkyl-1, 2-epoxide with a lower alkanediamine. The compounds may be incorporated into a laundry product and used in the wash cycle or may be applied in either the wash cycle or the rinse cycle.
摘要翻译： 通过使高级烷基-2-环氧化物与低级链烷二胺反应形成新的织物调理化合物。 化合物可以并入洗衣产品中并且在洗涤循环中使用，或者可以在洗涤循环或漂洗循环中施用。
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公开(公告)号：US3997453A
公开(公告)日：1976-12-14
申请号：US595104
申请日：1975-07-11
申请人： Harold E. Wixon
发明人： Harold E. Wixon
IPC分类号： C11D1/14 , C11D1/22 , C11D1/62 , C11D1/65 , C11D3/00 , D06M13/256 , D06M13/463 , D06M13/473 , D06M13/32 , D06M13/46
CPC分类号： D06M13/256 , C11D1/65 , C11D3/0015 , D06M13/463 , D06M13/473 , C11D1/14 , C11D1/22 , C11D1/62
摘要： Stable, fabric softening compositions having improved dispersibility in cold water are provided comprising a cationic quaternary ammonium softener as the sole fabric softening agent and an organic, anionic sulfonate, the weight ratio of cationic softener to anionic sulfonate being from about 80:1 to 3:1 and preferably 50:1 to 4:1 and more preferably 40:1 to 5:1. The presence of the cationic softener material in the described excess quantities assures a softening composition in the form of a stable, opaque, homogeneous liquid which is readily dispersible in water and having excellent softening properties with respect to various types of textile products.
摘要翻译： 提供了稳定的，在冷水中具有改善的分散性的织物柔软组合物，其包含阳离子季铵软化剂作为唯一织物软化剂和有机阴离子磺酸盐，阳离子软化剂与阴离子磺酸盐的重量比为约80:1至3:1， 1，优选为50：1〜4：1，更优选为40：1〜5：1。 所述过量的阳离子软化剂材料的存在确保柔软组合物的形式为稳定的，不透明的均匀液体，其易于分散在水中并且对于各种类型的纺织产品具有优异的软化性能。
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公开(公告)号：US4664817A
公开(公告)日：1987-05-12
申请号：US355242
申请日：1982-03-05
申请人： Harold E. Wixon
发明人： Harold E. Wixon
CPC分类号： C11D17/0039 , C11D1/72 , C11D17/065 , C11D3/001 , C11D3/1246
摘要： A free flowing, particulte detergent-softener of high bulk density is comprised of nucleus particles of builder salt, preferably a mixture of sodium carbonate and sodium bicarbonate, having nonionic detergent in the interior and on the surface thereof, to which is adhered a coating of smaller particles of ion exchanging zeolite, and quaternary ammonium halide fabric softening compound. In a preferred embodiment of the invention the quaternary ammonium halide is "insulated" from immediate contact with laundry when the detergent-softener is added to the wash water by being added to the nucleus particles with the nonionic detergent, after which the resulting particles are coated with the zeolite powder. In another embodiment of the invention the product described is further coated with nonionic detergent and zeolite.
摘要翻译： 自由流动的高堆积密度的洗涤剂 - 软化剂由助洗剂盐的核颗粒，优选碳酸钠和碳酸氢钠的混合物组成，在其内部和表面上具有非离子洗涤剂，其中粘附有 较小的离子交换沸石颗粒和季铵卤化物织物柔软化合物。 在本发明的一个优选实施方案中，当洗涤剂 - 软化剂通过用非离子型洗涤剂加入到核颗粒中而将洗涤剂 - 软化剂加入洗涤水中时，季铵卤化物“与绝缘”与衣物立即接触，然后将所得颗粒涂布 与沸石粉末。 在本发明的另一个实施方案中，所描述的产品进一步用非离子洗涤剂和沸石涂覆。
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公开(公告)号：US4524012A
公开(公告)日：1985-06-18
申请号：US500590
申请日：1983-06-08
申请人： Harold E. Wixon
发明人： Harold E. Wixon
摘要： A fabric softening and fluffing particulate detergent composition comprises a detersive proportion of an anionic synthetic organic detergent, such as sodium linear higher alkylbenzene sulfonate, a building proportion of a builder for the detergent, such as sodium tripolyphosphate, sodium carbonate and/or sodium silicate, a fabric softening proportion of bentonite, and a softening and fluffing proportion of a magnesium salt, which is at least slightly water soluble, such as magnesium sulfate. The basic detergent composition, containing the detergent and builder, sometimes with inert filler and preferably with desirable adjuvants, is preferably in the form of spray dried beads, and the bentonite and magnesium salt are preferably agglomerated together to particles of about the same size as the spray dried beads, and are mixed with the spray dried beads.The invention also relates to the mentioned agglomerate and to processes for making the detergent composition and the agglomerate.
摘要翻译： 织物软化和绒毛颗粒洗涤剂组合物包含去污剂比例的阴离子合成有机洗涤剂，例如线性高级烷基苯磺酸钠，用于洗涤剂的助洗剂如建筑物比例，例如三聚磷酸钠，碳酸钠和/或硅酸钠， 膨润土的织物软化比例，以及至少微溶于水的镁盐如硫酸镁的软化起毛比例。 含有洗涤剂和助洗剂的基本洗涤剂组合物有时具有惰性填料并且优选具有所需的助剂，优选为喷雾干燥珠的形式，并且膨润土和镁盐优选聚集在一起，与大约相同尺寸的颗粒 喷雾干燥的珠粒，并与喷雾干燥的珠粒混合。 本发明还涉及所述附聚物以及制备洗涤剂组合物和附聚物的方法。
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公开(公告)号：US4462804A
公开(公告)日：1984-07-31
申请号：US427945
申请日：1982-09-29
CPC分类号： C11D17/065 , C11D1/72 , C11D11/02 , C11D3/10 , C11D3/128
摘要： A free flowing phosphate-free high bulk density particulate heavy duty laundry detergent is comprised of particles of spray dried base beads containing ion exchanging zeolite, sodium carbonate and sodium bicarbonate into which is absorbed a nonionic detergent. The product is made by spray drying an aqueous mixture of the zeolite, carbonate and bicarbonate, optionally with soluble silicate present too, decomposing some of the bicarbonate to carbonate during the drying operation and mixing nonionic detergent in liquid form with the spray dried base beads produced and absorbing such detergent into such beads.
摘要翻译： 自由流动的无磷酸盐高体积密度颗粒重型衣物洗涤剂由含有离子交换沸石，碳酸钠和碳酸氢钠的喷雾干燥的基础颗粒的颗粒组成，其中吸收了非离子洗涤剂。 该产品通过喷雾干燥沸石，碳酸盐和碳酸氢盐的水性混合物，任选地含有可溶性硅酸盐，在干燥操作期间将一些碳酸氢盐分解成碳酸盐，并将液体形式的非离子洗涤剂与产生的喷雾干燥的基料珠混合 并将这种洗涤剂吸收到这种珠子中。
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公开(公告)号：US4427410A
公开(公告)日：1984-01-24
申请号：US338614
申请日：1982-01-11
申请人： William Chirash , Harold E. Wixon
发明人： William Chirash , Harold E. Wixon
摘要： A wash cycle fabric softening composition contains a water soluble organic cationic fabric softening agent and a water insoluble molecular sieve zeolite, usually in a weight ratio of 1:1 to 1:20. The composition effectively softens fabrics, reduces or eliminates static cling and is compatible with organic detergents, providing an excellent building effect, in detergent-softener combinations, even with wash waters of high calcium hardnesses and has good, low residue deposition characteristics. The composition may also contain a water soluble organic detergent and/or a bleaching agent.
摘要翻译： 洗涤循环织物软化组合物含有水溶性有机阳离子织物软化剂和水不溶性分子筛沸石，通常重量比为1：1至1:20。 该组合物即使在高钙硬度的洗涤水中也能有效地软化织物，减少或消除静电粘附，并且与洗涤剂 - 柔软剂组合中的有机洗涤剂相容，提供优异的建筑效果，并且具有良好的低残留沉积特性。 组合物还可以含有水溶性有机洗涤剂和/或漂白剂。
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公开(公告)号：US4347152A
公开(公告)日：1982-08-31
申请号：US183021
申请日：1980-09-02
申请人： Harold E. Wixon
发明人： Harold E. Wixon
CPC分类号： C11D17/0039 , C11D1/66 , C11D3/10 , C11D3/128
摘要： A free flowing phosphate-free particulate heavy duty laundry detergent is comprised of particles of a mixture of sodium carbonate and sodium bicarbonate having nonionic detergent in the interior and on the surface thereof, to which is adhered a coating of smaller particles of ion exchanging zeolite. The product made is exceptionally free flowing and, although the particles are relatively large, is also of high bulk density (over 0.6 g./cc.). Also within the invention is a method of making such products by contacting the particles of mixed sodium carbonate and sodium bicarbonate with a normally liquid or pasty nonionic detergent in the liquid state so that the detergent is largely absorbed by the particles and coats the surfaces thereof, which are then coated with powdered zeolite which adheres to the surface nonionic of the particles and makes them free flowing.
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公开(公告)号：US4326971A
公开(公告)日：1982-04-27
申请号：US259728
申请日：1981-05-01
申请人： Harold E. Wixon
发明人： Harold E. Wixon
IPC分类号： C11D1/14 , C11D1/62 , C11D1/72 , C11D3/00 , C11D3/22 , C11D10/04 , C11D1/86 , C11D3/04 , C11D17/06 , D06M13/48
摘要： The present invention provides heavy duty detergent compositions, particularly for imparting improved softness and detersive effects to fabrics laundered therewith, said composition including in addition to conventional builder and principally anionic surfactant components, cationic softener of the di-lower-di-higher alkyl quaternary ammonium and/or heterocyclic imide type, e.g. imidazolinium, and a mixture of fatty acid soap, nonionic organic surfactant, and magnesium sulfate, the weight ratio of soap to softener being about 8:1 to 1:3 preferably 5:1 to 1:2, more preferably 3:2:2:3, e.g., about unity. The soap-nonionic surfactant magnesium sulfate mixture is in the form of a spaghetti, flake, or other shape and is present in the product composition as substantially homogeneously dispersed, discrete particles. A process of laundering fabrics using the above-mentioned composition is also disclosed.
摘要翻译： 本发明提供重垢洗涤剂组合物，特别是用于赋予对其洗涤的织物提高的柔软度和去污效果，所述组合物除了常规助洗剂和主要是阴离子表面活性剂组分外，还包括二低级二高级烷基季铵盐的阳离子软化剂 和/或杂环酰亚胺类型，例如 咪唑啉鎓和脂肪酸皂，非离子有机表面活性剂和硫酸镁的混合物，皂与软化剂的重量比为约8:1至1:3，优选5:1至1:2，更优选3:2:2 ：3，例如关于团结。 皂 - 非离子表面活性剂硫酸镁混合物是意大利面，薄片或其他形状的形式，并且作为基本上均匀分散的离散颗粒存在于产品组合物中。 还公开了使用上述组合物洗涤织物的方法。
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